IP Library Granted Patent US 10,214,449
Granted Patent B2
US 10,214,449 · App. 14/954,377 · Granted Feb 26, 2019

Coating compositions for roofing granules, dark colored roofing granules with increased solar heat reflectance, solar heat-reflective shingles and process for producing the same

Inventors: Husnu M. Kalkanoglu (Swarthmore, PA); Thomas McShea (Wareham, MA); Ming Liang Shiao (Collegeville, PA)
Assignee: CertainTeed Corporation
C04B7/02C04B14/045C04B20/1085C04B28/04C04B28/26C04B41/5018C04B41/5024C04B41/524C09D1/00E04D7/005C04B2111/00586C04B2111/80Y02W30/94Y02W30/95Y10T428/24372Y10T428/24413Y10T428/24421Y10T428/252Y10T428/259Y10T428/2991Y10T428/2993Y10T428/2995Y10T428/31
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Quick Facts
Patent No.
US 10,214,449
App. No.
14/954,377
Granted
Feb 26, 2019
Kind
B2
Abstract

Dark colored roofing granules include an inert base particle coated with a composition including a metal silicate, a non-clay latent heat reactant, and a dark colored but solar reflective pigment.

Claims (35)

1. A plurality of dark-colored roofing granules, each of the dark-colored roofing granules comprising:

an inert base particle; and

a cured coating disposed about the inert base particle, the cured coating being a reaction product of a coating composition comprising:

an alkali metal silicate;

at least one non-clay latent heat reactant; and

at least one inorganic solar heat-reflective pigment, each of the at least one inorganic solar heat-reflective pigments having an L* less than 30 and a solar reflectance greater than 20 percent, and wherein the coating composition comprises at least about 5 percent to 25 percent of the at least one solar heat-reflective pigment,

wherein

the plurality of dark-colored roofing granules has an L* less than 30 and a solar reflectance greater than 20, and

wherein each of the dark-colored roofing granules lacks a light-colored base coat disposed between the inert base particle and the cured coating.

2. A plurality of dark-colored roofing granules according to claim 1 , wherein in the coating composition the at least one non-clay latent heat reactant is selected from the group consisting of Portland cement, aluminum fluoride, ammonium silicofluoride, alkali metal silicofluorides, and alkaline earth metal silicofluorides.

3. A plurality of dark-colored roofing granules according to claim 1 , wherein in the coating composition the at least one non-clay latent heat reactant comprises Portland cement, aluminum fluoride and at least one alkali metal silicofluoride.

4. A plurality of dark-colored roofing granules according to claim 3 , wherein in the coating composition the at least one alkali metal silicofluoride is sodium silicofluoride.

5. A plurality of dark-colored roofing granules according to claim 3 , wherein in the coating composition wherein the at least one non-clay latent heat reactant comprise from about 3 to 15 weight percent of the coating composition of aluminum fluoride, from about 0.5 to 5 weight percent of the coating composition of sodium silicofluoride, and from about 0.5 to 5 weight percent of the coating composition of Portland cement.

6. A plurality of dark-colored roofing granules according to claim 1 , wherein in the coating composition wherein the at least one inorganic solar heat-reflective pigment is selected from the group consisting of Arctic Black 10C909 (chromium green-black), Black 411 (chromium iron oxide), Brown 12 (zinc iron chromite), Brown 8 (iron titanium brown spinel), and Yellow 193 (chrome antimony titanium), 56, Eclipse Black 10201, Forest Green 10241, Eclipse Black 10202, Eclipse Black 10203, and H IR Green V-12650.

7. A plurality of dark-colored roofing granules of claim 1 wherein in each of the dark-colored roofing granules the cured coating comprises a first layer including a first metal silicate binder and a first inorganic solar heat-reflective pigment and a second layer including a second metal silicate binder and a second inorganic solar heat-reflective pigment.

8. A plurality of dark-colored roofing granules of claim 7 wherein in each of the dark-colored roofing granules the second inorganic solar heat-reflective pigment is identical to the first inorganic solar heat-reflective pigment.

9. A plurality of dark-colored roofing granules of claim 8 wherein in each of the dark-colored roofing granules the first and second inorganic solar heat-reflective pigments are selected from the group consisting of Arctic Black 10C909 (chromium green-black), Black 411 (chromium iron oxide), Brown 12 (zinc iron chromite), Brown 8 (iron titanium brown spinel), and Yellow 193 (chrome antimony titanium), Brown 10364, Eclipse Black 10201, Forest Green 10241, Eclipse Black 10202, Eclipse Black 10203, and H IR Green V-12650.

10. A plurality of dark-colored roofing granules of claim 8 wherein in each of the dark-colored roofing granules the first coating layer comprises at least about 30 percent to about 40 percent of the first inorganic solar heat-reflective pigment, and wherein the second coating layer comprises at least about 30 percent to about 40 percent of the second inorganic solar heat-reflective pigment.

11. A plurality of dark-colored roofing granules of claim 7 wherein in each of the dark-colored roofing granules the first and second coating layers form from about 4 percent by weight of the inert base particle to about 10 percent by weight of the inert base particle.

12. A plurality of dark-colored roofing granules of claim 7 wherein each of the dark-colored roofing granules further comprises a third coating layer, the third coating layer being identical to the second coating layer and the first coating layer.

13. A plurality of dark-colored roofing granules of claim 7 wherein in each of the dark-colored roofing granules the second inorganic solar heat-reflective pigment is different from the first inorganic solar heat-reflective pigment.

14. A plurality of dark-colored roofing granules of claim 13 wherein in each of the dark-colored roofing granules the first inorganic solar heat-reflective pigment is selected from the group consisting of Arctic Black 10C909 (chromium green-black), Black 411 (chromium iron oxide), Brown 12 (zinc iron chromite), Brown 8 (iron titanium brown spinel), and Yellow 193 (chrome antimony titanium), Brown 10364, Eclipse Black 10201, Forest Green 10241, Eclipse Black 10202, Eclipse Black 10203, and H IR Green V-12650.

15. A plurality of dark-colored roofing granules of claim 13 wherein in each of the dark-colored roofing granules the second inorganic solar heat -reflective pigment is selected from the group consisting of Arctic Black 10C909 (chromium green-black), Black 411 (chromium iron oxide), Brown 12 (zinc iron chromite), Brown 8 (iron titanium brown spinel), and Yellow 193 (chrome antimony titanium), Brown 10364, Eclipse Black 10201, Forest Green 10241, Eclipse Black 10202, Eclipse Black 10203, and H IR Green V-12650.

16. A plurality of dark-colored roofing granules of claim 13 wherein in each of the dark-colored roofing granules the second layer further comprises an inorganic solar-reflective functional pigment.

17. A plurality of dark-colored roofing granules of claim 16 wherein in each of the dark-colored roofing granules the solar-reflective functional pigment is selected from the group consisting of mirrorized silica flakes, metal flake pigments, and metal oxide coated flake pigments.

18. A plurality of dark-colored roofing granules of claim 16 wherein in each of the dark-colored roofing granules the second coating layer comprises at least about 1 percent to about 60 percent of the solar-reflective functional pigment.

19. A plurality of dark-colored roofing granules of claim 16 wherein in each of the dark-colored roofing granules the second coating layer comprises at least about 1 percent to about 60 percent of the second solar heat-reflective pigment.

20. A plurality of dark-colored roofing granules of claim 1 , wherein in each of the dark-colored roofing granules the inert base particle is an inert mineral particle and the cured coating is disposed directly on the inert mineral particle.

21. A plurality of dark-colored roofing granules of claim 1 , wherein in each of the dark-colored roofing granules the coating composition further includes aluminum oxide having a particle size in the range of 0.1 to 5 micrometers.

22. A plurality of dark-colored roofing granules of claim 1 , wherein in each of the dark-colored roofing granules the coating composition is free of kaolin clay.

23. A plurality of dark-colored roofing granules of claim 1 , wherein in each of the dark-colored roofing granules the at least one inorganic solar heat-reflective pigment is a metal oxide pigment.

24. A plurality of dark-colored roofing granules of claim 1 , wherein in each of the dark-colored roofing granules the at least one inorganic pigment is the only pigment in the coating composition.

25. A plurality of dark-colored roofing granules of claim 1 , wherein in each of the dark-colored roofing granules the inorganic solar heat-reflective pigments does not comprise a white pigment coated with a near infrared-absorbing colorant.

26. An asphalt shingle having a surface coated with the plurality of dark-colored roofing granules of claim 1 , the shingle having an L* less than 55 and a solar reflectance of greater than 20 percent.

27. An asphalt shingle having a surface coated with the plurality of dark-colored roofing granules of claim 1 , the shingle having an L* less than 30 and a solar reflectance of greater than 20 percent.

Assignments (3)
CONVERSION Recorded Jan 10, 2021
From: CERTAINTEED CORPORATION
To: CERTAINTEED LLC
Reel/Frame 054943/0542 →
CONVERSION, REVERSE MERGER, CONVERSION Recorded Jan 10, 2021
From: CERTAINTEED LLC
To: CERTAINTEED LLC
Reel/Frame 054943/0580 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 8, 2018
From: KALKANOGLU, HUSNU M.; SHIAO, MING LIANG; MCSHEA, THOMAS
To: CERTAINTEED CORPORATION
Reel/Frame 044876/0172 →
Continuity (4)
Continuation 13933579 · Jul 2, 2013
Continuation 12933144
Provisional Application 61040938 · Mar 31, 2008
Related Publication 20160107929A1 · Apr 21, 2016
Cited By (1)
US 12,624,550