IP Library Granted Patent US 10,463,069
Granted Patent B2
US 10,463,069 · App. 15/101,303 · Granted Nov 5, 2019

Nicotine liquid formulations for aerosol devices and methods thereof

Inventors: Adam Bowen (San Francisco, CA); Chenyue Xing (San Francisco, CA)
Assignee: JUUL LABS, INC.
A24B15/16A24B15/167A24B15/301A24B15/32A24F47/008
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,463,069
App. No.
15/101,303
Granted
Nov 5, 2019
Kind
B2
Abstract

A nicotine liquid formulation comprising nicotine, an acid, and a biologically acceptable liquid carrier, wherein heating an amount of said nicotine liquid formulation using low temperature electronic vaporization device, i.e. an electronic cigarette, generates an inhalable aerosol, and wherein at least about 50% of said acid in said amount is in said aerosol, and wherein at least about 90% of said nicotine in said amount is in said aerosol.

Claims (19)

1. A method of generating an inhalable aerosol comprising nicotine for delivery to a user, the method comprising forming an aerosol by heating an amount of a nicotine liquid formulation in an electronic cigarette, wherein:

(a) the electronic cigarette comprises the nicotine liquid formulation and a heater;

(b) the nicotine liquid formulation comprises said nicotine at a concentration of 1% (w/w) to 6% (w/w), benzoic acid, and a biologically acceptable liquid carrier; and

(c) the benzoic acid and nicotine are in a molar ratio from 0.7:1 to 1.5:1.

2. The method of claim 1 , wherein said amount comprises about 4 uL of said nicotine liquid formulation.

3. The method of claim 1 , wherein said amount comprises about 4.5 mg of said nicotine liquid formulation.

4. The method of claim 1 , wherein the concentration of said nicotine is at least 4% (w/w).

5. The method of claim 1 , wherein the nicotine is stabilized as a nicotine salt in said aerosol.

6. The method of claim 1 , wherein one or more particles of said aerosol are sized for delivery to alveoli in a lung of said user.

7. The method of claim 1 , wherein said molar ratio of said benzoic acid to said nicotine is from 0.9:1 to 1.2:1.

8. The method of claim 1 , wherein said molar ratio of said benzoic acid to said nicotine is about 1:1.

9. The method of claim 1 , wherein said nicotine concentration is about 5% (w/w).

10. The method of claim 1 , wherein said biologically acceptable liquid carrier comprises from about 20% to about 50% of propylene glycol and from about 80% to about 50% of vegetable glycerin.

11. The method of claim 1 , wherein said biologically acceptable liquid carrier comprises about 30% propylene glycol and about 70% vegetable glycerin.

12. The method of claim 1 , wherein said heater heats said amount of said nicotine liquid formulation from about 150° C. to about 250° C.

13. The method of claim 1 , wherein said heater heats said amount of said nicotine liquid formulation from about 180° C. to about 220° C.

14. The method of claim 1 , wherein said heater heats said amount of said nicotine liquid formulation to about 200° C.

15. The method of claim 1 , wherein said nicotine liquid formulation further comprises an additional acid selected from the group consisting of: pyruvic acid, salicylic acid, levulinic acid, malic acid, succinic acid, and citric acid.

16. The method of claim 15 wherein said additional acid forms an additional nicotine salt.

Assignments (14)
RELEASE OF SECURITY INTEREST Recorded Oct 17, 2024
From: ALTER DOMUS (US) LLC
To: JUUL LABS, INC.; VMR PRODUCTS LLC; ENVENIO INC.
Reel/Frame 069185/0228 →
SECURITY INTEREST Recorded Jul 11, 2023
From: JUUL LABS, INC.; VMR PRODUCTS LLC; ENVENIO INC.
To: ALTER DOMUS (US) LLC
Reel/Frame 064252/0225 →
CORRECTIVE ASSIGNMENT TO CORRECT THE THE ASSIGNEE ADDRESS PREVIOUSLY RECORDED AT REEL: 062114 FRAME: 0196. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Dec 23, 2022
From: JUUL LABS, INC.
To: JLI NATIONAL SETTLEMENT TRUST
Reel/Frame 062214/0142 →
SECURITY INTEREST Recorded Dec 10, 2022
From: JUUL LABS, INC.
To: JLI NATIONAL SETTLEMENT TRUST
Reel/Frame 062114/0195 →
RELEASE OF SECURITY INTEREST Recorded Oct 1, 2022
From: CORTLAND CAPITAL MARKET SERVICES LLC
To: JUUL LABS, INC.
Reel/Frame 061587/0947 →
SECURITY INTEREST Recorded Sep 30, 2022
From: JUUL LABS, INC.
To: ALTER DOMUS (US) LLC
Reel/Frame 061578/0865 →
RELEASE OF SECURITY INTEREST Recorded Jun 28, 2022
From: MUFG UNION BANK, N.A.
To: JUUL LABS, INC.
Reel/Frame 060446/0261 →
SECURITY INTEREST Recorded Aug 2, 2019
From: JUUL LABS, INC.
To: CORTLAND CAPITAL MARKET SERVICES LLC
Reel/Frame 049948/0881 →
TERMINATION OF PATENT SECURITY AGREEMENT Recorded Apr 26, 2019
From: MUFG UNION BANK, N.A
To: JUUL LABS, INC.
Reel/Frame 049013/0397 →
PATENT SECURITY AGREEMENT Recorded Apr 26, 2019
From: JUUL LABS, INC.
To: MUFG UNION BANK, N.A.
Reel/Frame 049013/0519 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNOR EXECUTION DATE PREVIOUSLY RECORDED AT REEL: 043544 FRAME: 0004. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF NAME. Recorded Aug 6, 2018
From: PAX LABS, INC.
To: JUUL LABS, INC.
Reel/Frame 046732/0847 →
PATENT SECURITY AGREEMENT Recorded Apr 3, 2018
From: JUUL LABS, INC
To: MUFG UNION BANK, N.A.
Reel/Frame 045832/0328 →
CHANGE OF NAME Recorded Aug 14, 2017
From: PAX LABS, INC.
To: JUUL LABS, INC.
Reel/Frame 043544/0004 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 14, 2016
From: BOWEN, ADAM; XING, CHENYUE
To: PAX LABS, INC.
Reel/Frame 040313/0638 →
Continuity (2)
Provisional Application 61912507 · Dec 5, 2013
Related Publication 20160302471A1 · Oct 20, 2016