IP Library Granted Patent US 9,650,661
Granted Patent B2
US 9,650,661 · App. 14/891,760 · Granted May 16, 2017

Nanostructured spore carrier

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Quick Facts
Patent No.
US 9,650,661
App. No.
14/891,760
Granted
May 16, 2017
Kind
B2
Abstract

Spore carriers suitable for use in biological indicators are described. The spore carriers include a substrate such as polymeric film or non-woven web with a hydrophilic nanostructured layer bonded to it. Spores are bonded to the nanostructured layer. Nanostructured layers including nanoparticles, such as acid-sintered silica nanoparticles are described. Biological indicators including such spore carriers are also described.

Claims (18)

1. A spore carrier comprising a substrate, a hydrophilic nanostructured layer bonded to a surface of the substrate; and spores bonded to the nanostructured layer; wherein the nanostructured layer comprises silica nanoparticles.

2. The spore carrier of claim 1 , wherein the nanostructured layer has a receding contact angle of no greater than 50 degrees as measured by the Contact Angle Method.

3. The spore carrier of claim 1 , wherein the nanostructured layer has a receding contact angle of no greater than 20 degrees as measured by the Contact Angle Method.

4. The spore carrier of claim 1 , wherein the silica nanoparticles are acid sintered.

5. The spore carrier of claim 1 , wherein the nanoparticles have an average diameter of no greater than 20 nm.

6. The spore carrier of claim 1 , wherein the nanostructured layer has an RMS roughness of at least 10 nm.

7. The spore carrier of claim 6 , the nanostructured layer has an RMS roughness of no greater than 500 nm.

8. The spore carrier of claim 1 , wherein the nanostructured layer further comprises microparticles.

9. The spore carrier of claim 1 , wherein the nanostructured layer further comprises a binder.

10. The spore carrier of claim 9 , wherein the binder comprises a tetraalkoxysilane.

11. The spore carrier of claim 1 , wherein the substrate is a polymeric substrate.

12. The spore carrier of claim 11 , wherein the polymeric substrate comprises polyester.

13. The spore carrier of claim 12 , wherein the polymeric substrate comprises polypropylene.

14. The spore carrier of claim 1 , wherein the substrate is a woven or non-woven web.

15. The spore carrier of claim 1 , wherein the substrate is a film.

16. The spore carrier of claim 1 , wherein the spores comprise at least one of Geobacillus stearothermophilus and Bacillus atrophaeus.

17. A biological indicator comprising a housing and the spore carrier of claim 1 .

18. The spore carrier of claim 1 , wherein the wherein the nanostructured layer comprises silica nanoparticles deposited out of an aqueous coating composition having a pH of less than 3.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2024
From: 3M INNOVATIVE PROPERTIES COMPANY
To: SOLVENTUM INTELLECTUAL PROPERTIES COMPANY
Reel/Frame 066435/0654 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 3, 2015
From: WITCHER, KELVIN J.; FOLTZ, WILLIAM E.; JING, NAIYONG
To: 3M INNOVATIVE PROPERTIES COMPANY
Reel/Frame 037197/0715 →