IP Library Granted Patent US 9,540,399
Granted Patent B2
US 9,540,399 · App. 14/888,581 · Granted Jan 10, 2017

Quinolone derivatives

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Quick Facts
Patent No.
US 9,540,399
App. No.
14/888,581
Granted
Jan 10, 2017
Kind
B2
Abstract

The invention relates to antibacterial compounds of formula I wherein R 1 , U, V and A are as defined in the description, to pharmaceutical compositions containing them and uses of these compounds in the manufacture of medicaments for the treatment of bacterial infections.

Claims (52)

1. A compound of formula I

wherein

R 1 represents (C 1 -C 3 )alkyl, or (C 3 -C 5 )cycloalkyl;

U represents CH or N;

V represents O or S; and

A represents a linker of 1-, 2-, or 3-membered saturated straight chain group which is attached to, or interrupted by a 6-membered cyclic group selected from cyclohexan-1,4-diyl, piperidin-1,4-diyl, or piperazin-1,4-diyl; wherein said linker group has a total of two or three nitrogen atoms, wherein said nitrogen atoms are separated from each other by at least two carbon atoms;

or a pharmaceutically acceptable salt thereof.

2. The compound of formula I according to claim 1 , wherein

R 1 represents methyl or ethyl; or R 1 represents cyclopropyl;

U represents CH or N;

V represents O or S;

and

A represents a group selected from:

wherein

D represents a bond or CH 2 ; and

E represents a bond, CH 2 or CH 2 CH 2 ;

or a pharmaceutically acceptable salt thereof.

3. The compound of formula I according to claim 2 , wherein R 1 represents methyl; or a pharmaceutically acceptable salt thereof.

4. The compound of formula I according to claim 2 , wherein R 1 represents cyclopropyl; or a pharmaceutically acceptable salt thereof.

5. The compound of formula I according to claim 1 , wherein V represents S; or a pharmaceutically acceptable salt thereof.

6. The compound of formula I according to claim 1 , wherein U represents N; or a pharmaceutically acceptable salt thereof.

7. The compound of formula I according to claim 1 , wherein A represents a group selected from:

or a pharmaceutically acceptable salt thereof.

8. The compound of formula I according to claim 1 , wherein A represents a group selected from:

or a pharmaceutically acceptable salt thereof.

9. The compound of formula I according to claim 1 , wherein the compound is:

1-Cyclopropyl-6-fluoro-4-oxo-7-(4-{[(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]thiazin-6-ylmethyl)-amino]-methyl}-cyclohexylamino)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-{4-[(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]thiazin-6-ylmethyl)-amino]-cyclohexylamino}-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-(2-{4-[(3-oxo-3,4-dihydro-2H-pyrido [3,2-b][1,4]thiazin-6-ylmethyl)-amino]-piperidin-1-yl}-ethyl)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-(4-{2-[(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]thiazin-6-ylmethyl)-amino]-ethyl}-piperazin-1-yl)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-(4-{2-[(3-oxo-3,4-dihydro-2H-pyrido [3,2-b][1,4]thiazin-6-ylmethyl)-amino]-ethyl}-piperidin-1-yl)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-{2-[1-(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]thiazin-6-ylmethyl)-piperidin-4-yl]-ethylamino}-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-(4-{[(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]thiazin-6-ylmethyl)-amino]-methyl}-piperidin-1-yl)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-(4-{[(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-ylmethyl)-amino]-methyl}-cyclohexylamino)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-(4-{[(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]thiazin-6-ylmethyl)-amino]-methyl}-piperidin-1-ylmethyl)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

1-Cyclopropyl-6-fluoro-4-oxo-7-{4-{[(3-oxo-3,4-dihydro-2H-pyrido [3,2-b][1,4]thiazin-6-ylmethyl)-amino]-piperidin-1-yl}-1,4-dihydro-[1, 8]naphthyridine-3-carboxylic acid; or

1-Cyclopropyl-6-fluoro-4-oxo-7-(4-{2-[(3-oxo-3,4-dihydro-2H-pyrido [3,2-b][1,4]thiazin-6-ylmethyl)-amino]-ethyl}-piperazin-1-yl)-1,4-dihydro-quinoline-3-carboxylic acid;

or a pharmaceutically acceptable salt thereof.

10. The compound of formula I according to claim 1 , wherein the compound is:

1-Cyclopropyl-6-fluoro-4-oxo-7-(4-{2-[(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-ylmethyl)-amino]-ethyl}-piperazin-1-yl)-1,4-dihydro-[ 1,8]naphthyridine-3-carboxylic acid;

trans-6-Fluoro-1-methyl-4-oxo-7-(4-{[(3-oxo-3,4-dihydro-2H-pyrido [3,2-b][1,4]thiazin-6-ylmethyl)-amino]-methyl}-cyclohexylamino)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

trans-6-Fluoro-1-methyl-4-oxo-7-(4-{[(3-oxo-3,4-dihydro-2H-pyrido [3,2-b][1,4]oxazin-6-ylmethyl)-amino]-methyl}-cyclohexylamino)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

trans-1-Ethyl-6-fluoro-4-oxo-7-(4-{[(3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]thiazin-6-ylmethyl)-amino]-methyl}-cyclohexylamino)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

6-Fluoro-1-methyl-4-oxo-7-(4-{2-[(3-oxo-3,4-dihydro-2H-pyrido [3,2-b][1,4]oxazin-6-ylmethyl)-amino]-ethyl}-piperidin-1-yl)-1,4-dihydro-[1, 8]naphthyridine-3-carboxylic acid; or

6-Fluoro-1-methyl-4-oxo-7-(4-{2-[(3-oxo-3,4-dihydro-2H-pyrido [3,2-b][1,4]thiazin-6-ylmethyl)-amino]-ethyl}-piperidin-1-yl)-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid;

or a pharmaceutically acceptable salt thereof.

11. The compound of formula I according to claim 1 , formulated as a medicament, or a pharmaceutically acceptable salt thereof.

12. A pharmaceutical composition comprising, as active principle, the compound of formula I according to claim 1 , or a pharmaceutically acceptable salt thereof, and at least one therapeutically inert excipient.

13. A method of treating a bacterial infection comprising administering to a subject in need thereof a compound according to claim 1 .

14. The method according to claim 13 , wherein said bacterial infection is nosocomial pneumonia, urinary tract infections, systemic infections, skin and soft tissue infections, surgical infections, intraabdominal infections, lung infections, endocarditis, diabetic foot infections, osteomyelitis, or central nervous system infections.

15. The method according to claim 13 , wherein said bacterial infection is mediated by fermentative or non-fermentative Gram negative bacteria.

16. The method according to claim 13 , wherein said bacterial infection is mediated by Acinetobacter baumannii, Burkholderia, Citrobacter spp., Enterobacter aerogenes, Enterobacter cloacae, Escherichia coli, Klebsiella oxytoca, Klebsiella pneumoniae, Serratia marcescens, Stenotrophomonas maltophilia , or Pseudomonas aeruginosa.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE ADDRESS PREVIOUSLY RECORDED AT REEL: 042464 FRAME: 0407. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 28, 2017
From: ACTELION PHARMACEUTICALS LTD
To: IDORSIA PHARMACEUTICALS LTD
Reel/Frame 043017/0022 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 13, 2017
From: ACTELION PHARMACEUTICALS LTD
To: IDORSIA PHARMACEUTICALS LTD
Reel/Frame 042464/0407 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2015
From: ENDERLIN-PAPUT, STEPHANIE; HUBSCHWERLEN, CHRISTIAN; RUEEDI, GEORG; ZUMBRUNN, CORNELIA
To: ACTELION PHARMACEUTICALS LTD
Reel/Frame 037175/0359 →