IP Library Granted Patent US 10,400,367
Granted Patent B2
US 10,400,367 · App. 15/120,969 · Granted Sep 3, 2019

Part made from oxide/oxide composite material for 3-D reinforcing and method for manufacture of same

Inventors: Pascal Diss (Le Haillan, FR); Eric Bouillon (Le Haillan, FR); Eric Lavasserie (Begles, FR)
Assignee: SAFRAN CERAMICS
D03D25/005B28B7/46B28B13/021B28B23/0006C04B35/6224C04B35/62236C04B35/62245C04B35/64C04B35/803D03D11/00C04B2235/3217C04B2235/3418C04B2235/3463C04B2235/447C04B2235/522C04B2235/5224C04B2235/5228C04B2235/5232C04B2235/5252C04B2235/616C04B2235/77C04B2235/96D10B2505/02
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Quick Facts
Patent No.
US 10,400,367
App. No.
15/120,969
Granted
Sep 3, 2019
Kind
B2
Abstract

A part made of oxide/oxide composite material includes fiber reinforcement constituted by a plurality of warp yarn layers and of weft yarn layers interlinked by three-dimensional weaving, with the spaces present between the reinforcing yarns being filled with a refractory oxide matrix. The fiber reinforcement presents a weave selected from the following weaves: interlock; multi-plain; multi-satin; and multi-serge, with warp and weft thread counts lying in the range 4 yarns/cm to 20 yarns/cm. The fiber reinforcement also presents a fiber volume fraction lying in the range 40% to 51%.

Claims (22)

1. A part made of oxide/oxide composite material comprising fiber reinforcement constituted by a plurality of warp yarn layers and of weft yarn layers interlinked by three-dimensional weaving, with the spaces present between the reinforcing yarns being filled with a refractory oxide matrix;

wherein the fiber reinforcement presents a weave selected from the following weaves: interlock; multi-plain; multi-satin; and multi-serge; and warp and weft thread counts lying in the range 4 yarns/cm to 20 yarns/cm, and wherein the fiber reinforcement presents a fiber volume fraction lying in the range 40% to 51%, and wherein spaces present between the yarns of the fiber reinforcement are of dimensions that are less than five times a maximum section of the yarns of the fiber reinforcement.

2. A part according to claim 1 , wherein the part presents, in monotonic traction, at ambient temperature, and in the warp direction:

a modulus of elasticity lying in the range 120 GPa to 170 GPa;

a breaking deformation of not less than 0.35%; and

a breaking stress greater than 250 MPa.

3. A part according to claim 1 , wherein the yarns of the fiber reinforcement are made of fibers constituted by one or more of the following materials: alumina;

mullite; silica; an aluminosilicate; and a borosilicate.

4. A part according to claim 1 , wherein the material of the matrix is selected from: alumina; mullite; silica; an aluminosilicate; and an aluminophosphate.

5. A method of fabricating an oxide/oxide composite material part, the method comprising the following steps:

forming a fiber texture by three-dimensional weaving of refractory oxide yarns;

compacting said fiber texture;

placing on one side of the fiber texture a slip containing a submicrometer powder of refractory oxide particles;

establishing a pressure difference to force the slip to pass through the fiber texture;

filtering a liquid of the slip that has passed through the fiber texture so as to retain the powder of refractory oxide particles inside said texture and to form a filled preform;

drying the filled preform; and

sintering the submicrometer powder of refractory oxide particles in order to form a refractory oxide matrix in the preform;

wherein during the step of forming the fiber texture the yarns are woven with a weave selected from the following weaves: interlock; multi-plain; multi-satin; and multi-serge; with warp and weft thread counts lying in the range 4 yarns/cm to 20 yarns/cm, and in that, after the compacting step, said fiber reinforcement presents a fiber volume fraction lying in the range 40% to 51%, such that spaces present between the yarns of the fiber reinforcement are of dimensions that are less than five times a maximum section of the yarns of the fiber reinforcement.

6. A method according to claim 5 , wherein the yarns of the preform are made of fibers constituted by one or more of the following materials: alumina; mullite; silica; an aluminosilicate; and a borosilicate.

7. A method according to claim 5 , wherein the submicrometer particles are made of a material selected from: alumina; mullite; silica; an aluminosilicate; and an aluminophosphate.

8. A method according to claim 5 , wherein the yarns of the fiber reinforcement comprise continuous fibers.

9. A part according to claim 1 , wherein the yarns of the fiber reinforcement comprise continous fibers.

Assignments (2)
CHANGE OF NAME Recorded Apr 22, 2018
From: HERAKLES
To: SAFRAN CERAMICS
Reel/Frame 046678/0455 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2017
From: DISS, PASCAL; BOUILLON, ERIC; LAVASSERIE, ERIC
To: HERAKLES
Reel/Frame 042429/0889 →
Cited By (1)
US 12,195,403