IP Library Granted Patent US 9,944,635
Granted Patent B2
US 9,944,635 · App. 14/958,461 · Granted Apr 17, 2018

Deuterated pyrazino[2,1-a]isoquinoline compounds and methods of treatment using the same

Inventors: Julie F. Liu (Lexington, MA); Scott L. Harbeson (Cambridge, MA); Roger D. Tung (Lexington, MA)
Assignee: Concert Pharmaceuticals, Inc.
C07D471/04A61K31/4184A61K31/4985C07B59/002
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Quick Facts
Patent No.
US 9,944,635
App. No.
14/958,461
Granted
Apr 17, 2018
Kind
B2
Abstract

This invention in one embodiment is directed to a compound of Formula Ia; where the designation (R) indicates that the designated carbon has the (R) stereochemistry; and wherein Z 1 is hydrogen or fluorine; Z 2 is hydrogen, deuterium, or fluorine; Z 3 is deuterium; Z 4 is fluorine; m is an integer from 0 to 10; n is an integer from 0 to 2; provided that: the sum of m+n does not exceed 10; and when both Z 1 and Z 2 are hydrogen, the sum of m+n is greater than 0, and pharmaceutically acceptable salts thereof. This invention also provides compositions comprising one or more compounds of this invention and a carrier and the use of the disclosed compounds and compositions in methods of treating diseases and conditions that are beneficially treated by administering an antihelminthic agent, such as praziquantel.

Claims (33)

1. A compound selected from:

or a pharmaceutically acceptable salt thereof, wherein the compound has a deuterium incorporation at each designated deuterium atom of at least 90%.

2. The compound of claim 1 , wherein the deuterium incorporation at each designated deuterium atom is at least 95%.

3. The compound of claim 1 , wherein the deuterium incorporation at each designated deuterium atom is at least 97%.

4. A pharmaceutical composition comprising a compound of claim 1 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier.

5. A compound selected from:

or a pharmaceutically acceptable salt thereof, wherein the compound has a deuterium incorporation at each designated deuterium atom of at least 90%.

6. The compound of claim 5 , wherein the deuterium incorporation at each designated deuterium atom is at least 95%.

7. The compound of claim 5 , wherein the deuterium incorporation at each designated deuterium atom is at least 97%.

8. A pharmaceutical composition comprising a compound of claim 5 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier.

9. A method of treating schistosoma infections, infections due to Clonorchis sinensis or Opisthorchis viverrini , cysticercosis, neurocysticercosis, or malaria in a patient comprising administering to a patient in need thereof an effective amount of a compound of Formula Ia:

or a pharmaceutically acceptable salt thereof, wherein:

Z 1 is hydrogen or fluorine;

Z 2 is hydrogen, deuterium, or fluorine;

Z 3 is deuterium;

Z 4 is fluorine;

m is 2, 4, 6, 8 or 10; and

n is 0 or 2;

provided that:

the sum of m and n does not exceed 10;

wherein the compound has a deuterium incorporation at each designated deuterium atom of at least 90%.

10. The method of claim 9 , wherein 2, 4, 6, 8 or 10 geminal Z 3 are present.

11. The method of claim 9 , wherein Z 2 is hydrogen.

12. The method of claim 9 , wherein Z 2 is deuterium.

13. The method of claim 9 , wherein 2 geminal Z 4 are present.

14. The method of claim 9 , wherein the compound is selected from:

or a pharmaceutically acceptable salt thereof.

15. The method of claim 9 , wherein the compound is selected from:

or a pharmaceutically acceptable salt thereof.

16. The method of claim 14 , wherein the deuterium incorporation at each designated deuterium atom is at least 95%.

17. The method of claim 14 , wherein the deuterium incorporation at each designated deuterium atom is at least 97%.

18. The method of claim 15 , wherein the deuterium incorporation at each designated deuterium atom is at least 95%.

19. The method of claim 15 , wherein the deuterium incorporation at each designated deuterium atom is at least 97%.

Assignments (2)
MERGER Recorded Aug 2, 2023
From: CONCERT PHARMACEUTICALS, INC.
To: SUN PHARMACEUTICAL INDUSTRIES, INC.
Reel/Frame 064465/0383 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 18, 2015
From: LIU, JULIE F.; TUNG, ROGER; HARBESON, SCOTT L.
To: CONCERT PHARMACEUTICALS, INC.
Reel/Frame 037323/0098 →
Continuity (5)
Continuation 14518254 · Oct 20, 2014
Continuation 13411198 · Mar 2, 2012
Provisional Application 61599147 · Feb 15, 2012
Provisional Application 61449312 · Mar 4, 2011
Related Publication 20160083385A1 · Mar 24, 2016