IP Library Granted Patent US 10,135,074
Granted Patent B2
US 10,135,074 · App. 15/025,354 · Granted Nov 20, 2018

Carbon powder for catalyst, catalyst, electrode catalyst layer, membrane electrode assembly, and fuel cell using the carbon powder

Inventors: Shinichi Takahashi (Kanagawa, JP); Atsushi Ohma (Kanagawa, JP); Tetsuya Mashio (Kanagawa, JP); Ken Akizuki (Kanagawa, JP)
Assignees: NISSAN MOTOR CO., LTD.; NIPPON STEEL & SUMIKIN CHEMICAL CO., LTD.
H01M4/926B01J21/18H01M4/8673H01M4/9083H01M8/1004B01J23/40B01J35/0033B01J35/108B01J35/1028B01J35/1042B01J35/1057B01J35/1061B01J37/08C01B31/00C01P2006/12H01M2008/1095
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Quick Facts
Patent No.
US 10,135,074
App. No.
15/025,354
Granted
Nov 20, 2018
Kind
B2
Abstract

The present invention is to provide a carbon powder that can provide a catalyst having excellent durability and a catalyst. A carbon powder for catalyst of the present invention is a carbon powder containing as a main component carbon, which has a BET specific surface area per unit weight of 900 m 2 /g or greater, and a ratio R′ (D′/G intensity ratio) of peak intensity for a D′-band (D′ intensity) measured in the vicinity of 1620 cm −1 to peak intensity for a G-band (G intensity) measured in the vicinity of 1580 cm −1 by Raman spectroscopy of 0.6 or less.

Claims (14)

1. A catalyst having a catalyst metal supported on a carbon powder for catalyst, the carbon powder containing as a main component carbon and comprising:

a BET specific surface area per unit weight of 900 m 2 /g or greater;

a ratio R′ (D′/G intensity ratio) of peak intensity for a D′-band (D′ intensity) measured in the vicinity of 1620 cm −1 to peak intensity for a G-band (G intensity) measured in the vicinity of 1580 cm −1 by Raman spectroscopy of 0.6 or less; and

a ratio R (D/G intensity ratio) of peak intensity for a D-band (D intensity) measured in the vicinity of 1360 cm −1 to the peak intensity for the G-band (G intensity) measured in the vicinity of 1580 cm −1 by Raman spectroscopy is 1.7 or more,

wherein the carbon powder contains micropores having a radius of less than 1 nm and mesopores having a radius of 1 nm or more, and

wherein at least a portion of the catalyst metal is supported inside the mesopores.

2. The catalyst according to claim 1 , wherein the catalyst metal is platinum or comprises platinum and at least one of ruthenium, iridium, rhodium, palladium, osmium, tungsten, lead, iron, copper, silver, chromium, cobalt, nickel, manganese, vanadium, molybdenum, gallium, or aluminum.

3. An electrode catalyst layer for fuel cell comprising the catalyst according to claim 1 and an electrolyte.

4. A membrane electrode assembly for fuel cell comprising the electrode catalyst layer for fuel cell according to claim 3 .

5. A fuel cell comprising the membrane electrode assembly for fuel cell according to claim 4 .

6. An electrode catalyst layer for fuel cell comprising the catalyst according to claim 2 and an electrolyte.

7. The catalyst according to claim 1 , wherein a pore volume of the micropores is 0.3 cc/g-carbon powder or more.

8. The catalyst according to claim 1 , wherein a mode radius of pore distribution of micropores is 0.3 nm or more and less than 1 nm.

9. The catalyst according to claim 1 , wherein the ratio R (D/G intensity ratio) of peak intensity for a D-band (D intensity) measured in the vicinity of 1360 cm −1 to the peak intensity for the G-band (G intensity) measured in the vicinity of 1580 cm −1 by Raman spectroscopy is 1.7 or more and 2.5 or less.

Assignments (5)
CHANGE OF ADDRESS Recorded Nov 8, 2019
From: NIPPON STEEL CHEMICAL & MATERIAL CO., LTD.
To: NISSAN STEEL CHEMICAL & MATERIAL CO., LTD.
Reel/Frame 050968/0286 →
CORRECTIVE ASSIGNMENT TO CORRECT THE THE NAME OF THE ASSIGNEE PREVIOUSLY RECORDED ON REEL 048153 FRAME 0246. ASSIGNOR(S) HEREBY CONFIRMS THE NAME CHANGE. Recorded Mar 15, 2019
From: NIPPON STEEL & SUMIKIN CHEMICAL CO., LTD.
To: NIPPON STEEL CHEMICAL & MATERIAL CO., LTD.
Reel/Frame 048610/0244 →
CHANGE OF NAME Recorded Jan 28, 2019
From: NIPPON STEEL & SUMIKIN CHEMICAL CO., LTD.
To: NISSAN STEEL CHEMICAL & MATERIAL CO., LTD.
Reel/Frame 048153/0246 →
ASSIGNOR ASSIGNS ONE-HALF RIGHTS TO ASSIGNEE Recorded Oct 24, 2017
From: NISSAN MOTOR CO., LTD.
To: NIPPON STEEL & SUMIKIN CHEMICAL CO., LTD.
Reel/Frame 044280/0902 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 28, 2016
From: TAKAHASHI, SHINICHI; OHMA, ATSUSHI; MASHIO, TETSUYA; AKIZUKI, KEN
To: NISSAN MOTOR CO., LTD.
Reel/Frame 038112/0474 →
Priority Claims (1)
JP 2013-204163 · Sep 30, 2013 · national
Continuity (1)
Related Publication 20160233520A1 · Aug 11, 2016