IP Library Granted Patent US 9,819,029
Granted Patent B2
US 9,819,029 · App. 15/043,726 · Granted Nov 14, 2017

Method of making a fuel cell component

Inventors: Kevin Arpin (Coventry, CT); Nicole Hofstetter (Coventry, CT)
Assignee: DOOSAN FUEL CELL AMERICA, INC.
H01M4/8807H01M4/8605H01M4/8657H01M4/8668H01M4/8828H01M4/8835H01M4/8878H01M4/8882H01M4/9041
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,819,029
App. No.
15/043,726
Granted
Nov 14, 2017
Kind
B2
Abstract

An illustrative example method of making a fuel cell component includes mixing a catalyst material with a hydrophobic binder in a solvent to establish a liquid mixture having at least some coagulation of the catalyst material and the hydrophobic binder. The liquid mixture is applied to at least one side of a porous gas diffusion layer. At least some of the solvent of the applied liquid mixture is removed from the porous gas diffusion layer. The catalyst material remaining on the porous gas diffusion layer is dried under pressure.

Claims (36)

1. A method of making a fuel cell component, the method comprising:

mixing a catalyst material with a hydrophobic binder in a solvent to establish a liquid mixture having at least some coagulation of the catalyst material and the hydrophobic binder;

applying the liquid mixture to at least one side of a porous gas diffusion layer;

removing at least some of the solvent of the applied liquid mixture from the porous gas diffusion layer using a vacuum to pull the at least some of the solvent through the porous gas diffusion layer; and

drying the catalyst material remaining on the porous gas diffusion layer under pressure.

2. The method of claim 1 , wherein the mixing includes flocculating the mixture to establish the at least some coagulation of the catalyst material and the hydrophobic binder.

3. The method of claim 1 , wherein the mixing includes mixing water, the catalyst material and the hydrophobic binder.

4. The method of claim 3 , wherein the catalyst material comprises a metal and the hydrophobic binder comprises polytetrafluoroethylene.

5. The method of claim 1 , wherein the applying comprises coating the at least one side of the porous gas diffusion layer with the mixture.

6. The method of claim 5 , wherein the applying comprises at least one of

curtain coating the mixture onto the porous gas diffusion layer;

spray coating the mixture onto the porous gas diffusion layer;

doctor blading the mixture onto the porous gas diffusion layer;

slot die coating the mixture onto the porous gas diffusion layer;

transfer printing the mixture onto the porous gas diffusion layer; and

screen printing the mixture onto the porous gas diffusion layer.

7. The method of claim 1 , comprising

supporting the porous gas diffusion layer on a first side of a surface; and

establishing the vacuum from a second, opposite side of the surface.

8. The method of claim 7 , wherein the established vacuum pulls the at least some of the solvent through the porous gas diffusion layer and the surface.

9. The method of claim 7 , wherein the surface comprises at least one of a table and a belt.

10. The method of claim 1 , wherein the drying comprises heating the catalyst material remaining on the porous gas diffusion layer using a temperature of 240° F. (115° C.).

11. The method of claim 10 , wherein the pressure is 200 psi (14 bar).

12. The method of claim 1 , wherein the drying comprises applying an axial load using a press to achieve the pressure.

13. The method of claim 12 , the press comprises at least one of a hot press, a heated roll press, and a heated double belt press.

14. The method of claim 1 , comprising sintering the catalyst material remaining on the porous gas diffusion layer after controlled drying.

15. The method of claim 1 , wherein a resulting layer of catalyst material covers the at least one side of the porous gas diffusion layer.

16. The method of claim 15 , wherein the resulting layer of catalyst material is generally uniform across the at least one side of the porous gas diffusion layer.

17. The method of claim 15 , wherein the resulting layer of catalyst material is at least 50 microns thick.

18. A method of making a fuel cell component, the method comprising:

mixing a catalyst material with a hydrophobic binder in a solvent to establish a liquid mixture having at least some coagulation of the catalyst material and the hydrophobic binder;

applying the liquid mixture to at least one side of a porous gas diffusion layer;

removing at least some of the solvent of the applied liquid mixture from the porous gas diffusion layer by supporting the porous gas diffusion layer on a first side of a surface, establishing a vacuum from a second, opposite side of the surface and using the vacuum for the removing; and

drying the catalyst material remaining on the porous gas diffusion layer under pressure.

19. The method of claim 18 , wherein the established vacuum pulls the at least some of the solvent through the porous gas diffusion layer and the surface.

20. The method of claim 18 , wherein the surface comprises at least one of a table and a belt.

Assignments (2)
CHANGE OF NAME Recorded Apr 21, 2022
From: DOOSAN FUEL CELL AMERICA, INC.
To: HYAXIOM, INC.
Reel/Frame 059747/0284 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 15, 2016
From: ARPIN, KEVIN; HOFSTETTER, NICOLE
To: DOOSAN FUEL CELL AMERICA, INC.
Reel/Frame 037734/0428 →
Continuity (1)
Related Publication 20170237077A1 · Aug 17, 2017