IP Library Granted Patent US 10,464,855
Granted Patent B2
US 10,464,855 · App. 15/110,239 · Granted Nov 5, 2019

Process for preparing a urea-sulphur fertilizer

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Quick Facts
Patent No.
US 10,464,855
App. No.
15/110,239
Granted
Nov 5, 2019
Kind
B2
Abstract

A process for preparing a urea-sulphur fertiliser is disclosed. Urea and sulphur are supplied to a dispersion mill wherein a rotor turns within a slotted stator, thereby providing a dispersion of molten urea and molten sulphur; and the dispersion of molten urea and molten sulphur is supplied to a forming unit to provide the urea-sulphur fertiliser.

Claims (14)

1. A process for preparing a urea-sulphur fertilizer comprising steps of:

(a) supplying urea and sulphur to a dispersion mill wherein a rotor turns within a slotted stator, thereby providing a homogenous dispersion of molten urea in molten sulphur, where the molten sulphur is the main constituent of the homogenous dispersion; and

(b) supplying the dispersion of molten urea in molten sulphur to a forming unit to provide the urea-sulphur fertiliser;

wherein the dispersion mill simultaneously melts and mixes the urea and sulphur to provide the homogenous dispersion of molten urea in molten sulphur; and

wherein at least 5 wt % of the total urea supplied to the dispersion mill is solid urea prills.

2. A process according to claim 1 , wherein solid sulphur is supplied to the dispersion mill.

3. A process according to claim 2 , wherein all of the sulphur supplied to the dispersion mill is solid sulphur.

4. A process according to claim 1 , wherein at least 10 wt % of the total urea supplied to the dispersion mill is solid urea.

5. A process according to claim 4 , wherein all of the urea is supplied to the dispersion mill as solid urea, and all of the sulphur supplied to the dispersion mill is molten sulphur.

6. A process according to claim 1 , wherein solid urea-sulphur is supplied to the dispersion mill.

7. A process according to claim 6 , wherein molten urea and molten sulphur are supplied to the dispersion mill.

8. A process according to claim 1 , wherein oversized granules and/or fines of urea, sulphur or urea-sulphur are supplied to the dispersion mill.

9. A process according to claim 1 , wherein one or more surfactants is added during step (a).

10. A process according to claim 9 , wherein a lignosulphonate is added during step (a).

Assignments (2)
CHANGE OF NAME Recorded Mar 7, 2022
From: SHELL OIL COMPANY
To: SHELL USA, INC.
Reel/Frame 059694/0819 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 23, 2016
From: ALLAIS, CYRILLE PAUL; GARCIA MARTINEZ, RAFAEL ALBERTO
To: SHELL OIL COMPANY
Reel/Frame 039504/0747 →