Method of using a heat-treated titanium nitride film
View Patent ↗A heat-treated titanium nitride film including a polymeric substrate and at least one titanium nitride layer is disclosed. The titanium nitride layer of the film is characterized by microscopic uniform generally parallel surface cracking in the machine direction of the film. The film is particularly useful as a solar control film suitable for application to a contoured transparent substrate with reduced or eliminated ghosting. A method for treating a titanium nitride film prior to application to a transparent contoured substrate and a method for applying a titanium nitride film to a transparent contoured substrate are also described.
1. A method for applying a titanium nitride film to a transparent contoured substrate, said method comprising:
i. heating said titanium nitride film in a substantially uniform temperature environment for a specified period and at a specified temperature to form a uniformly heat-treated titanium nitride film, wherein said heating step is performed at a temperature of between 60° C. and 130° C. for a period of from 15 to 120 minutes; and
ii. applying the uniformly heat-treated titanium nitride film to the transparent contoured substrate.
2. The method of claim 1 , wherein the titanium nitride film is a film blank.
3. The method of claim 1 , wherein the titanium nitride film is a solar control film.
4. The method of claim 3 , wherein said solar control film is a solar control window film and said contoured transparent substrate is a window.
5. The method of claim 1 , wherein said heating step is performed at a temperature of between 90° C. and 100° C. for a period of from 30 to 90 minutes.
6. The method of claim 1 , wherein said heating step is performed at a temperature of between 90° C. and 95° C. for a period of from 45 to 60 minutes.
7. The method of claim 1 , wherein said substantially uniform temperature environment is an enclosed oven.
8. The method of claim 1 , wherein the substantially uniform temperature environment is a continuous feed oven.
9. The method of claim 1 , wherein the temperature of said substantially uniform temperature environment for said heating step is substantially constant over said period for said heating step.