IP Library Granted Patent US 10,485,811
Granted Patent B2
US 10,485,811 · App. 15/113,986 · Granted Nov 26, 2019

Orally available compounds, a process for preparing the same and their uses as anti-adhesive drugs for treating

Inventors: Julie Bouckaert (Kortrijk, BE); Sebastien Gouin (Thouare sur Loire, FR); Adeline Sivignon (Gerzat, FR); Arlette Darfeuille-Michaud (La Roche-Blanche, FR); Rostyslav Bilyy (Lviv, UA); Dimitri Alvarez-Dorta (Nantes, FR); Nao Yamakawa (Haubourdin, FR); Tetiana Dumych (Volyn Oblast, UA)
Assignees: CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; UNIVERSITE D'AUVERGNE; UNIVERSITE DES SCIENCES ET TECHNOLOGIES DE LILLE 1; UNIVERSITE DE NANTES; INSERM (INSTITUT NATIONAL DE LA SANTE ET DE LA RECHERCHE MEDICALE)
A61K31/70A61K9/0053A61K31/7004A61K31/706A61K31/7028A61K31/7056A61K31/7064A61K31/724A61K45/06A61K47/549C07D309/10C07D309/14C07D405/12C07D405/14C07H7/02C07H15/00C07H15/04C07H15/14C07H15/26C08B37/0012C08B37/0015C08L5/16
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Quick Facts
Patent No.
US 10,485,811
App. No.
15/113,986
Granted
Nov 26, 2019
Kind
B2
Abstract

Orally available compounds, a process for preparing the same and their uses as anti-adhesive drugs for treating E. coli induced inflammatory bowel diseases such as crohn's disease.

Claims (127)

1. A pharmaceutical composition comprising, in combination with a pharmaceutically acceptable vehicle:

(i) at least one compound of the following formula (I-0):

wherein:

X represents NH, O, S or CH 2 ;

n represents an integer comprised from 3 to 7;

Y represents a group selected from:

Z representing O, S or NH;

R representing a moiety selected from the group consisting of:

H

a linear or branched (C 1 -C 7 )-alkyl,

a group of formula —(CH 2 ) i —X′—(CH 2 ) j —H, wherein X′ represents O, S or NH, i is an integer from 1 to 7, and j is an integer from 0 to 7,

a linear or branched (C 2 -C 7 )-alkenyl,

a linear or branched (C 2 -C 7 )-alkynyl,

a (C 3 -C 7 )-cycloalkyl,

a (C 5 -C 7 )-cycloalkenyl,

a (C 3 -C 7 )-heterocycloalkyl,

a (C 5 -C 7 )-heterocycloalkenyl,

an aryl, said aryl being an aromatic or heteroaromatic group,

an alkyl aryl, wherein the aryl is an aromatic or heteroaromatic group,

a CO—(C 1 -C 7 )-alkyl,

a CO-aryl, wherein aryl is an aromatic or heteroaromatic group,

a CO 2 H,

a CO 2 —(C 1 -C 7 )-alkyl,

a CONH—(C 1 -C 7 )-alkyl,

CF 3 ,

adamantyl,

CHRa—NH 2 , wherein Ra represents the side chain of a proteinogenic amino acid, and

a cyclodextrin,

said (C 1 -C 7 )-alkyl, group of formula —(CH 2 ) i —X′—(CH 2 ) j —H, (C 2 -C 7 )-alkenyl, (C 2 -C 7 )-alkynyl, (C 3 -C 7 )-cycloalkyl, (C 5 -C 7 )-cycloalkenyl, C 3 -C 7 )-heterocycloalkyl, (C 5 -C 7 )-heterocycloalkenyl, CO—(C 1 -C 7 )-alkyl, CO 2 —(C 1 -C 7 )-alkyl, CONH—(C 1 -C 7 )-alkyl, aryl, alkyl aryl, CO-aryl and cyclodextrin being optionally substituted by one or more substituent(s), each independently selected from the group consisting of:

a linear or branched (C 1 -C 7 )-alkyl,

a linear or branched (C 2 -C 7 )-alkenyl,

a linear or branched (C 2 -C 7 )-alkynyl,

a (C 3 -C 7 )-cycloalkyl,

a (C 5 -C 7 )-cycloalkenyl,

a (C 3 -C 7 )-heterocycloalkyl,

a (C 5 -C 7 )-heterocycloalkenyl,

an aryl, wherein the aryl is an aromatic or heteroaromatic group

an alkyl aryl, wherein the aryl is an aromatic or heteroaromatic group,

a CHO,

a CO—(C 1 -C 7 )-alkyl,

a CO-aryl, wherein aryl is an aromatic or heteroaromatic group,

a CO 2 H,

a CO 2 —(C 1 -C 7 )-alkyl,

a CONH—(C 1 -C 7 )-alkyl,

a halogen selected from the group consisting of F, Cl, Br, and I,

CF 3 ,

OR a , wherein R a represents:

H, a linear or branched (C 1 -C 7 )-alkyl, a (C 3 -C 7 )-cycloalkyl, CO—(C 1 -C 7 )-alkyl, or CO-aryl, wherein aryl is an aromatic or heteroaromatic group,

NR b R c , wherein R b and R c represent independently from each other:

H, a linear or branched (C 1 -C 7 )-alkyl, a (C 3 -C 7 )-cycloalkyl, CO—(C 1 -C 7 )-alkyl, or CO-aryl, wherein aryl is an aromatic or heteroaromatic group,

NO 2 ,

CN,

SO 3 H or a salt thereof; and

pharmaceutically acceptable salts thereof,

provided that when R represents CHRa—NH 2 , then Y can only represent the following group (a):

with the proviso that said compound is not of the following structure:

and salts thereof; and

(ii) at least one compound selected from the group consisting of antibiotics, anti-inflammatory compounds, glucocorticoids, immunosuppressive compounds and anti-TNF-alpha therapies,

said pharmaceutical composition being used for simultaneous or separate use or use spread over time intended for the treatment of inflammatory bowel disease.

2. The pharmaceutical composition according to claim 1 , wherein said at least one compound of the formula (I-0) is of the following formula (I-1):

wherein:

X represents NH, O, S or CH 2 ;

n represents an integer comprised from 3 to 7;

Y represents a group selected from the group consisting of:

Z representing O, S or NH;

R 1 representing:

H

a linear or branched (C 1 -C 7 )-alkyl,

a linear or branched (C 2 -C 7 )-alkenyl,

a linear or branched (C 2 -C 7 )-alkynyl,

a (C 3 -C 7 )-cycloalkyl,

a (C 5 -C 7 )-cycloalkenyl,

a (C 3 -C 7 )-heterocycloalkyl,

a (C 5 -C 7 )-heterocycloalkenyl,

an aryl, said aryl being an aromatic or heteroaromatic group,

an alkyl aryl, wherein the aryl is an aromatic or heteroaromatic group,

a CO—(C 1 -C 7 )-alkyl,

a CO-aryl, wherein aryl is an aromatic or heteroaromatic group,

a CO 2 H,

a CO 2 —(C 1 -C 7 )-alkyl,

a CONH—(C 1 -C 7 )-alkyl,

CF 3 ,

adamantyl,

CHRa—NH 2 , wherein Ra represents the side chain of a proteinogenic amino acid,

said (C 1 -C 7 )-alkyl, (C 2 -C 7 )-alkenyl, (C 2 -C 7 )-alkynyl, (C 3 -C 7 )-cycloalkyl, (C 5 -C 7 )-cycloalkenyl, (C 3 -C 7 )-heterocycloalkyl, (C 5 -C 7 )-heterocycloalkenyl, CO—(C 1 -C 7 )-alkyl, CO 2 —(C 1 -C 7 )-alkyl, CONH—(C 1 -C 7 )-alkyl, aryl, alkyl aryl and CO-aryl being optionally substituted by one or more substituent(s), each independently selected from the group consisting of:

a linear or branched (C 1 -C 7 )-alkyl, a linear or branched (C 2 -C 7 )-alkenyl,

a linear or branched (C 2 -C 7 )-alkynyl,

a (C 3 -C 7 )-cycloalkyl,

a (C 5 -C 7 )-cycloalkenyl,

a (C 3 -C 7 )-heterocycloalkyl,

a (C 5 -C 7 )-heterocycloalkenyl,

an aryl, wherein the aryl is an aromatic or heteroaromatic group,

an alkyl aryl, wherein the aryl is an aromatic or heteroaromatic group,

a CHO,

a CO—(C 1 -C 7 )-alkyl,

a CO-aryl, wherein aryl is an aromatic or heteroaromatic group,

a CO 2 H,

a CO 2 —(C 1 -C 7 )-alkyl,

a CONH—(C 1 -C 7 )-alkyl,

a halogen selected from the group consisting of F, Cl, Br, and I,

CF 3 ,

OR a , wherein R a represents:

H, a linear or branched (C 1 -C 7 )-alkyl, a (C 3 -C 7 )-cycloalkyl, CO—(C 1 -C 7 )-alkyl, or CO-aryl, wherein aryl is an aromatic or heteroaromatic group,

NR b R c , wherein R b and R c represent independently from each other:

H, a linear or branched (C 1 -C 7 )-alkyl, a (C 3 -C 7 )-cycloalkyl, CO—(C 1 -C 7 )-alkyl, or CO-aryl, wherein aryl is an aromatic or heteroaromatic group,

NO 2 ,

CN; and

pharmaceutically acceptable salts thereof,

provided that when R 1 represents CHRa—NH 2 , then Y can only represent the following group (a):

3. The pharmaceutical composition according to claim 2 , wherein:

Y represents

said at least one compound of the formula (I-0) being of following formula (I-1a):

X, n and R 1 being as previously defined;

or

Y represents

said at least one compound of the formula (I-0) being of following formula (I-1b):

X, n and R 1 being as previously defined;

or

Y represents

said at least one compound of the formula (I-0) being of following formula (I-1c):

X, n, Z and R 1 being as previously defined.

4. A compound selected from the group consisting of:

and salts thereof.

5. A pharmaceutical composition comprising, in combination with a pharmaceutically acceptable vehicle:

at least one compound according to claim 4 , and

at least one compound selected from the group consisting of antibiotics, anti-inflammatory compounds, glucocorticoids, immunosuppressive compounds and anti-TNF-alpha therapies,

said pharmaceutical composition being used for simultaneous or separate use or use spread over time intended for the treatment of inflammatory bowel disease.

Assignments (2)
MERGER Recorded Sep 7, 2023
From: UNIVERSITE DE NANTES
To: NANTES UNIVERSITE
Reel/Frame 064824/0596 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 17, 2018
From: BOUCKAERT, JULIE; GOUIN, SEBASTIEN; SIVIGNON, ADELINE; MICHAUD (LEGAL REPRESENTATIVE OF ARLETTE DARFEUILLE-MICHAUD - DECEASED), JEAN-ERIC; BILYY, ROSTYSLAV; ALVAREZ-DORTA, DIMITRI; YAMAKAWA, NAO; DUMYCH, TETIANA
To: CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; UNIVERSITE D'AUVERGNE; UNIVERSITE DES SCIENCES ET TECHNOLOGIES DE LILLE 1; UNIVERSITE DE NANTES; INSERM INSTITUT NATIONAL DE LA SANTE ET DE LA RECHERCHE MEDICALE
Reel/Frame 044644/0169 →
Priority Claims (1)
EP 14305107 · Jan 24, 2014 · regional
Continuity (1)
Related Publication 20160340445A1 · Nov 24, 2016