IP Library Granted Patent US 10,597,540
Granted Patent B2
US 10,597,540 · App. 14/893,585 · Granted Mar 24, 2020

Surface treatment agent for surface configured from inorganic material, tool and device having modified surface, and method for manufacturing tool and device

Inventors: Naoki Hayashi (Minato-ku, JP); Tomoki Itooka (Minato-ku, JP); Shin-ya Omote (Minato-ku, JP); Kazuhiro Iso (Minato-ku, JP)
Assignees: JSR CORPORATION; JSR LIFE SCIENCES CORPORATION
C09D5/1637A61L17/145A61L27/02A61L27/34A61L29/02A61L29/085A61L31/02A61L31/10C03C17/32C08F220/28C09D7/65C09D133/14G01N33/54393B32B7/04B32B2255/06B32B2255/26B32B2535/00C03C17/00C03C17/28C03C2217/70C08F220/22C08F220/34C08F220/36C08F220/58C08F2220/282C08F2220/286C08L33/02C08L33/04C08L33/14C09D5/16C09D5/1656C09D5/1668C09D133/02C09D133/04G01N33/543Y10T428/31678Y10T428/31692Y10T428/31699
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Quick Facts
Patent No.
US 10,597,540
App. No.
14/893,585
Granted
Mar 24, 2020
Kind
B2
Abstract

A surface treatment method for treating a surface formed of an inorganic material by using a polymer is provided. The polymer contains a repeating unit (A) having a cationic group with a particular structure in a side chain thereof and a repeating unit (B) having a group of a particular structure in a side chain thereof. Also provided are a tool and a device having a modified surface, and a method for producing the tool and the device.

Claims (30)

1. A tool, comprising:

a surface formed of an inorganic material, and

a non-crosslinked polymer comprising a repeating unit (A) and a repeating unit (B) physically adsorbed directly on at least a part of the surface formed of an inorganic material, wherein the repeating unit (A) is represented by Formula (3):

where R 5 represents a hydrogen atom or a methyl group, R 6 represents —O—, *—(C═O)—O—, *—(C═O)—NR 8 —, *—NR 8 —(C═O)—(R 8 represents a hydrogen atom or an organic group with 1 to 10 carbon atoms, and * denotes the position of bonding to the carbon atom to which R 5 is bonded in Formula (3)), or a phenylene group, R 7 represents a divalent organic group with 1 to 8 carbon atoms, and X represents a monovalent group represented by Formula (4-1):

where R 1 and R 2 each independently represents a hydrocarbon group comprising 1 to 10 carbon atoms, and R 9 represents a hydrocarbon group with 1 to 10 carbon atoms,

and the repeating unit (B) comprises a group represented by Formula (2) in a side chain thereof

where R 3 represents an alkanediyl group comprising 2 to 8 carbon atoms, R 4 represents a hydrogen atom or an organic group comprising 1 to 40 carbon atoms, and n has an average value of 1 or more.

2. A modified glass surface, comprising:

a surface formed of oxide glass, chalcogenide, inorganic glass, metal alloy glass, or quartz, and

a non-crosslinked polymer directly physically adsorbed to at least a part of said surface formed of oxide glass, chalcogenide, inorganic glass, metal alloy glass, or quartz, wherein

the non-crosslinked polymer comprises a repeating unit (A) and a repeating unit (B), the repeating unit (A) is represented by Formula (3):

where R 5 represents a hydrogen atom or a methyl group, R 6 represents —O—, *—(C═O)—O—, *—(C═O)—NR 8 —, *—NR 8 —(C═O)— where R 8 represents a hydrogen atom or an organic group with 1 to 10 carbon atoms, and * denotes the position of bonding to the carbon atom to which R 5 is bonded in Formula (3), or a phenylene group, R 7 represents a divalent organic group with 1 to 8 carbon atoms, and X represents a monovalent group represented by Formula (4-1):

where R 1 and R 2 each independently represents a hydrocarbon group comprising 1 to 10 carbon atoms, and R 9 represents a hydrocarbon group with 1 to 10 carbon atoms, and the repeating unit (B) comprises a group represented by Formula (2) in a side chain thereof

where R 3 represents an alkanediyl group comprising 2 to 8 carbon atoms, R 4 represents a hydrogen atom or an organic group comprising 1 to 40 carbon atoms, and n has an average value of 1 or more.

3. A method for treating a surface formed of an inorganic material, the method comprising:

physically adsorbing a non-crosslinked polymer directly to at least a part of said surface formed of an inorganic material, wherein

the non-crosslinked polymer comprises a repeating unit (A) and a repeating unit (B), the repeating unit (A) is represented by Formula (3):

where R 5 represents a hydrogen atom or a methyl group, R 6 represents —O—, *—(C═O)—O—, *—(C═O)—NR 8 —, *—NR 8 —(C═O)— where R 8 represents a hydrogen atom or an organic group with 1 to 10 carbon atoms, and * denotes the position of bonding to the carbon atom to which R 5 is bonded in Formula (3), or a phenylene group, R 7 represents a divalent organic group with 1 to 8 carbon atoms, and X represents a monovalent group represented by Formula (4-1):

where R 1 and R 2 each independently represents a hydrocarbon group comprising 1 to 10 carbon atoms, and R 9 represents a hydrocarbon group with 1 to 10 carbon atoms, and the repeating unit (B) comprises a group represented by Formula (2) in a side chain thereof

where R 3 represents an alkanediyl group comprising 2 to 8 carbon atoms, R 4 represents a hydrogen atom or an organic group comprising 1 to 40 carbon atoms, and n has an average value of 1 or more.

4. The method according to claim 3 , wherein:

said surface formed of an inorganic material is a glass surface;

R 6 represents *—(C═O)—O— or *—(C═O)—NR 8 —, and R 7 represents a divalent hydrocarbon group with 1 to 8 carbon atoms;

a content of repeating unit (A) is 0.01 - 20% by mass;

repeating unit (B) consists of a repeating unit represented by Formula (5):

where

R 12 represents a hydrogen atom or a methyl group,

R 13 represents a phenylene group, —O—, **—(C═O)—O—, **—(C═O)—NR 14 —, or **—NR 14− (C═O)—, where R 14 represents a hydrogen atom or an organic group comprising 1 to 10 carbon atoms, and ** denotes a position of bonding to a carbon atom to which R 12 is bonded in the Formula (5), and

R 3 represents an alkanediyl group comprising 2 to 8 carbon atoms, R 4 represents a hydrogen atom or an organic group comprising 1 to 40 carbon atoms, and n has an average value of 1 or more; and

a content of repeating unit (B) is 30 - 99.99% by mass.

Assignments (5)
CHANGE OF NAME Recorded Mar 25, 2026
From: JSR LIFE SCIENCES CORPORATION
To: MBL MATERIALS CO., LTD.
Reel/Frame 075228/0228 →
CHANGE OF ADDRESS Recorded Mar 25, 2026
From: MBL MATERIALS CO., LTD.
To: MBL MATERIALS CO., LTD.
Reel/Frame 075228/0238 →
CHANGE OF NAME Recorded Sep 22, 2025
From: JICC-02 CORPORATION
To: JSR CORPORATION
Reel/Frame 072326/0282 →
MERGER Recorded Sep 22, 2025
From: JSR CORPORATION
To: JICC-02 CORPORATION
Reel/Frame 072935/0152 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 24, 2015
From: HAYASHI, NAOKI; ITOOKA, TOMOKI; OMOTE, SHIN-YA; ISO, KAZUHIRO
To: JSR CORPORATION; JSR LIFE SCIENCES CORPORATION
Reel/Frame 037128/0618 →
Priority Claims (1)
JP 2013-111087 · May 27, 2013 · national
Continuity (1)
Related Publication 20160102213A1 · Apr 14, 2016