IP Library Granted Patent US 9,587,319
Granted Patent B2
US 9,587,319 · App. 15/000,722 · Granted Mar 7, 2017

Hot-rolled steel sheet, cold-rolled steel sheet, galvanized steel sheet, and methods of manufacturing the same

Inventors: Nobuhiro Fujita (Tokyo, JP); Kunio Hayashi (Tokyo, JP); Riki Okamoto (Tokyo, JP); Manabu Takahashi (Tokyo, JP); Tetsuo Kishimoto (Tokyo, JP); Hiroshi Yoshida (Tokyo, JP)
Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATION
C25D3/22B21B35/00C21D6/004C21D6/005C21D6/007C21D6/008C21D8/0205C21D8/0226C21D8/0236C21D8/0247C21D8/0263C21D8/0273C21D9/46C22C38/001C22C38/002C22C38/004C22C38/005C22C38/008C22C38/02C22C38/04C22C38/06C22C38/08C22C38/10C22C38/105C22C38/12C22C38/14C22C38/16C22C38/18C22C38/20C22C38/22C22C38/24C22C38/26C22C38/28C22C38/30C22C38/32C22C38/34C22C38/38C22C38/40C22C38/42C22C38/44C22C38/46C22C38/48C22C38/50C22C38/52C22C38/54C22C38/58C23C2/02C23C2/06C23C2/28C23C2/40C25D5/36C21D2201/05C21D2211/00C21D2211/001C21D2211/002C21D2211/005C21D2211/009
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,587,319
App. No.
15/000,722
Granted
Mar 7, 2017
Kind
B2
Abstract

A hot-rolled steel sheet has an average value of the X-ray random intensity ratio of a {100} <011> to {223} <110> orientation group at least in a sheet thickness central portion that is in a sheet thickness range of ⅝ to ⅜ from a steel sheet surface of 1.0 to 6.0, an X-ray random intensity ratio of a {332} <113> crystal orientation of 1.0 to 5.0, rC which is an r value in a direction perpendicular to a rolling direction of 0.70 to 1.10, and r30 which is an r value in a direction that forms an angle of 30° with respect to the rolling direction of 0.70 to 1.10.

Claims (86)

1. A method of manufacturing a hot-rolled steel sheet, the method comprising,

first hot rolling carried out at least once at a rolling reduction ratio of 20% or more in a temperature range of 1000° C. to 1200° C., and an austenite grain diameter is set to 200 μm or less, wherein

an ingot or a slab containing, by mass %:

C: 0.0001% to 0.40%,

Si: 0.001% to 2.5%,

Mn: 0.001% to 4.0%,

P: 0.001% to 0.15%,

S: 0.0005% to 0.03%,

Al: 0.001% to 2.0%,

N: 0.0005% to 0.01%,

O: 0.0005% to 0.01%,

and further comprising one or two or more of:

Ti: 0.001% to 0.20%,

Nb: 0.001% to 0.20%,

V: 0.001% to 1.0%,

W: 0.001% to 1.0%,

B: 0.0001% to 0.0050%,

Mo: 0.001% to 1.0%,

Cr: 0.001% to 2.0%,

Cu: 0.001% to 2.0%,

Ni: 0.001% to 2.0%,

Co: 0.0001% to 1.0%,

Sn: 0.0001% to 0.2%,

Zr: 0.0001% to 0.2%,

As: 0.0001% to 0.50%,

Mg: 0.0001% to 0.010%,

Ca: 0.0001% to 0.010%, and

REM: 0.0001% to 0.1%

and balance composed of iron and inevitable impurities;

second hot rolling in which a total of rolling reduction ratios is 50% or more is carried out in a temperature range of T1+30° C. to T1+200° C.;

third hot rolling in which a total of rolling reduction ratios is less than 30% is carried out in a temperature range of T1° C. to lower than T1+30° C.; and

hot rolling ends at an Ar3 transformation temperature or higher,

where, T1 is a temperature determined by steel sheet components, and expressed by the following formula 1,

T1(° C.)=850+10×(C+N)×Mn+350×Nb+250×Ti+40×B+10×Cr+100×Mo+100×V  (Formula 1),

wherein an average value of an X-ray random intensity ratio of a {100} <011> to {223} <110> orientation group at least in a sheet thickness central portion that is in a sheet thickness range of ⅝ to ⅜ from a steel sheet surface is 1.0 to 6.0 in the hot-rolled steel sheet, an X-ray random intensity ratio of a {332} <113> crystal orientation is 1.0 to 5.0 in the hot-rolled steel sheet; and

rC which is an r value in a direction perpendicular to a rolling direction is 0.70 to 1.10, and r30 which is an r value in a direction that forms an angle of 30° with respect to the rolling direction is 0.70 to 1.10 in the hot-rolled steel sheet.

2. The method of manufacturing a hot-rolled steel sheet according to claim 1 ,

wherein, in the second hot rolling in the temperature range of T1+30° C. to T1+200° C., the ingot or slab is rolled at least once at a rolling reduction ratio of 30% or more in a pass.

3. The method of manufacturing a hot-rolled steel sheet according to claim 1 ,

wherein, in the first hot rolling in a temperature range of 1000° C. to 1200° C., the ingot or slab is rolled at least twice at a rolling reduction ratio of 20% or more, and the austenite grain diameter is set to 100 μm or less.

4. The method of manufacturing a hot-rolled steel sheet according to claim 1 ,

wherein, in a case in which a pass in which a rolling reduction ratio is 30% or more in the temperature range of T1+30° C. to T1+200° C. is defined as a large reduction pass, a waiting time t from completion of a final pass of the large reduction pass to initiation of cooling employs a configuration that satisfies the following formula 2,

t 1≦ t≦t 1×2.5  (Formula 2)

where t1 is expressed by the following formula 3;

t 1=0.001×(( Tf−T 1)× P 1) 2 −0.109×(( Tf−T 1)× P 1)+3.1  (Formula 3)

where Tf represents a temperature after the final pass, and P1 represents a rolling reduction ratio in the final pass.

5. The method of manufacturing a hot-rolled steel sheet according to claim 4 ,

wherein a temperature of the steel sheet increases by 18° C. or less between respective passes of the second hot rolling in the temperature range of T1+30° C. to T1+200° C.

6. A method of manufacturing a cold-rolled steel sheet, the method comprising,

pickling the hot-rolled steel sheet according to claim 1 ;

cold-rolling the hot-rolled steel sheet at 20% to 90%, and obtaining the cold-rolled steel sheet;

annealing the cold-rolled steel sheet at a temperature range of 720° C. to 900° C. for a holding time of 1 second to 300 seconds;

acceleration-cooling the cold-rolled steel sheet at a cooling rate of 10° C./s to 200° C./s from 650° C. to 500° C.; and

holding the cold-rolled steel sheet at a temperature of 200° C. to 500° C.

7. The method of manufacturing a cold-rolled steel sheet according to claim 6 ,

wherein, in the second hot rolling in the temperature range of T1+30° C. to T1+200° C., rolling at a rolling reduction ratio of 30% or more in a pass is carried out at least once.

8. The method of manufacturing a cold-rolled steel sheet according to claim 6 ,

wherein, in the first hot rolling in the temperature range of 1000° C. to 1200° C., rolling at a rolling reduction ratio of 20% or more is carried out at least twice, and the austenite grain diameter is set to 100 μm or less.

9. The method of manufacturing a cold-rolled steel sheet according to claim 6 ,

wherein, in a case in which a pass in which a rolling reduction ratio is 30% or more in the temperature range of T1+30° C. to T1+200° C. is defined as a large reduction pass, a waiting time t from completion of a final pass of the large reduction pass to initiation of cooling employs a configuration that satisfies the following formula 4,

t 1≦ t≦t 1×2.5  (Formula 4)

where t1 is expressed by the following formula 5;

t 1=0.001×(( Tf−T 1)× P 1) 2 −0.109×(( Tf−T 1)× P 1)+3.1  (Formula 5)

where Tf represents a temperature after the final pass, and P1 represents a rolling reduction ratio in the final pass.

10. The method of manufacturing a cold-rolled steel sheet according to claim 9 ,

wherein a temperature of the steel sheet increases by 18° C. or less between respective passes of the second hot rolling in the temperature range of T1+30° C. to T1+200° C.

11. A method of manufacturing a galvanized steel sheet, the method comprising,

winding the hot-rolled steel sheet according to claim 1 in a temperature range of 680° C. to room temperature;

pickling the hot-rolled steel sheet;

cold-rolling the hot-rolled steel sheet at 20% to 90%, and obtaining a cold-rolled steel sheet;

heating the cold-rolled steel sheet to a temperature range of 650° C. to 900° C.;

annealing the cold-rolled steel sheet for a holding time of 1 second to 300 seconds;

cooling the cold-rolled steel sheet at a cooling rate of 0.1° C./s to 100° C./s from 720° C. to 580° C.; and

galvanizing treating the cold-rolled steel sheet.

12. The method of manufacturing a galvanized steel sheet according to claim 11 ,

wherein, in the second hot rolling in the temperature range of T1+30° C. to T1+200° C., rolling at a rolling reduction ratio of 30% or more in a pass is carried out at least once.

13. The method of manufacturing a galvanized steel sheet according to claim 11 ,

wherein, in the first hot rolling in the temperature range of 1000° C. to 1200° C., rolling at a rolling reduction ratio of 20% or more is carried out at least twice, and the austenite grain diameter is set to 100 μm or less.

14. The method of manufacturing a galvanized steel sheet according to claim 11 ,

wherein, in a case in which a pass in which a rolling reduction ratio is 30% or more in the temperature range of T1+30° C. to T1+200° C. is defined as a large reduction pass, a waiting time t from completion of a final pass of the large reduction pass to initiation of cooling employs a configuration that satisfies the following formula 6,

t 1≦ t≦t 1×2.5  (Formula 6)

where t1 is expressed by the following formula 7;

t 1=0.001×(( Tf−T 1)× P 1) 2 −0.109×(( Tf−T 1)× P 1)+3.1  (Formula 7)

where Tf represents a temperature after the final pass, and P1 represents a rolling reduction ratio in the final pass.

15. The method of manufacturing a galvanized steel sheet according to claim 14 ,

wherein a temperature of the steel sheet increases by 18° C. or less between respective passes of the second hot rolling in the temperature range of T1+30° C. to T1+200° C.

Assignments (1)
CHANGE OF NAME Recorded May 14, 2019
From: NIPPON STEEL & SUMITOMO METAL CORPORATION
To: NIPPON STEEL CORPORATION
Reel/Frame 049257/0828 →
Priority Claims (8)
JP 2010-169230 · Jul 28, 2010 · national
JP 2010-169627 · Jul 28, 2010 · national
JP 2010-169670 · Jul 28, 2010 · national
JP 2010-204671 · Sep 13, 2010 · national
JP 2011-048236 · Mar 4, 2011 · national
JP 2011-048246 · Mar 4, 2011 · national
JP 2011-048253 · Mar 4, 2011 · national
JP 2011-048272 · Mar 4, 2011 · national
Continuity (2)
Division 13811902
Related Publication 20160130711A1 · May 12, 2016