IP Library Granted Patent US 9,970,032
Granted Patent B2
US 9,970,032 · App. 14/886,983 · Granted May 15, 2018

Biorefinery system, methods and compositions thereof

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Quick Facts
Patent No.
US 9,970,032
App. No.
14/886,983
Granted
May 15, 2018
Kind
B2
Abstract

The present disclosure relates to bioengineering approaches for producing biofuel and, in particular, to the use of a C 1 metabolizing microorganism reactor system for converting C 1 substrates, such as methane or methanol, into biomass and subsequently into biofuels, bioplastics, or the like.

Claims (22)

1. A method for making fuel, comprising converting biomass from a culture primarily comprising methanotrophic bacteria grown under unbalanced growth conditions on a C 1 substrate comprising methane and/or methanol as a carbon source, into an oil composition and refining the oil composition into a liquid fuel, wherein the methanotrophic bacteria grown under unbalanced growth conditions contain an increased amount of lipid to total biomass yield as compared to a parent methanotrophic bacteria grown under balanced growth conditions, and wherein the culture is a mixed culture comprising the methanotrophic bacteria and one or more heterologous organisms.

2. The method of claim 1 , wherein the oil composition is from cell membrane of the methanotrophic bacteria.

3. The method of claim 1 , wherein the C 1 substrate is natural gas or methane.

4. The method of claim 1 , wherein the culture is grown in a controlled culturing unit, the controlled culturing unit being a fermentor or bioreactor.

5. The method of claim 1 , wherein the culture is from a liquid-phase fermentation or a solid phase fermentation.

6. The method of claim 1 , wherein the biomass is converted into an oil composition by extraction, wherein the extraction is selected from a wet extraction, a supercritical fluid extraction, or a dry extraction.

7. The method of claim 6 , wherein the extraction is a wet extraction, which comprises use of a polar solvent, non-polar solvent, neutral solvent, acidic solvent, hexane, or any combination thereof.

8. The method of claim 4 , wherein the controlled culturing unit is a solid phase fermentation unit and the oil composition is extracted from the biomass by supercritical fluid extraction.

9. The method of claim 8 , wherein the supercritical fluid comprises CO 2 .

10. The method of claim 1 , wherein the oil composition is refined by a process of cracking, transesterification, reforming, distilling, hydroprocessing, isomerization, or a combination thereof.

11. The method of claim 10 , wherein the hydroprocessing is hydrogenation, hydrotreating, hydrocracking, hydroisomerization, or a combination thereof.

12. The method of claim 11 , wherein the hydrotreating is hydrodenitrogenation (HDN), hydrodeoxygenation (HDO), hydrodesulfurization (HDS), hydrodemetallization (HDM), saturation of olefins, distillate hydrotreating, vacuum gas oil hydrotreating, fixed-bed residue hydrotreating, or a combination thereof.

13. The method of claim 10 , wherein the cracking is catalytic cracking, fluid catalytic cracking, steam cracking, hydrocracking, thermal cracking, thermal catalytic cracking, or a combination thereof.

14. The method of claim 1 , wherein the liquid fuel comprises jet fuel, diesel fuel, paraffinic kerosene, gasoline, or any combination thereof.

15. The method of claim 1 , wherein the methanotrophic bacteria is a Methylomonas, Methylobacter, Methylococcus, Methylosinus, Methylocystis, Methylomicrobium, Methanomonas , or a combination thereof.

16. The method of claim 1 , wherein the methanotrophic bacteria is a Methylomonas sp. 16a, Methylosinus trichosporium, Methylosinus sporium, Methylocystis parvus, Methylomonas methanica, Methylomonas albus, Methylobacter capsulatus, Methylobacterium organophilum, Methylomonas sp. AJ-3670, Methylocella silvestris, Methylacidiphilum infernorum, Methylibium petroleiphilum, Methylomicrobium alcaliphilum , or a high growth variant thereof.

17. The method of claim 1 , wherein the methanotrophic bacteria is Methylobacterium extorquens, Methylobacterium radiotolerans, Methylobacterium populi, Methylobacterium chloromethanicum, Methylobacterium nodulans , or a high growth variant thereof.

18. The method of claim 1 , wherein the methanotrophic bacteria is an obligate methanotrophic bacteria.

19. The method of claim 1 , wherein the methanotrophic bacteria is a recombinant methanotrophic bacteria comprising a heterologous polynucleotide encoding a fatty acid producing enzyme, a formaldehyde assimilation enzyme, or a combination thereof.

20. The method of claim 1 , wherein the biomass is from (a) the methanotrophic bacteria cultured under aerobic conditions with the C 1 substrate comprising methane; or (b) methanotrophic bacteria cultured with the C 1 substrate comprising methane, and the unbalanced growth condition comprises a limiting nutrient selected from phosphorus, nitrogen, trace elements, oxygen, or any combination thereof.

21. The method of claim 1 , wherein the process is carried out at a biorefinery.

22. The method of claim 1 , wherein the unbalanced growth conditions comprises methanotrophic bacteria grown on unbalanced media comprising a limiting quantity of phosphorus, nitrogen, trace elements, oxygen, or any combination thereof.

Assignments (4)
RELEASE OF SECURITY INTEREST Recorded Sep 12, 2025
From: VENTURE LENDING & LEASING IX, INC.
To: CALYSTA, INC.
Reel/Frame 072242/0047 →
SECURITY INTEREST Recorded Oct 7, 2024
From: CALYSTA, INC.
To: AQUA-SPARK CALYSTA LLC
Reel/Frame 069116/0150 →
SECURITY INTEREST Recorded Feb 29, 2024
From: CALYSTA, INC.
To: OCEAN 14 CAPITAL FUND 1 SCSP
Reel/Frame 066607/0888 →
SECURITY INTEREST Recorded Aug 27, 2021
From: CALYSTA, INC.
To: VENTURE LENDING & LEASING IX, INC.
Reel/Frame 057337/0355 →