IP Library Granted Patent US 10,036,078
Granted Patent B2
US 10,036,078 · App. 14/905,311 · Granted Jul 31, 2018

Low alloy oil well steel pipe and method for manufacturing same

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Quick Facts
Patent No.
US 10,036,078
App. No.
14/905,311
Granted
Jul 31, 2018
Kind
B2
Abstract

Low-alloy oil-well steel pipe includes a composition consisting, in mass %, of C: 0.40 to 0.65%, Si: 0.05 to 0.50%, Mn: 0.10 to 1.00%, P: 0.020% or less, S: 0.0020% or less, Cu: 0.15% or less, Cr: 0.40 to 1.50%, Mo: 0.50 to 2.50%, V: 0.05 to 0.25%, Ti: 0 to less than 0.01%, Nb: 0.01 to 0.2%, sol. Al: 0.010 to 0.100%, N: 0.006% or less, B: 0 to 0.0015%, and Ca: 0 to 0.003%, the balance being Fe and impurities. The structure has tempered martensite and 0 to less than 2% volume ratio of retained austenite. A grain size number of prior-austenite grain in the structure is 9.0 or more. An equivalent circular diameter of a sub-structure surrounded by a boundary having a crystal orientation difference of 15° or more from a packet boundary, a block boundary and a lath boundary is 3 μm or less for the tempered martensite.

Claims (28)

1. A low-alloy oil-well steel pipe characterized by comprising:

a chemical composition consisting, in mass %, of

C: 0.40 to 0.65%,

Si: 0.05 to 0.50%,

Mn: 0.10 to 1.00%,

P: 0.020% or less,

S: 0.0020% or less,

Cu: 0.15% or less,

Cr: 0.40 to 1.50%,

Mo: 0.50 to 2.50%,

V: 0.05 to 0.25%,

Ti: 0 to less than 0.01%,

Nb: 0.01 to 0.2%,

sol. Al: 0.010 to 0.100%,

N: 0.006% or less,

B: 0 to 0.0015%, and

Ca: 0 to 0.003%,

the balance being Fe and impurities; and

a structure consisting of tempered martensite and 0 to less than 2% in volume ratio of retained austenite,

wherein the steel pipe has yield strength of 965 MPa or more;

wherein a grain size number of a prior-austenite grain in the structure is 9.0 or more; and

wherein in the tempered martensite, a equivalent circular diameter of a sub-structure surrounded by a boundary having a crystal orientation difference of 15° or more from among a packet boundary, a block boundary and a lath boundary is 3 μm or less.

2. A method for manufacturing a low-alloy oil-well steel pipe, which has a yield stress of 965 MPa or more, comprising:

a hot working step of hot-working a starting material having the chemical composition according to claim 1 to form a hollow shell;

a final quenching step of subjecting the hollow shell to quenching in which a cooling rate when a temperature of the hollow shell is between 500° C. and 100° C. is set to 1° C./s to less than 15° C./s and the temperature of the hollow shell at which cooling is stopped is set to 100° C. or less; and

a step of tempering the quenched hollow shell.

3. The method according to claim 2 , characterized in that

the method further comprises an intermediate heat treatment step of soaking the hollow shell at a temperature of an A 1 point or more after the hot working step and before the final quenching step.

Assignments (2)
CHANGE OF NAME Recorded May 14, 2019
From: NIPPON STEEL & SUMITOMO METAL CORPORATION
To: NIPPON STEEL CORPORATION
Reel/Frame 049257/0828 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 17, 2016
From: ARAI, YUJI; OMURA, TOMOHIKO; KONDO, KEIICHI
To: NIPPON STEEL & SUMITOMO METAL CORPORATION
Reel/Frame 038008/0743 →