IP Library Granted Patent US 10,189,963
Granted Patent B2
US 10,189,963 · App. 14/851,054 · Granted Jan 29, 2019

Additives for improving polyurethane foam performance

Inventors: Juan Jesus Burdeniuc (Colmar, PA); James Douglas Tobias (Center Valley, PA); Renee Jo Keller (Orwigsburg, PA); You-Moon Jeon (Breinigsville, PA)
Assignee: Evonik Degussa GmbH
C08J9/0042C08G18/1825C08G18/1875C08G18/325C08G18/3268C08G18/3838C08G18/4841C08G18/6688C08G18/678C08K5/31C08G2101/00C08G2101/005C08G2101/0008C08G2101/0083C08G2290/00C08J2375/08
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Quick Facts
Patent No.
US 10,189,963
App. No.
14/851,054
Granted
Jan 29, 2019
Kind
B2
Abstract

Polyurethane foam compositions and processes to make flexible polyurethane foams are disclosed. Polyurethane foam is produced in the presence of additives comprising guanidine derivatives. Improvements in physical properties such as air flow, dimensional stability, tensile, tear, elongation and foam hardness is observed when these additives are present in polyurethane formulations. In addition, these additives can minimize polymer degradation under humid ageing conditions resulting in foam products with better mechanical properties.

Claims (16)

1. A composition comprising: at least one polyol, at least one blowing agent, at least one catalyst, at least one surfactant, and a solution comprising dimethyl sulfoxide and at least one guanidine derivative selected from the group consisting of guanidine hydrochloride salt, guanidine phosphate salts, guanidine sulfate salts, cyano guanidine, 1-acetylguanidine, nitroguanidine, 1-(o-tolyl)-biguanidine, and mixtures thereof.

2. The composition of claim 1 wherein the catalyst comprises at least one tertiary amine.

3. The composition of claim 1 wherein the polyol comprises at least one polyether polyol.

4. The composition of claim 1 wherein the blowing agent comprises water.

5. The composition of claim 1 wherein the surfactant comprises at least one silicone surfactant.

6. A composition comprising: at least one polyether polyol, water, at least one tertiary amine catalyst, at least one silicone surfactant, at least one cross linker and a solution comprising dimethyl sulfoxide and at least one guanidine derivative selected from the group consisting of guanidine hydrochloride salt, guanidine phosphate salts, guanidine sulfate salts, and cyano guanidine.

7. The composition of claim 6 wherein the cross linker comprises at least one compound containing at least two moieties selected from hydroxyl groups, primary amino groups, secondary amino groups, and other active hydrogen-containing groups which are reactive with an isocyanate group.

8. The composition of claim 6 wherein the cross linker comprises at least one member selected from the group consisting of polyhydric alcohols, polyamines, diethyltoluenediamine, chlorodiaminobenzene, diethanolamine, diisopropanolamine, triethanolamine, tripropanolamine, and 1,6-hexanediamine.

9. The composition of claim 1 further comprising at least one polyol selected from the group consisting of graft polyols, polyurea modified polyols, and combinations thereof.

10. The composition of claim 1 wherein the guanidine derivative is present and in an amount less than about 1.0 pphp.

11. The composition of claim 9 wherein the polyol comprises the graft polyol.

12. The composition of claim 11 wherein the graft polyol comprises a homopolymer of styrene.

13. The composition of claim 11 wherein the graft polyol comprises a homopolymer of acrylonitrile.

14. The composition of claim 11 wherein the graft polyol comprises a homopolymer of styrene and a homopolymer of acrylonitrile.

15. The composition of claim 9 wherein the polyol comprises the polyurea modified polyol.

16. The composition of claim 15 wherein the polyurea modified polyol comprises a polyisocyanate polyaddition polylol.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2019
From: EVONIK DEGUSSA GMBH
To: EVONIK OPERATIONS GMBH
Reel/Frame 051284/0491 →
CORRECTIVE ASSIGNMENT TO CORRECT THE THIRD AND FOURTH INVENTORS EXECUTION DATES PREVIOUSLY RECORDED AT REEL: 043547 FRAME: 0070. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Oct 10, 2017
From: BURDENIUC, JUAN JESUS; TOBIAS, JAMES DOUGLAS; KELLER, RENEE JO; JEON, YOU-MOON
To: AIR PRODUCTS AND CHEMICALS, INC.
Reel/Frame 044166/0431 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 11, 2017
From: BURDENIUC, JUAN JESUS; TOBIAS, JAMES DOUGLAS; KELLER, RENEE JO; JEON, YOU-MOON
To: AIR PRODUCTS AND CHEMICALS, INC.
Reel/Frame 043547/0070 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 4, 2017
From: AIR PRODUCTS AND CHEMICALS, INC.
To: EVONIK DEGUSSA GMBH
Reel/Frame 042402/0301 →
Continuity (3)
Continuation 13178558 · Jul 8, 2011
Provisional Application 61362964 · Jul 9, 2010
Related Publication 20160002425A1 · Jan 7, 2016
Cited By (2)
US 12,595,332 US 12,662,566