IP Library Granted Patent US 10,441,659
Granted Patent B2
US 10,441,659 · App. 14/872,951 · Granted Oct 15, 2019

Lipids for therapeutic agent delivery formulations

Inventors: Joseph E. Payne (Oceanside, CA); John A. Gaudette (Poway, CA); Zheng Hou (San Diego, CA); Mohammad Ahmadian (Carlsbad, CA); Lei Yu (Carlsbad, CA); Victor Knopov (Oceanside, CA); Violetta Akopian (Oceanside, CA); Priya Karmali (San Diego, CA); Richard P. Witte (San Diego, CA); Neda Safarzadeh (Poway, CA); Wenbin Ying (San Diego, CA); Jun Zhang (San Diego, CA)
Assignee: Nitto Denko Corporation
A61K47/20A61K9/1272A61K47/14A61K47/18A61K47/22C07C235/08C07C237/08C07C237/16C07C271/16C07C317/44C07C323/60C07C333/04C07D207/16C07D333/38C07D333/40Y10T428/2998
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Quick Facts
Patent No.
US 10,441,659
App. No.
14/872,951
Granted
Oct 15, 2019
Kind
B2
Abstract

The description is directed to ionizable lipids useful for enhancing the delivery of therapeutic agents in liposomes.

Claims (67)

1. A composition comprising lipid molecules comprising an ionizable lipid compound of formula I:

wherein

n and m are independently 1, 2, 3, or 4;

R 1 and R 2 are independently C 10-18 alkyl-;

X is —CH 2 —, wherein L is —OC 1-4 alkylene- or

—OC(O)C 1-4 alkylene-; or

X is absent, wherein L is —C 1 alkylene-, —C 3 alkylene-, —C 4 alkylene-, —OC 1-4 alkylene-, or —OC(O)C 1-4 alkylene-; or

X is O or N, wherein L is —C 1-4 alkylene-, or

—C(O)C 1-4 alkylene-;

or a pharmaceutically acceptable salt form thereof;

and a cationic lipid, wherein the cationic lipid is

2. The composition of claim 1 , comprising the compound of formula I, wherein n and m are 1 or 2.

3. The composition of claim 1 , comprising the compound of formula I, wherein X is absent.

4. The composition compound of claim 3 , comprising the compound of formula I, wherein L is —OC 1-4 alkylene-, or —OC(O)C 1-4 alkylene-.

5. The composition of claim 3 , comprising the compound of formula I, wherein L is —CH 2 —, —CH 2 CH 2 CH 2 —, or —CH 2 CH 2 CH 2 CH 2 —.

6. The composition of claim 1 , comprising the compound of formula I, wherein X is —CH 2 —.

7. The composition of claim 6 , comprising the compound of formula I, wherein L is —OC 1-4 alkylene-.

8. The composition of claim 7 , comprising the compound of formula I, wherein L is —OCH 2 CH 2 — or —OCH 2 CH 2 CH 2 —.

9. The composition of claim 6 , comprising the compound of formula I, wherein L is —OC(O)C 1-4 alkylene-.

10. The composition of claim 9 , comprising the compound of formula I, wherein L is —OC(O)CH 2 CH 2 CH 2 —.

11. The composition of claim 1 , comprising the compound of formula I, wherein X is O.

12. The composition of claim 1 , comprising the compound of formula I, wherein R 1 and R 2 are each C 10-18 alkyl-.

13. The composition of claim 12 , comprising the compound of formula I, wherein R 1 and R 2 are each C 13 alkyl-.

14. A composition comprising a compound selected from the group consisting of

or a pharmaceutically acceptable salt form thereof;

and a cationic lipid, wherein the cationic lipid is

15. The composition of claim 1 , wherein the ionizable lipid compound is 5 to 50 mol % of the total lipid molecules.

16. A composition comprising lipid molecules comprising an ionizable lipid compound of formula I:

wherein

n and m are independently 1, 2, 3, or 4;

R 1 and R 2 are independently C 10-18 alkyl-;

X is absent;

L is —CH 2 CH 2 —;

or a pharmaceutically acceptable salt form thereof;

and a cationic lipid, wherein the cationic lipid is

17. The composition of claim 16 , wherein the ionizable lipid compound of formula I consists of

18. A composition comprising lipid molecules comprising an ionizable lipid compound of formula I:

wherein

n and m are independently 2, 3, or 4;

R 1 and R 2 are independently C 12-18 alkenyl-;

X is absent;

L is —CH 2 CH 2 —;

or a pharmaceutically acceptable salt form thereof;

and a cationic lipid, wherein the cationic lipid is

19. A composition comprising lipid molecules comprising an ionizable lipid compound of formula I:

wherein

n and m are independently 2, 3, or 4;

R 1 and R 2 independently are a C 12-18 alkenyl-;

X is —CH 2 —, wherein L is —OC 1-4 alkylene or —OC(O)C 1-4 alkylene-; or

X is absent, wherein L is C 1 -C 4 alkylene, —OC 1-4 alkylene, or

—OC(O)C 1-4 alkylene-; or

X is O or N, wherein L is —C 1-4 alkylene-, or

—C(O)C 1-4 alkylene-;

or a pharmaceutically acceptable salt form thereof;

and a cationic lipid, wherein the cationic lipid is

20. The composition of claim 19 , wherein the ionizable lipid compound of formula I consists of i-Pr-DODC

21. A composition comprising lipid molecules comprising an ionizable lipid compound of formula I:

wherein

n and m are 1;

R 1 and R 2 independently are a C 12-18 alkenyl;

X is —CH 2 —, wherein L is —OC 1-4 alkylene- or —OC(O)C 1-4 alkylene-; or

X is absent, wherein L is —C 1-4 alkylene-, —OC 1-4 alkylene-, or —OC(O)C 1-4 alkylene-; or

X is O or N, wherein L is —C 1-4 alkylene-, or

—C(O)C 1-4 alkylene-;

or a pharmaceutically acceptable salt form thereof;

and a cationic lipid, wherein the cationic lipid is

22. The composition of claim 21 , wherein the ionizable lipid compound of formula I consists of C104-DO

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2019
From: YU, LEI
To: NITTO DENKO CORPORATION
Reel/Frame 050946/0264 →
Continuity (3)
Division 13913918 · Jun 10, 2013
Provisional Application 61657480 · Jun 8, 2012
Related Publication 20160074514A1 · Mar 17, 2016
Cited By (2)
US 12,319,643 US 12,721,909