Microwave resonator with distributed bragg reflector (=DBR)
View Patent ↗An NMR (nuclear magnetic resonance) probe head has a microwave resonator with at least two elements which are reflective in the microwave range, at least one of which is focusing. The reflective elements at least partly delimit a resonance volume of the microwave resonator. At least one of the reflective elements is a DBR (“Distributed Bragg Reflector”), and the NMR probe head has at least one NMR coil integrated into the DBR. The NMR detection coil can thereby be positioned particularly near to the sample and the distortions of the static field by resonator components are reduced, such that the detection sensitivity and the spectral resolution of the experiment are significantly improved.
1. An NMR (nuclear magnetic resonance) probe head, the probe head comprising:
a microwave resonator having at least two reflective elements which are reflective in the microwave range, wherein at least one of said two reflective elements is focusing, said at least two reflective elements at least partly delimiting a resonance volume of the microwave resonator, wherein at least one of said at least two reflective elements is a DBR (distributed Bragg reflector); and
at least one NMR coil which is integrated in said DBR.
2. The NMR probe head of claim 1 , wherein at least two reflective elements are focusing.
3. The NMR probe head of claim 1 , wherein all reflective elements are focusing.
4. The NMR probe head of claim 1 , wherein one reflective element is focusing and one is planar.
5. The NMR probe head of claim 1 , wherein one reflective element is focusing and one is defocusing.
6. The NMR probe head of claim 1 , wherein a surface of at least one of said reflective elements has a spherical or elliptical shape.
7. The NMR probe head of claim 1 , further comprising a coupling element for microwave radiation disposed on a side of said DBR facing away from said resonance volume of said microwave resonator.
8. The NMR probe head of claim 1 , wherein a sample position of the probe head is disposed in said resonance volume.
9. The NMR probe head of claim 1 , wherein a sample position of the probe head is disposed at a minimum of an electric field of said microwave resonator during measuring operation.
10. The NMR probe head of claim 8 , wherein the NMR probe head comprises at least one NMR coil which induces a magnetic RF (radio frequency) field at the sample position.
11. The NMR probe head of claim 10 , wherein the NMR probe head further comprises an element for supplying a sample to the sample position.
12. The NMR probe head of claim 1 , wherein said at least one NMR coil which is integrated in said DBR is disposed on a surface of said DBR.
13. The NMR probe head of claim 12 , wherein said DBR has a plurality of layers and said NMR coil is designed as an RF coil, wherein said NMR coil is disposed on a first layer of said DBR and is transparent to microwave radiation.
14. The NMR probe head of claim 13 , wherein said NMR coil is designed as a grid.
15. The NMR probe head of claim 1 , wherein said at least one NMR coil is designed as an RF coil and said DBR has a plurality of layers, wherein said NMR coil is disposed on a rear side, facing away from an other reflective element, of a first layer of said DBR.
16. The NMR probe head of claim 1 , wherein said DBR comprises a plurality of dielectric layers and channels are provided in a front side, facing an other reflective element, of at least a first layer of said DBR, said channels enabling exact spatial positioning of an NMR sample.
17. The NMR probe head of claim 16 , wherein channels are provided in a plurality of layers of said DBR for spatially positioning an NMR sample.