IP Library Granted Patent US 9,644,322
Granted Patent B2
US 9,644,322 · App. 15/013,279 · Granted May 9, 2017

Solid articles from poly alpha-1,3-glucan and wood pulp

Inventor: Debora Flanagan Massouda (Wilmington, DE)
Assignee: E I DU PONT DE NEMOURS AND COMPANY
D21J3/12C12P19/04
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Quick Facts
Patent No.
US 9,644,322
App. No.
15/013,279
Granted
May 9, 2017
Kind
B2
Abstract

A solid article formed from poly alpha-1,3-glucan and wood pulp is disclosed as are methods for making the solid article. The articles are not water sensitive and are useful for producing strong molded articles from wood pulp.

Claims (17)

1. A solid article comprising:

(a) from 50 to 90% by wt. poly alpha-1,3-glucan; and

(b) from 10 to 50% by wt. wood pulp.

2. The solid article of claim 1 , further comprising: plasticizers, tougheners and/or fibrillar strengthening agents.

3. The solid article of claim 2 , wherein the plasticizer is glycerol.

4. The solid article of claim 1 , in the form of sheets, composites, laminates and molded parts.

5. A process for making a solid article comprising:

(a) preparing a poly alpha-1,3-glucan wet cake comprising;

(i) heating an enzyme reaction solution comprising an aqueous basic buffered solution of S. salivarius gtfJ enzyme, sucrose and, optionally, antimicrobial agent to make a slurry containing poly alpha-1,3-glucan;

(ii) filtering the slurry to isolate the poly alpha-1,3-glucan in the form of a wet cake; and

(iii) washing the wet cake with water;

(b) preparing a mixture from the wet cake with wood pulp, water and, optionally, plasticizers, tougheners and/or fibrillar strengthening agents;

(c) homogenizing the mixture;

(d) removing some water to form a flowable or malleable material;

(e) forming the flowable or malleable material into a shape; and

(f) drying the shape to form a solid article.

6. A solid article prepared according to claim 5 .

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2020
From: DUPONT INDUSTRIAL BIOSCIENCES USA, LLC
To: NUTRITION & BIOSCIENCES USA 4, INC.
Reel/Frame 055028/0496 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ENTITY TYPE PREVIOUSLY RECORDED AT REEL: 049879 FRAME: 0043. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Sep 6, 2019
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: DUPONT INDUSTRIAL BIOSCIENCES USA, LLC
Reel/Frame 050300/0408 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 26, 2019
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: DUPONT INDUSTRIAL BIOSCIENCES USA, LLC
Reel/Frame 049879/0043 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 2, 2016
From: MASSOUDA, DEBORA FLANAGAN
To: E.I. DUPONT DE NEMOURS AND COMPANY
Reel/Frame 038438/0162 →
Continuity (2)
Provisional Application 62112916 · Feb 6, 2015
Related Publication 20160230348A1 · Aug 11, 2016