IP Library Granted Patent US 10,220,409
Granted Patent B2
US 10,220,409 · App. 15/107,927 · Granted Mar 5, 2019

Methods and systems for increasing surface smoothness of three-dimensional printed article

Inventor: Seth Adrian Miller (Englewood, CO)
Assignee: EMPIRE TECHNOLOGY DEVELOPMENT LLC
B05D1/18B05C3/05B05C9/12B05C9/14B05D1/38B05D3/007B05D3/0254B05D5/00B05D7/00B05D7/02B05D7/542B08B3/12B29C64/35B29C71/0009B33Y40/00C08J7/042B05D1/36B05D7/52B05D7/56B29C2071/0018C08J2425/06C08J2433/10C08J2439/02C08J2475/04C08J2479/02C08J2479/04
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Quick Facts
Patent No.
US 10,220,409
App. No.
15/107,927
Granted
Mar 5, 2019
Kind
B2
Abstract

Technologies are generally described to increase a surface smoothness of a 3D printed article implementing a water-based treatment using layer by layer (LBL) deposition. An initial 3D printed article having an anionic surface may be treated with a first aqueous solution comprising at least one polycation that may bind to the anionic surface to produce a first treated surface, which may be rinsed with water to remove the first aqueous solution. The first treated surface may be treated with a second aqueous solution comprising at least one anionic microparticle that may bind to the polycation to produce a final 3D printed article having a second treated surface, which may be rinsed with water to remove the second aqueous solution. The bound polycation and anionic microparticle may be present as a single layer in the final 3D printed article that may act as a conformal coating to increase the surface smoothness.

Claims (17)

1. A method to treat a surface of an initial three-dimensional (3D) printed article, the method comprising:

providing the initial 3D printed article that has an anionic surface;

treating the anionic surface with a first aqueous solution for a time period based on a first concentration of the first aqueous solution, wherein the first aqueous solution includes at least one polycation to produce a first treated surface; and

treating the first treated surface with a second aqueous solution for another time period based on a second concentration of the second aqueous solution, wherein the second aqueous solution includes at least one anionic microparticle to produce a final 3D printed article that has a second treated surface;

wherein:

the polycation binds to the anionic surface; and

the anionic microparticle binds to the polycation.

2. The method of claim 1 , wherein the polycation is present in the final 3D printed article as a single layer that has thickness such that a smoothness of the surface of the final 3D printed article is higher than a smoothness of the surface of the initial 3D article.

3. The method of claim 1 , further comprising:

heating the final 3D printed article to a temperature above a glass transition temperature (T g ) of the anionic microparticle.

4. The method of claim 3 , wherein the surface of the final 3D printed article has a higher smoothness after the heating step than immediately before the heating step.

5. The method of claim 1 , further comprising:

adding at least one titania particle, at least one polyionic dye, or both to the second aqueous solution prior to the second treatment step.

6. The method of claim 5 , wherein the polyionic dye is a porphyrin dye or a phthalocyanine dye.

7. The method of claim 1 , further comprising:

adding at least one silica particle to the second aqueous solution prior to the second treatment step.

8. The method of claim 7 , wherein the final 3D printed article has a scratch resistance that is higher than a substantially identical final 3D printed article made without an addition of the at least one silica particle.

Assignments (4)
RELEASE OF SECURITY INTEREST IN PATENTS, RECORDED ON JANUARY 29, 2019 AT REEL 048373 FRAME 0217 Recorded Sep 22, 2025
From: CRESTLINE DIRECT FINANCE, L.P., AS COLLATERAL AGENT
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 072936/0464 →
SECURITY INTEREST Recorded Jan 29, 2019
From: EMPIRE TECHNOLOGY DEVELOPMENT LLC
To: CRESTLINE DIRECT FINANCE, L.P.
Reel/Frame 048373/0217 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 24, 2016
From: MILLER, SETH ADRIAN
To: ARDENT RESEARCH CORPORATION
Reel/Frame 039001/0058 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 24, 2016
From: ARDENT RESEARCH CORPORATION
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 039001/0072 →
Continuity (1)
Related Publication 20170028432A1 · Feb 2, 2017