IP Library Granted Patent US 10,087,305
Granted Patent B2
US 10,087,305 · App. 15/104,376 · Granted Oct 2, 2018

Nucleated crystallization of poly(trimethylene-2,5-furandicarboxylate) (PTF) and articles made therefrom

Inventors: Gordon Mark Cohen (Wynnewood, PA); Fredrik Nederberg (East Amherst, NY); Bhuma Rajagopalan (Wilmington, DE)
Assignee: E I DU PONT DE NEMOURS AND COMPANY
C08K5/0083C08G63/672C08G63/78C08J5/18C08K3/32C08K5/098C08K5/52C08G2250/00C08J2367/02C08K2003/324
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Quick Facts
Patent No.
US 10,087,305
App. No.
15/104,376
Granted
Oct 2, 2018
Kind
B2
Abstract

Disclosed herein are compositions and articles made therefrom, the compositions comprising poly(trimethylene-2,5-furandicarboxylate) and one or more of a plasticizer, a neutralized carboxylic acid salt or trisodium phosphate as a nucleating agent, and a copolyester derived from furandicarboxylic acid, 1,3 propanediol and at least one poly(alkylene ether) glycol (PAEG), the copolyester comprising a Furan-PAEG soft segment and a PTF hard segment.

Claims (16)

1. A composition comprising:

a) 80-99 wt % of poly(trimethylene-2,5-furandicarboxylate); and

b) 1-20 wt % of a plasticizer of the formula:

A-O—[CHX—(CH 2 ) k —O] j —B,

where

k is an integer from 1 to 3,

j is an integer from 4 to 25,

A and B are each independently selected from an alkyl group, an acyl group, or an aroyl group, each containing 1 to 10 carbon atoms,

X is H, CH 3 or C 2 H 5 ,

wherein the amounts are based on the total weight of the composition.

2. The composition of claim 1 , further comprising 0.1-10 wt % of a neutralized carboxylic acid salt or trisodium phosphate as a nucleating agent, wherein the amounts are based on the total weight of the composition.

3. An article comprising the composition of claim 1 , wherein the article is in the form of a sheet, film, or molded article.

4. The composition of claim 1 , wherein the plasticizer is polyethylene glycol bis(2-ethylhexanoate).

5. The composition of claim 4 , further comprising 0.1-10 wt % of a neutralized carboxylic acid salt or trisodium phosphate as a nucleating agent, wherein the amounts are based on the total weight of the composition.

6. An article comprising the composition of claim 4 , wherein the article is in the form of a sheet, film, or molded article.

7. An article comprising the composition of claim 5 , wherein the article is in the form of a sheet, film, or molded article.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 29, 2024
From: DUPONT INDUSTRIAL BIOSCIENCES USA, LLC
To: COVATION INC.
Reel/Frame 066376/0798 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 18, 2024
From: DUPONT INDUSTRIAL BIOSCIENCES USA, LLC
To: COVATION INC.
Reel/Frame 066350/0534 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ENTITY TYPE PREVIOUSLY RECORDED AT REEL: 049879 FRAME: 0043. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Sep 6, 2019
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: DUPONT INDUSTRIAL BIOSCIENCES USA, LLC
Reel/Frame 050300/0408 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 26, 2019
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: DUPONT INDUSTRIAL BIOSCIENCES USA, LLC
Reel/Frame 049879/0043 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 16, 2016
From: COHEN, GORDON MARK; NEDERBERG, FREDRIK; RAJAGOPALAN, BHUMA
To: E. I. DU PONT DE NEMOURS AND COMPANY
Reel/Frame 039455/0541 →
Continuity (3)
Provisional Application 61918728 · Dec 20, 2013
Provisional Application 62055730 · Sep 26, 2014
Related Publication 20160312001A1 · Oct 27, 2016