IP Library Granted Patent US 9,669,384
Granted Patent B2
US 9,669,384 · App. 15/011,732 · Granted Jun 6, 2017

Water-absorbing resin and preparing method thereof

Inventors: Ju-Hee Kim (Daejeon, KR); Du-Youn Ka (Daejeon, KR); Byoung-Tak Yim (Daejeon, KR); Byoung-Cheon Jo (Seoul, KR)
Assignees: SK GLOBAL CHEMICAL CO., LTD.; SK INNOVATION CO., LTD.
B01J20/261B01J20/3085C08F220/06
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Quick Facts
Patent No.
US 9,669,384
App. No.
15/011,732
Granted
Jun 6, 2017
Kind
B2
Abstract

Disclosed are a water-absorbing resin and a method of preparing the same, wherein absorbency under unload of the water-absorbing resin is 25 g/g or more, the absorbency under load is 20 g/g or more, and an increase in extractables at a high temperature represented by Equation 1 ranges from 1 or more but less than 3, thereby it is possible to solve a problem that gel-blocking of the water-absorbing resin is accelerated at a high temperature, and improve absorption rate and dry efficiency of the water-absorbing resin.

Claims (17)

1. A water-absorbing resin, having an absorbency under unload of 25 g/g or more, an absorbency under load of 20 g/g or more, and an increase in extractables at a high temperature in a range of 1 or more but less than 3, which is represented by Equation 1 below:

Increase in extractables at a high temperature=(Content of extractables at 90° C.)/(Content of extractables at 23° C.)  [Equation 1].

2. The water-absorbing resin according to claim 1 , wherein the water-absorbing resin is an acrylic polymer.

3. The water-absorbing resin according to claim 1 , wherein the water-absorbing resin is polymerized by including an internal cross-linking agent.

4. The water-absorbing resin according to claim 1 , wherein the absorbency under unload ranges from 25 g/g to 45 g/g.

5. The water-absorbing resin according to claim 1 , wherein the absorbency under load ranges from 20 g/g to 40 g/g.

6. The water-absorbing resin according to the claim 1 , wherein the increase in extractables at a high temperature represented by the above Equation 1 ranges from 1 to 2.8.

7. The water-absorbing resin according to the claim 1 , wherein the increase in extractables at a high temperature represented by the above Equation 1 ranges from 1 to 2.5.

8. The water-absorbing resin according to the claim 1 , wherein the increase in extractables at a high temperature represented by the above Equation 1 ranges from 1 to 2.

9. The water-absorbing resin according to the claim 1 , high-temperature swollen liquid permeability of the water-absorbing resin is 5.0 Darcy or more.

10. The water-absorbing resin according to the claim 1 , wherein the water-absorbing resin is produced by a process comprising:

polymerizing a composition which includes an acrylic monomer, a polymerization initiator and an internal cross-linking agent represented by Formula 1 below:

wherein R1 is an alkylene group having 1 to 20 carbon atoms, an arylene group having 6 to 12 carbon atoms or a combination of alkylene group and arylene group having a total 7 to 20 carbon atoms;

R2 is hydrogen, an alkyl group having 1 to 20 carbon atoms, an aryl group having 6 to 12 carbon atoms, or an alkyl group having 1 to 20 alkyl groups substituted with an aryl group having 6 to 12 carbon atoms; and

X is a vinyl group.

11. The water-absorbing resin according to the claim 1 , wherein the internal cross-linking agent is 5-benzyl-2,2-dimethyl-5-(4-vinylbenzyl)-[1,3]dioxane-4,6-dione.

12. The water-absorbing resin according to the claim 1 , wherein the internal cross-linking agent is included in an amount of 0.001 to 2 parts by weight to 100 parts by weight of the monomer.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 31, 2025
From: SK GEO CENTRIC CO., LTD.
To: SK INNOVATION CO., LTD.
Reel/Frame 073341/0952 →
CHANGE OF NAME Recorded Sep 2, 2022
From: SK GLOBAL CHEMICAL CO., LTD
To: SK GEO CENTRIC CO., LTD.
Reel/Frame 061371/0332 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 1, 2016
From: KIM, JU-HEE; KA, DU-YOUN; YIM, BYOUNG-TAK; JO, BYOUNG-CHEON
To: SK GLOBAL CHEMICAL CO., LTD.; SK INNOVATION CO., LTD.
Reel/Frame 037859/0779 →
Priority Claims (1)
KR 10-2015-0015467 · Jan 30, 2015 · national
Continuity (1)
Related Publication 20160220980A1 · Aug 4, 2016