IP Library Granted Patent US 11,660,267
Granted Patent B2
US 11,660,267 · App. 15/100,160 · Granted May 30, 2023

Sublingual formulation of riluzole

Inventors: Vladimir Coric (Madison, CT); Robert Berman (Stonington, CT); Ronald S. Vladyka (Somerset, NJ); Amgad Saleh (Dayton, NJ); Danny Yu (Somerville, MA)
Assignee: Biohaven Therapeutics Ltd.
A61K9/006A61K9/0056A61K9/08A61K9/20A61K31/428A61K47/20A61K47/26A61P25/00A61P25/16A61P25/18A61P25/22A61P25/24A61P25/28A61P25/30
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Quick Facts
Patent No.
US 11,660,267
App. No.
15/100,160
Granted
May 30, 2023
Kind
B2
Abstract

Disclosed is sublingual administration of riluzole. In particular, a method for treating a neuropsychiatric disorder or symptom by administering a sublingual formulation of riluzole is provided. In addition, a method of relieving or reducing oral pain using the sublingual formulation of riluzole is disclosed.

Claims (13)

1. A sublingual formulation in the form of a lyophilized, tableted pharmaceutical composition that provides sublingual absorption of riluzole comprising a pharmaceutically effective amount of riluzole or a pharmaceutically acceptable salt thereof, said formulation further comprising gelatin as a tablet binder in an amount of 1-10% based on the total weight of the pharmaceutical composition, mannitol or sorbitol as a bulking agent in an amount of 2-4% based on the total weight of the pharmaceutical composition, and docusate sodium as a solubilizing agent in an amount of 0.01-0.5% based on the total weight of the pharmaceutical composition, wherein the sublingual formulation has a great C max an earlier or less T max , or a great AUC per milligram of the riluzole than the same dose of orally administered riluzole.

2. The sublingual formulation of claim 1 further comprising a flavoring agent.

3. The sublingual formulation of claim 1 further comprising a sweetener.

4. The sublingual formulation of claim 3 wherein said sweetener comprises sucralose.

5. A sublingual formulation in the form of a lyophilized, tableted pharmaceutical composition that provides sublingual absorption of riluzole comprising an effective amount of riluzole or a pharmaceutically acceptable salt, solvate, anomer, enantiomer, hydrate or prodrug thereof, said formulation further comprising gelatin as a tablet binder in an amount of 1-10% based on the total weight of the pharmaceutical composition, mannitol or sorbitol as a bulking agent in an amount of 2-4% based on the total weight of the pharmaceutical composition, and docusate sodium as a solubilizing agent in an amount of 0.01-0.5% based on the total weight of the pharmaceutical composition, said sublingual formulation in the form of a lyophilized, tableted pharmaceutical composition capable of providing an AUC at a dose of 35 mg 10 of from 110% to 180% of the AUC of an oral tablet formulation at a dose of 50 mg, said AUC being measured at 0.5 hours, 1 hour or 2 hours after administration as measured in accordance with Example 6.

6. The sublingual formulation of claim 5 which further comprises mint flavoring.

7. The sublingual formulation of claim 5 which further comprises sucralose.

8. A lyophilized, tableted pharmaceutical composition suitable for sublingual administration comprising riluzole in an amount of 5-25% based on the total weight of the pharmaceutical composition, gelatin as a tablet binder in an amount of 1-10% based on the total weight of the pharmaceutical composition, mannitol in an amount of 2-4% based on the total weight of the pharmaceutical composition, docusate sodium in an amount of 0.01-0.5% based on the total weight of the pharmaceutical composition, sucralose and mint flavoring; said composition capable of providing a higher AUC ratio than the predicted AUC ratio of an oral tablet formulation comprising 50 mg of riluzole, said AUC being measured at 0.5 hours, 1 hour or 2 hours as measured in accordance with Example 6.

9. The lyophilized, tableted pharmaceutical composition of claim 8 wherein the AUC 0-0.5 ratio for a lyophilized pharmaceutical composition comprising 35 mg of riluzole is about 180% of the predicted AUC 0-0.5 ratio of an oral tablet formulation comprising 50 mg of riluzole.

10. The lyophilized, tableted pharmaceutical composition of claim 8 wherein the AUC 0-1 ratio for a lyophilized pharmaceutical composition comprising 35 mg of riluzole is about 136% of the predicted AUC 0-1 ratio of an oral tablet formulation comprising 50 mg of riluzole.

11. The lyophilized, tableted pharmaceutical composition of claim 8 wherein the AUC 0-2 ratio for a lyophilized pharmaceutical composition comprising 35 mg of riluzole is about 110% of the predicted AUC 0-2 ratio of an oral tablet formulation comprising 50 mg of riluzole.

12. The lyophilized, tableted pharmaceutical composition of claim 8 comprising an effective amount of riluzole to provide a daily dose of 80 mg.

13. The lyophilized, tableted pharmaceutical composition of claim 12 comprising 40 mg of riluzole.

Assignments (4)
RELEASE OF SECURITY INTEREST Recorded Apr 27, 2025
From: SIXTH STREET SPECIALTY LENDING, INC.
To: BIOHAVEN PHARMACEUTICAL HOLDING COMPANY LTD.; BIOHAVEN THERAPEUTICS LTD.; BIOHAVEN PHARMACEUTICAL IRELAND DESIGNATED ACTIVITY COMPANY
Reel/Frame 071083/0399 →
PATENT SECURITY AGREEMENT Recorded Aug 7, 2020
From: BIOHAVEN PHARMACEUTICAL HOLDING COMPANY LTD.; BIOHAVEN THERAPEUTICS LTD; BIOHAVEN PHARMACEUTICAL IRELAND DESIGNATED ACTIVITY COMPANY
To: SIXTH STREET SPECIALTY LENDING, INC., AS ADMINISTRATIVE AGENT
Reel/Frame 053428/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2020
From: BIOHAVEN PHARMACEUTICAL HOLDING COMPANY LTD.
To: BIOHAVEN THERAPEUTICS LTD.
Reel/Frame 053403/0391 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 24, 2017
From: CORIC, VLADIMIR; BERMAN, ROBERT; VLADYKA, RONALD SAMUEL; SALEH, AMGAD; YU, DANNY
To: BIOHAVEN PHARMACEUTICAL HOLDING COMPANY, LTD.
Reel/Frame 043928/0530 →
Continuity (2)
Provisional Application 62083094 · Nov 21, 2014
Related Publication 20180153794A1 · Jun 7, 2018
Cited By (1)
US 12,496,301