IP Library Granted Patent US 10,071,910
Granted Patent B2
US 10,071,910 · App. 15/033,002 · Granted Sep 11, 2018

Methods and systems for producing carbon aerogel

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Quick Facts
Patent No.
US 10,071,910
App. No.
15/033,002
Granted
Sep 11, 2018
Kind
B2
Abstract

Methods described herein generally relate to producing carbon aerogel. The method may include providing a carbon-containing polymeric material, and contacting the carbon-containing polymeric material with light, heat or both to produce the carbon aerogel. Systems and kits for producing carbon aerogel are also disclosed.

Claims (29)

1. A method of producing carbon aerogel, the method comprising:

providing a carbon-containing polymeric material;

exposing the carbon-containing polymeric material to at least one of light or heat selected to produce a carbon aerogel powder; and

collecting the produced carbon aerogel powder,

wherein the produced carbon aerogel powder comprises carbon nanoparticles, and wherein the carbon aerogel powder has a porous structure with an average pore diameter of about 2.5 nm.

2. The method of claim 1 , wherein the carbon-containing polymeric material comprises a synthetic polymer, a natural polymer, or a combination thereof.

3. The method of claim 1 , wherein the carbon-containing polymeric material comprises an epoxy resin, a phenolic resin, a urea resin, camphor, castor oil, turpentine, a polypropylene, a polystyrene, or a combination thereof.

4. The method of claim 1 , further comprising raising a temperature of the carbon-containing polymeric material to about 350° C. to about 650° C. when the carbon-containing polymeric material is exposed to light.

5. The method of claim 1 , wherein exposing the carbon-containing polymeric material to light comprises irradiating the carbon-containing polymeric material with the light for about 2 seconds to about 1 minute.

6. The method of claim 1 , wherein the light comprises a light beam produced by a laser that has a power of at least about 5 W.

7. The method of claim 6 , wherein the light beam has a wavelength of about 200 nm to about 11 μm.

8. The method of claim 1 , wherein the light comprises a focused beam of sunlight.

9. The method of claim 1 , wherein exposing the carbon-containing polymeric material to heat comprises heating the carbon-containing polymeric material for at least 10 minutes.

10. The method of claim 1 , wherein exposing the carbon-containing polymeric material to heat comprises heating the carbon-containing polymeric material for about 2 seconds to 1 minute.

11. The method of claim 1 , wherein the carbon nanoparticles have an average size of about 30 nm to about 75 nm.

12. The method of claim 1 , wherein the carbon nanoparticles have an average size of about 50 nm to about 55 nm.

13. The method of claim 1 , wherein at least about 60% of the carbon nanoparticles have a size of about 30 nm to about 75 nm.

14. The method of claim 1 , wherein at least about 50% of the carbon nanoparticles are porous carbon nanoparticles.

15. The method of claim 14 , wherein the porous carbon nanoparticles have an average pore diameter of at least about 1.5 nm and not more than about 50 nm.

16. The method of claim 1 , wherein the carbon aerogel powder has a BET surface area of about 600 m 2 /g to about 1100 m 2 /g.

17. The method of claim 1 , wherein the carbon aerogel powder has a bulk density of about 6 mg/cm 3 .

18. A method of producing carbon aerogel, the method comprising:

providing a carbon-containing polymeric material including at least one of an epoxy resin, a phenolic resin, a urea resin, camphor, castor oil, turpentine, a polypropylene, or a polystyrene;

exposing the carbon-containing polymeric material to at least one of light or heat selected to produce the carbon aerogel; and

collecting the produced carbon aerogel,

wherein the carbon aerogel powder has a porous structure with an average pore diameter of about 2.5 nm.

19. The method of claim 18 , wherein exposing the carbon-containing polymeric material to the at least one of light or heat produces carbon aerogel including a carbon aerogel powder that includes carbon nanoparticles.

20. The method of claim 19 , wherein the carbon nanoparticles have an average size of about 30 nm to about 75 nm.

21. The method of claim 19 , wherein the carbon nanoparticles have an average size of about 50 nm to about 55 nm.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Jul 31, 2019
From: CRESTLINE DIRECT FINANCE, L.P.
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 049924/0794 →
SECURITY INTEREST Recorded Jan 29, 2019
From: EMPIRE TECHNOLOGY DEVELOPMENT LLC
To: CRESTLINE DIRECT FINANCE, L.P.
Reel/Frame 048373/0217 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 28, 2016
From: ZHAO, CHONGJUN; DONG, JIANBO; HUANG, YOUFU; MA, JINGWEI; QIAN, XIUZHEN
To: EAST CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY
Reel/Frame 038414/0092 →