IP Library Granted Patent US 9,296,767
Granted Patent B1
US 9,296,767 · App. 14/943,170 · Granted Mar 29, 2016

Surface-treated calcium phosphate particles suitable for oral care and dental compositions

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Quick Facts
Patent No.
US 9,296,767
App. No.
14/943,170
Granted
Mar 29, 2016
Kind
B1
Abstract

Calcium phosphate particles are described comprising a surface treatment wherein the surface treatment comprises at least one sugar alcohol. Also described are various oral care compositions comprising surface treated calcium phosphate particles and methods of surface treating calcium phosphate particles.

Claims (13)

1. A method of surface treating calcium phosphate particles comprising

dissolving at least one sugar alcohol into a liquid medium to provide a surface treatment solution;

dispersing calcium phosphate particles in the surface treatment solution; and

removing the liquid medium to obtain dried surface treated calcium phosphate particles.

2. The method of claim 1 wherein the liquid medium is an aqueous medium.

3. The method of claim 1 , wherein the calcium phosphate particles comprise tricalcium phosphate.

4. The method of claim 1 , wherein the sugar alcohol has the general formula HOCH 2 [CH(OH)] n CH 2 OH, wherein n ranges from 4 to 6.

5. The method of claim 4 , wherein the sugar alcohol is xylitol.

6. The method of claim 1 , wherein the calcium phosphate particles comprise at least one of: Sr, Ba, Mg, Zn; Na, K, a rare earth metal, OH, F, carbonate, and combinations thereof.

7. The method of claim 1 , wherein the calcium phosphate particles have a particle size no greater than 100 micrometers.

8. The method of claim 1 , wherein the calcium phosphate particles have a particle size no greater than 500 nanometers.

9. The method of claim 1 , wherein the largest calcium phosphate particles are 5 to 100 times the size of the smallest calcium phosphate particles.

10. The method of claim 1 , wherein the concentration of surface treatment on the calcium phosphate particles is at least 0.05% by weight.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2024
From: 3M INNOVATIVE PROPERTIES COMPANY
To: SOLVENTUM INTELLECTUAL PROPERTIES COMPANY
Reel/Frame 066433/0105 →