IP Library Granted Patent US 9,676,907
Granted Patent B2
US 9,676,907 · App. 15/009,373 · Granted Jun 13, 2017

Methods and systems of graft polymerization on a functionalized substrate

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Quick Facts
Patent No.
US 9,676,907
App. No.
15/009,373
Granted
Jun 13, 2017
Kind
B2
Abstract

Graft polymerization is fulfilled on a functionalized substrate. The functionalized substrate is prepared from a disulfide bond-containing feedstock and has been prepared for polymerization through the introduction of one or more polyfunctional monomers containing a disulfide bond breaking material functional group.

Claims (20)

1. A grafted substrate comprising:

a substrate;

a polyfunctional monomer; and

a graft polymer grafted on the substrate via the polyfunctional monomer,

wherein the polyfunctional monomer is chemically bonded to the substrate and the polymer,

wherein the graft polymer is formed using a condensation polymerization reaction, and

wherein the polyfunctional monomer is bonded to the substrate via a disulfide bond.

2. The grafted substrate of claim 1 , wherein the polyfunctional monomer is bonded to the polymer via a sulfur-carbon bond.

3. The grafted substrate of claim 1 , wherein the substrate includes cysteine or cysteine-containing material.

4. The grafted substrate of claim 1 , wherein the polyfunctional monomer includes a functional group, the functional group includes at least one of an acid anhydride, an isothiocyanate, an acyl halide, an alcohol, an aldehyde, an alkene, an alkyne, an amine, a carboxylic acid, an ester and/or a thiol.

5. The grafted substrate of claim 1 , wherein the polyfunctional monomer includes a functional group, the functional group includes at least one ring, the ring being adapted to be opened to form at least a second functional group.

6. The grafted substrate of claim 1 , further comprising a polyester polymer,

wherein the polyester polymer is bonded to the polyfunctional monomer via an ester bond.

7. A functionalized substrate and graft polymer combination comprising:

a substrate; and

a polyfunctional monomer,

wherein the polyfunctional monomer including at least one first functional group and at least one second functional group, the first functional group including a first thiol group, and the second functional group including a second thiol group configured to react with a condensation polymerizable monomer, the first thiol group forming a disulfide bond with the substrate,

wherein the graft polymer is formed using a condensation polymerization reaction.

8. The functionalized substrate and graft polymer combination of claim 7 , wherein the polyfunctional group includes a third functional group, the third functional group includes at least one of an acid anhydride, an acyl halide, an isothiocyanate, an alcohol, an aldehyde, an alkene, an alkyne, an amine, a carboxylic acid, an ester and/or a thiol.

9. The functional substrate of claim 7 , wherein the polyfunctional group includes a third functional group, the third functional group includes at least one ring, the ring being adapted to be opened to form at least a fourth functional group.

Assignments (2)
SECURITY INTEREST Recorded Sep 19, 2023
From: H.B. FULLER COMPANY
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 064951/0856 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 10, 2023
From: ASPEN RESEARCH CORPORATION
To: H.B. FULLER COMPANY
Reel/Frame 062661/0630 →