IP Library Granted Patent US 10,035,947
Granted Patent B2
US 10,035,947 · App. 15/068,134 · Granted Jul 31, 2018

Method for chemically controlling delay time for breaking polymers

Inventors: Ayodele Okunola (Calgary, CA); Dawn Friesen (Calgary, CA); Sally Lawrence (Calgary, CA)
Assignee: LOS ACQUISITION CO. I LLC
C09K8/68C09K8/88C09K8/90E21B43/26C09K2208/26C09K2208/28
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Quick Facts
Patent No.
US 10,035,947
App. No.
15/068,134
Granted
Jul 31, 2018
Kind
B2
Abstract

A breaker system for a fracturing fluid having a polymer, includes an oxidative polymer breaker which includes water, a persulfate and a transition metal chelate having more than one accessible oxidation state, which inhibits or delays the break of the polymer by the breaker.

Claims (7)

1. A breaker system for a fracturing fluid having a polymer, comprising an oxidative polymer breaker comprising water, a persulfate and an inhibitor system comprising a transition metal chelate which inhibits the oxidative breaking action of the persulfate on the polymer.

2. The breaker system of claim 1 wherein the transition metal has more than one accessible oxidation state.

3. The breaker system of claim 1 wherein the transition metal chelate comprises an iron aminocarboxylate.

4. The breaker system of claim 3 wherein the iron aminocarboxylate comprises iron methylglycinediacetic acid (MGDA) ethylenediaminetetraacetic acid (EDTA), or nitriloacetic acid (NTA).

5. The breaker system of claim 1 wherein the persulfate is a persulfate of sodium, ammonium or potassium.

6. The breaker system of claim 1 wherein the water comprises fresh water or brine.

7. The breaker system of claim 1 wherein the inhibitor system increases either an end point or a delay time of the breaker system, or both, by at least 50%, or 100%, or 200%, under the same conditions as the breaker system without the inhibitor system.

Assignments (4)
CHANGE OF NAME Recorded Jan 13, 2025
From: LIBERTY OILFIELD SERVICES LLC
To: LIBERTY ENERGY SERVICES LLC
Reel/Frame 069881/0664 →
MERGER AND CHANGE OF NAME Recorded Dec 9, 2021
From: LOS ACQUISITION CO I LLC; LIBERTY OILFIELD SERVICES LLC
To: LIBERTY OILFIELD SERVICES LLC
Reel/Frame 058351/0853 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 3, 2021
From: SANJEL CANADA LTD.
To: LOS ACQUISITION CO I LLC
Reel/Frame 058277/0736 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 23, 2021
From: OKUNOLA, AYODELE; FRIESEN, DAWN; LAWRENCE, SALLY
To: SANJEL CANADA LTD.
Reel/Frame 058189/0966 →
Continuity (2)
Provisional Application 62133065 · Mar 13, 2015
Related Publication 20160264850A1 · Sep 15, 2016