IP Library Granted Patent US 10,465,152
Granted Patent B2
US 10,465,152 · App. 15/015,355 · Granted Nov 5, 2019

Systems and methods for stillage fractionation

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Quick Facts
Patent No.
US 10,465,152
App. No.
15/015,355
Granted
Nov 5, 2019
Kind
B2
Abstract

Systems and methods for fractionating whole stillage from an ethanol production facility are provided. Whole stillage undergoes a separation of its liquid portion (thin stillage) from the solid portion (fiber cake). In some embodiments, the solids and liquids in whole stillage may be separated utilizing a screening centrifuge. The fiber cake may be dried to generate a high fiber animal feed. The thin stillage may be provided to a three-phase separator for separation into an oil emulsion, an aqueous clarified stillage, and a protein paste. The protein paste may be dried to generate a high protein animal feed with greater than about 45% protein content. The clarified thin stillage is condensed to yield a syrup with greater than around 60% solids. The oil emulsion is subjected to a pH adjustment to liberate the oil from the emulsion, which is then separated.

Claims (22)

1. An ethanol plant that processes whole stillage comprising:

a fermentation apparatus for making a fermentation product;

a distillation apparatus adapted to separate ethanol from the fermentation product and form whole stillage;

a first separator for separating a thin stillage liquid output from the whole stillage, wherein the first separator comprises a centrifuge;

a second separator for separating a clarified liquid stillage output from at least a portion of the thin stillage liquid output, wherein said second separator comprises a centrifuge;

and

a connection for recycling a portion of the clarified liquid stillage output upstream for utilization as fermentation backset.

2. The ethanol plant of claim 1 , wherein the first separator produces a high fiber wet cake.

3. The ethanol plant of claim 2 further comprising:

a cake dryer for drying the high fiber wet cake to provide a high fiber animal feed product.

4. The ethanol plant of claim 3 , wherein the solid content of the high fiber wet cake is between 40% and 45% before drying.

5. The ethanol plant of claim 1 further comprising an evaporation apparatus or a reverse osmosis system for condensing a portion of the clarified liquid stillage to form a syrup.

6. The ethanol plant of claim 1 wherein the clarified liquid stillage contains less unfermentable solids than the thin stillage liquid.

7. The ethanol plant of claim 1 further comprising an evaporation apparatus for condensing a portion of the thin stillage liquid output.

8. An ethanol plant that processes whole stillage comprising:

a fermentation system adapted to produce a fermentation product;

a distillation system in fluid communication with the fermentation system, wherein the distillation system is adapted to separate ethanol from the fermentation product and form whole stillage;

a first centrifugation separation system in fluid communication with the distillation system, wherein the first centrifugation separation system is adapted to separate the whole stillage into wet cake and thin stillage output; and

a second centrifugation separation system in fluid communication with the first centrifugation separation system, wherein the second centrifugation separation system is adapted to separate at least a portion of the thin stillage output into an aqueous fraction output, an oil emulsion fraction, and a protein fraction, wherein the aqueous fraction output is in fluid communication with the fermentation system for utilization as backset.

9. The ethanol plant of claim 8 , further comprising:

a paste dryer for drying the protein fraction to provide a high protein animal feed product.

10. The ethanol plant of claim 8 further comprising: a third centrifugation separation system in fluid communication with the oil emulsion fraction and adapted to separate oil from the oil emulsion fraction.

Assignments (5)
SECURITY INTEREST Recorded Apr 3, 2020
From: POET RESEARCH, INC.
To: COBANK, ACB, AS ADMINISTRATIVE AGENT
Reel/Frame 052312/0801 →
SECURITY INTEREST Recorded Apr 2, 2020
From: POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 052295/0712 →
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 45398/0080 Recorded Apr 2, 2020
From: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: POET, LLC; POET RESEARCH, INC.; POET INVESTMENTS, INC.
Reel/Frame 052299/0822 →
SECURITY INTEREST Recorded Mar 30, 2018
From: POET, LLC; POET INVESTMENTS, INC.; POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 045398/0080 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 4, 2016
From: BOOTSMA, JASON ALAN
To: POET RESEARCH, INC.
Reel/Frame 037663/0554 →