IP Library Granted Patent US 10,028,921
Granted Patent B1
US 10,028,921 · App. 15/054,797 · Granted Jul 24, 2018

Phytonadione compositions and related methods

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Quick Facts
Patent No.
US 10,028,921
App. No.
15/054,797
Granted
Jul 24, 2018
Kind
B1
Abstract

Stable Phytonadione compositions for parenteral administration are provided which comprise (E) isomer of phytonadione at or greater than 97% w/w as the active ingredient, and is substantially free of (Z) isomer. Said compositions are stable, sterile, and particulate-free. Further, said compositions reduce or avoid allergic reactions to benzyl alcohol and polysorbate. In some aspects, the compositions are free or substantially free of benzyl alcohol and/or reduced amounts of polysorbate. Methods of manufacture and methods of administration also provided.

Claims (12)

1. A stable, injectable, sterile, particulate-matter-free, aqueous phytonadione composition comprising Phytonadione in its (E) isomer form that has less than or equal to 3% w/w of its (Z) isomer, at a concentration of from about 100 ug/ml to about 20 mg/ml; and optionally a pH adjuster, wherein the composition has a pH of from about 3.5 to about 8.0.

2. The composition of claim 1 , wherein said (Z) isomer is present from 0.5% to less than or equal to 3% w/w of the (E) isomer.

3. The composition of claim 1 , wherein said composition is free of benzyl alcohol.

4. The composition of claim 1 , wherein said composition is free of cremophor and propylene glycol.

5. The composition of claim 1 , wherein the composition comprises less than 1:10 ratio of (E)-isomer of phytonadione:polysorbate.

6. The composition of claim 1 , wherein said composition is provided in a non-reacting glass or non-reacting polymeric container selected from a vial container or a pre-filled syringe container.

7. The composition of claim 6 , wherein the non-reacting polymeric container is made of polyethylene or polypropylene or a combination thereof.

8. The composition of claim 1 , wherein an epoxide derivative of the (E) isomer of phytonadione is present at less than 4% w/w of the (E) isomer.

9. A method comprising: administering the composition of claim 1 to a mammal.

10. The method of claim 9 , wherein the mammal is a human.

11. A method of reducing the potential for anaphylactic reaction associated with phytonadione administration comprising: administering a composition to a patient in need thereof, the composition comprising Phytonadione in its (E) isomer form that has less than or equal to 3% w/w of (Z) isomer, at a concentration of from about 100 ug/ml to about 20 mg/ml; and optionally a pH adjuster, wherein the composition has a pH of from about 3.5 to about 8.0, and wherein said composition is free of benzyl alcohol and wherein the composition comprises polysorbate at a concentration of less than about 1:10 ratio of (E) isomer of phytonadione:polysorbate.

12. The method of claim 11 , wherein the composition is administered from a vial or a pre-filled syringe wherein the vial or pre-filled syringe is selected from a non-reacting glass or polymeric material.

Assignments (5)
SECURITY INTEREST Recorded Jun 30, 2021
From: EXELA HOLDINGS, INC.; EXELA PHARMA SCIENCES, LLC; EXELA PHARMSCI, INC.; EXELA STERILE MEDICINES LLC; EXELA STERILE PRODUCTS LLC; EXELA STERILE EQUIPMENT, LLC; EXELA ADVANCED STRATEGIES LLC; AGELEX, LLC; EXELA HEALTH SYSTEMS, LLC; EXELA INITIATIVES, LLC; EXELA INNOVATIONS, LLC
To: LIVE OAK BANKING COMPANY
Reel/Frame 056722/0188 →
SECURITY INTEREST Recorded Jun 30, 2021
From: EXELA HOLDINGS, INC.; EXELA PHARMA SCIENCES, LLC; EXELA PHARMSCI, INC.; EXELA STERILE MEDICINES LLC; EXELA STERILE PRODUCTS LLC; EXELA STERILE EQUIPMENT, LLC; EXELA ADVANCED STRATEGIES LLC; AGELEX, LLC; EXELA HEALTH SYSTEMS, LLC; EXELA INITIATIVES, LLC; EXELA INNOVATIONS, LLC
To: LIVE OAK BANKING COMPANY
Reel/Frame 056722/0250 →
SECURITY INTEREST Recorded Jun 30, 2020
From: EXELA HOLDINGS, INC.
To: DEERFIELD PRIVATE DESIGN FUND IV, L.P.
Reel/Frame 053083/0884 →
SECURITY INTEREST Recorded Apr 19, 2017
From: EXELA PHARMA SCIENCES, LLC
To: DEERFIELD PRIVATE DESIGN FUND IV, L.P., AS COLLATERAL AGENT
Reel/Frame 042061/0473 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 15, 2016
From: KONERU, PHANESH; MALLIPEDDI, SREERARAMA MURTHY; STERLING, JONATHAN E.
To: EXELA HOLDINGS, INC
Reel/Frame 039437/0538 →