Method of treatment against corrosion and against wear
Subjecting an aluminum or aluminum alloy substrate to anti-corrosion and anti-wear treatment that is applicable in particular in the field of aviation for protecting certain mechanical parts of airplanes or helicopters that are subjected simultaneously to corrosion and to wear, including applying to the substrate, a sol-gel treatment step forming a sol-gel layer; and after the sol-gel treatment step, a hard oxidation step forming a hard oxide layer.
1. A method of subjecting an aluminum or aluminum alloy substrate to treatment against corrosion and against wear, the method comprising:
forming a first oxide layer on a surface of the substrate, the first oxide layer being porous and including pores;
applying a sol-gel layer to the first oxide layer, the sol-gel filling in the pores of the first oxide layer;
locally removing only the first oxide layer and the sol-gel layer at a zone of the substrate such that the surface of substrate at the zone of the substrate is free of the first oxide layer and the sol-gel layer and a geometry of the surface of the substrate at the zone of the substrate is unchanged; and
forming a second oxide layer at the zone of the substrate, the second oxide layer being a hard oxide layer,
wherein a thickness of the hard oxide layer is in a range of 40 μm to 100 μm,
wherein the applying the sol-gel layer comprises a sol-gel deposition substep and a sol-gel baking substep,
wherein the sol-gel baking substep is performed at a temperature in a range of 100° C. to 200° C. for a duration in a range of 40 minutes to 60 minutes so as to present a solidified sol-gel layer,
wherein the hard oxide layer does not overlap the first oxide layer and the solidified sol-gel layer,
wherein outside of the zone of the substrate, the first oxide layer presents a thickness in a range of 2 μm to 12 μm surmounted by the solidified sol-gel layer presenting a thickness in a range of 1 μm to 10 μm, the pores of the first oxide layer being filled in with the sol-gel,
wherein the applying the sol-gel takes place on the first oxide layer without a prior step of filling in the first oxide layer, and
wherein at least a portion of the sol-gel comprises glycidoxypropyltrimethoxysilane.
2. The method according to claim 1 , wherein the second oxide layer is formed by hard anodic oxidation (HAO).
3. The method according to claim 1 , wherein the first oxide layer is formed by sulfuric anodic oxidation (SAO), tartro-sulfuric anodic oxidation, or phosphoric anodic oxidation.
4. The method according to claim 1 , wherein the hard oxide layer is a hard alumina layer.