IP Library Granted Patent US 9,914,845
Granted Patent B2
US 9,914,845 · App. 15/101,014 · Granted Mar 13, 2018

Fine silver particle dispersing solution

Inventors: Takashi Hinotsu (Okayama, JP); Tomonori Shibayama (Okayama, JP); Hiromasa Miyoshi (Okayama, JP)
Assignee: Dowa Electronics Materials Co., Ltd.
C09D11/52B22F1/0022B22F1/0062B22F1/0074B22F9/24C09C1/62C09D11/033C09D11/037C09D11/322C09D11/36H01B1/22B22F1/0018
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Quick Facts
Patent No.
US 9,914,845
App. No.
15/101,014
Granted
Mar 13, 2018
Kind
B2
Abstract

There is produced a fine silver particle dispersing solution which contains: fine silver particles (the content of silver in the fine silver particle dispersing solution is 30 to 90% by weight), which have an average primary particle diameter of 1 to 100 nm and which are coated with an amine having a carbon number of 8 to 12, such as octylamine, serving as an organic protective material; a polar solvent (5 to 70% by weight) having a boiling point of 150 to 300° C.; and an acrylic dispersing agent (1.5 to 5% by weight with respect to the fine silver particles), such as a dispersing agent of at least one of acrylic acid ester and methacrylic acid ester.

Claims (13)

1. A fine silver particle dispersing solution comprising:

a polar solvent having a boiling point of 150 to 300° C. and having a solubility parameter (SP value) of 8.0 to 12.0;

fine silver particles coated with an amine having a carbon number of 8 to 12 as an organic protective material, the fine silver particles being added to the polar solvent; and

an acrylic dispersing agent added to the polar solvent, the amount of the acrylic dispersing agent being in the range of from 1.5% to (2.0×100/65.9) % by weight with respect to that of the fine silver particles.

2. A fine silver particle dispersing solution as set forth in claim 1 , wherein said amine is octylamine.

3. A fine silver particle dispersing solution as set forth in claim 1 , wherein said fine silver particles have an average primary particle diameter of 1 to 100 nm.

4. A fine silver particle dispersing solution as set forth in claim 1 , wherein said polar solvent having the boiling point of 150 to 300° C. is terpineol.

5. A fine silver particle dispersing solution as set forth in claim 1 , wherein said polar solvent having the boiling point of 150 to 300° C. is diethylene glycol monobutyl ether, diethylene glycol dibutyl ether or diethylene glycol monobutyl ether acetate.

6. A fine silver particle dispersing solution as set forth in claim 1 , wherein said acrylic dispersing agent is a dispersing agent of at least one of acrylic acid ester and methacrylic acid ester.

7. A fine silver particle dispersing solution as set forth in claim 1 , wherein said acrylic dispersing agent is a dispersing agent of methacrylic acid butyl ester.

8. A fine silver particle dispersing solution as set forth in claim 1 , wherein the content of silver in said fine silver particle dispersing solution is 30 to 90% by weight.

9. A fine silver particle dispersing solution as set forth in claim 1 , wherein the content of said polar solvent in said fine silver particle dispersing solution is 5 to 70% by weight.

10. A fine silver particle dispersing solution as set forth in claim 1 , wherein the amount of said acrylic dispersing agent is in the range of from 1.5% to 3% by weight with respect to that of the fine silver particles.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2016
From: HINOTSU, TAKASHI; SHIBAYAMA, TOMONORI; MIYOSHI, HIROMASA
To: DOWA ELECTRONICS MATERIALS CO., LTD.
Reel/Frame 038773/0504 →
Priority Claims (3)
JP 2013-255191 · Dec 10, 2013 · national
JP 2014-079824 · Apr 9, 2014 · national
JP 2014-213600 · Oct 20, 2014 · national
Continuity (1)
Related Publication 20160297982A1 · Oct 13, 2016