IP Library Granted Patent US 9,963,757
Granted Patent B2
US 9,963,757 · App. 15/026,261 · Granted May 8, 2018

Precipitation hardening of tantalum coated metals

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Quick Facts
Patent No.
US 9,963,757
App. No.
15/026,261
Granted
May 8, 2018
Kind
B2
Abstract

A process includes: (a) providing a tantalum-coated metal alloy substrate; (b) heat annealing the tantalum-coated metal alloy substrate by heating to an annealing temperature for the tantalum-coated metal alloy substrate, holding at the annealing temperature for a period of time and then quenching to a temperature below 50 degrees Celsius; (c) heating the tantalum-coated metal substrate to the precipitation hardening temperature of the metal alloy substrate; and (d) cooling the tantalum-coated metal alloy substrate to a temperature below 50 degrees Celsius; wherein the process is further characterized by carrying out steps (b)-(d) under a tantalum-inert gas atmosphere and by quenching in step (b) and cooling in step (d) being carried out by flowing a tantalum-inert gas having a temperature of less than 50 degrees Celsius over the tantalum-coated metal alloy substrate.

Claims (10)

1. A process comprising:

(a) providing a tantalum-coated metal alloy substrate prepared by providing a precipitation hardened metal alloy substrate and applying tantalum to the substrate while sustaining a temperature greater than 700 degrees Celsius, characterized by resulting in a homogeneous tantalum coating over the metal alloy substrate;

(b) heat annealing the tantalum-coated metal alloy substrate by heating to an annealing temperature for the tantalum-coated metal alloy substrate, holding at the annealing temperature for a period of time and then quenching to a temperature below 50 degrees Celsius;

(c) heating the tantalum-coated metal substrate to the precipitation hardening temperature of the metal alloy substrate; and

(d) cooling the tantalum-coated metal alloy substrate to a temperature below 50 degrees Celsius;

wherein the process is further characterized by carrying out steps (b)-(d) under a tantalum-inert gas atmosphere and by quenching in step (b) and cooling in step (d) being carried out by flowing a tantalum-inert gas having a temperature of less than 50 degrees Celsius over the tantalum-coated metal alloy substrate.

2. The process of claim 1 , further characterized by the tantalum-inert gas comprising a noble gas.

3. The process of claim 1 , further characterize by the tantalum-inert gas comprising at least 99.999 mole-percent argon based on total tantalum-inert gas composition.

4. The process of claim 1 , further characterized by the metal alloy substrate that is tantalum-coated being a stainless steel.

5. The process of claim 1 , further characterized by step (d) causing the tantalum-coated metal alloy substrate to cool from the precipitation hardening temperature to a temperature below 50 degrees Celsius at a rate of 100 degrees Celsius per hour or faster and 200° C. per hour or slower.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 10, 2024
From: DOW GLOBAL TECHNOLOGIES LLC
To: THE DOW CHEMICAL COMPANY
Reel/Frame 069923/0030 →
CHANGE OF LEGAL ENTITY Recorded Sep 10, 2024
From: DDP SPECIALTY ELECTRONIC MATERIALS US, INC
To: DDP SPECIALTY ELECTRONIC MATERIALS US, LLC
Reel/Frame 068907/0881 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 10, 2024
From: THE DOW CHEMICAL COMPANY
To: DDP SPECIALTY ELECTRONIC MATERIALS US, INC
Reel/Frame 068922/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 15, 2018
From: WOODCRAFT, VALENTINA A.; LIENING, EUGENE L.
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 045221/0953 →