IP Library Granted Patent US 9,598,445
Granted Patent B2
US 9,598,445 · App. 14/982,431 · Granted Mar 21, 2017

Methods for producing functionalized graphenes

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Quick Facts
Patent No.
US 9,598,445
App. No.
14/982,431
Granted
Mar 21, 2017
Kind
B2
Abstract

Methods for producing functionalized graphene from graphite oxide or graphite are disclosed in which ionic liquids are used as a reaction medium to promote chemical functionalization of the graphene through electrochemically interacted exfoliation of graphene sheets.

Claims (8)

1. A functionalized graphene comprising a graphene moiety functionalized with a plurality of silane moieties, and wherein each silane moiety is linked to at least one other silane moiety by a siloxane bond.

2. The functionalized graphene of claim 1 , wherein the graphene moiety further comprises an epoxide group.

3. The functionalized graphene of claim 1 , wherein the silane moiety further comprises an amino group.

4. The functionalized graphene of claim 1 , wherein the silane moiety further comprises a primary amino group.

5. The functionalized graphene of claim 1 , wherein the silane moiety further comprises a hydroxyl group.

6. A composition comprising the functionalized graphene of claim 1 .

7. The functionalized graphene of claim 1 , wherein the silane moiety is selected from (3-aminopropyl)trimethoxysilane, 3-glycidoxypropyldimethoxy-methylsilane, (3-mercaptopropyl)trimethoxysilane, 3-(triethoxysilyl)propylisocyanate, N1-(3-trimethoxysilylpropyl)diethylene-triamine, N-[3-(trimethoxysilyl)propyl]ethylenediamine, (3-aminopropyl)triethoxysilane and any combination thereof.

8. The functionalized graphene of claim 1 , wherein the graphene moiety is covalently linked with the silane moiety through a carboxylate group.

Assignments (3)
RELEASE OF SECURITY INTEREST IN PATENTS, RECORDED ON JANUARY 29, 2019 AT REEL 048373 FRAME 0217 Recorded Sep 22, 2025
From: CRESTLINE DIRECT FINANCE, L.P., AS COLLATERAL AGENT
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 072936/0464 →
RELEASE OF SECURITY INTEREST Recorded Jul 31, 2019
From: CRESTLINE DIRECT FINANCE, L.P.
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 049924/0794 →
SECURITY INTEREST Recorded Jan 29, 2019
From: EMPIRE TECHNOLOGY DEVELOPMENT LLC
To: CRESTLINE DIRECT FINANCE, L.P.
Reel/Frame 048373/0217 →