Cryogenic workstation using nitrogen
Cryogenic devices are provided in which liquid nitrogen is used to maintain ultra-low temperatures in which samples can be manipulated.
1. A system comprising:
a container comprising one or more sides and a floor with an open-top surface forming an interior chamber wherein a liquid-tight metal tank, comprising at least one opening at the open-top surface of the liquid-tight metal tank capable of exhausting gas directly into the chamber is mounted on or in close proximity to an interior side wall; and
a laser mounting system on the container, the laser mounting system comprising:
a laser carriage comprising a laser diode electrically connected to a first electrical terminal, and further comprising a first magnet,
a mounting plate comprising a second electrical terminal and a second magnet, the second electrical terminal and second magnet being positioned to align with the first electrical terminal and the first magnet when laser carriage is coupled to the mounting plate,
a harness adapter having a first surface for receiving an outer surface of a sensor harness and an opposing surface for receiving the mounting plate, the harness adapter being interposed between the harness and the mounting plate, and
a lead wire coupled to the second electrical terminal.
2. The system of claim 1 wherein the container comprises a material with a thermal conductivity less than 0.2 watts per meter kelvin.
3. The system of claim 2 , wherein the material comprises cross-linked polyethylene foam, urethane foam, styrene foam, polyvinyl foam, or a polymer blend foam.
4. The system of claim 1 , wherein the liquid-tight metal tank comprises steel, stainless steel, copper, a copper alloy, aluminum, or an aluminum alloy.
5. The system of claim 1 wherein the liquid-tight metal tank comprises one or more liquid-filling ports, sensor mounts, and sensor housings.
6. The system of claim 1 in which the chamber temperature may be regulated to a predetermined temperature range.
7. The system of claim 5 wherein the system comprises a liquid level sensor or a temperature sensor or both.
8. The system of claim 7 to which is attached piping, tubing or gravity chutes to direct liquid into the liquid-tight metal tank.
9. The system of claim 8 to which is attached a microprocessor receiving electric signals from a liquid level sensor or from temperature sensor or both, and delivering an electric signal to a liquid delivery regulator.
10. The system of claim 9 wherein the chamber comprises one or more temperature sensors to monitor the interior gas temperature.
11. The system of claim 10 wherein the temperature sensor is a thermocouple or an RTD sensor.
12. The system of claim 1 , further comprising an attached external liquid refrigerant reservoir, wherein the attached external liquid refrigerant reservoir is pressurized by an electric current passed through a resistance coil that is submerged in a liquid refrigerant, or wherein the liquid refrigerant is moved through an action of a mechanical pump.
13. The system of claim 12 wherein a liquid nitrogen delivery system comprises a covered gravity chute.
14. The system of claim 1 wherein
the liquid-tight metal tank comprises a plurality of rims to limit spillage, and
the liquid-tight metal tank is positioned in the interior chamber so that a lowest rim of the plurality of rims of the at least one opening of the liquid-tight metal tank no lower than seventy-five percent of a height of the interior chamber.
15. The system of claim 14 wherein the liquid-tight metal tank has one or more level top edges whereby overflow of cold gas from the liquid-tight metal tank will fall evenly down a tank face beneath the level to edge.
16. The system of claim 15 wherein the liquid-tight metal tank is constructed with a long dimension greater than fifty percent of a length of a chamber wall on which it is affixed.
17. The system of claim 14 wherein an interior of the liquid-tight metal tank comprises removable or permanently attached baffles, screens, or porous materials that may suppress or restrict liquid movement in the interior of the liquid-tight tank.
18. The system of claim 1 wherein a deck covers a portion of the interior chamber.
19. The system of claim 18 whereupon one or more instruments, panel interfaces, control features, sensors, electronics, data recorders, wireless linkages, power connections, and liquid nitrogen delivery ports and linkages is affixed to said deck.
20. The system of claim 1 , wherein the laser diode comprises a pair of laser diodes.
21. The system of claim 20 , wherein a front surface of the laser carriage comprises a plane, and wherein a side corner edge of the front surface is angled inwardly in the range of 10°-50°, and wherein a central axis of the laser diode is angled at approximately 30° relative to the plane of the front surface.
22. The system of claim 21 , wherein the laser diode comprises a first laser diode positioned on a first angled corner of the front surface, and a second laser diode positioned on a second angled corner of the front surface, wherein the first angled corner is opposite the second angled corner on the front surface.
23. The system of claim 22 , wherein an angle between a central axis of the first laser diode and a central axis of the second laser diode is in the range of 20°-100°.
24. The system of claim 23 , wherein the laser carriage is selectively removable from the mounting plate.
25. The system of claim 24 , wherein the harness adapter is permanently attached to the harness.
26. The system of claim 25 , wherein the mounting plate is removably coupled to the harness adapter via a fastener.
27. The system of claim 26 , further comprising a magnetic interface between the mounting plate and the laser carriage.
28. The system of claim 27 , further comprising a keyed connection between the mounting plate and the laser carriage.
29. A method for creating a container with an open-top cavity filled with low temperature gas wherein a portion of the low temperature gas is at a temperature below −80 degrees Celsius comprising:
providing a laser mounting system, wherein the laser mounting system is on the container, the laser mounting system comprising:
a laser carriage comprising a laser diode electrically connected to a first electrical terminal, and further comprising a first magnet,
a mounting plate comprising a second electrical terminal and a second magnet, the second electrical terminal and second magnet being positioned to align with the first electrical terminal and the first magnet when laser carriage is coupled to the mounting plate, and
a harness adapter having a first surface for receiving an outer surface of a sensor harness and an opposing surface for receiving the mounting plate, the harness adapter being interposed between the harness and the mounting plate, and a lead wire coupled to the second electrical terminal;
evaporating liquid nitrogen within a metal tank affixed to a container wall to form a nitrogen vapor and exhausting the nitrogen vapor directly into the container cavity.
30. The method of claim 29 wherein the low temperature gas temperature is regulated by control of a level of liquid nitrogen contained within the metal tank.
31. The method of claim 29 , further comprising mixing the low temperature gas within the container cavity at an increased rate relative to a rate of mixing the low temperature gas within the container cavity obtained when the liquid nitrogen is contained in the metal tank resting on a floor of a chamber of the container.
32. The method of claim 31 wherein the uniformity of the gas temperature within the container cavity is increased by the mixing effect of the liquid nitrogen from the metal tank.
33. The method of claim 29 wherein the chamber temperature is at a reduced temperature compared to the metal tank when resting on a floor of a chamber of the container.
34. The method of claim 29 wherein a flow of the low temperature gas from the metal tank increases exposure of a warmer cavity gas to a surface of the liquid nitrogen.
35. The method of claim 29 , further comprising exposing a chamber of the container to the low temperature gas by flowing the nitrogen vapor downward in a direction of a gravitational field.