IP Library Granted Patent US 10,066,168
Granted Patent B2
US 10,066,168 · App. 15/157,020 · Granted Sep 4, 2018

Process for liquefying a cellulosic material and its products

Inventors: Klaas Lambertus Von Hebel (Amsterdam, NL); Jean Paul Andre Marie Joseph Ghislain Lange (Amsterdam, NL)
Assignee: SHELL OIL COMPANY
C10G1/002C08H8/00C10G1/065C10G3/50C10L1/02C10L1/04C10G2300/1014C10G2300/208C10G2300/44C10G2400/02C10G2400/04C10G2400/08C10L2200/0469C10L2290/544Y02E50/13Y02P30/20
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Quick Facts
Patent No.
US 10,066,168
App. No.
15/157,020
Granted
Sep 4, 2018
Kind
B2
Abstract

A process for liquefying a cellulosic material to produce a liquefied product from cellulosic material is provided. Products obtained from such process and use of such products to prepare biofuels is also provided.

Claims (15)

1. A product comprising:

(a) from 20 to 80 wt % of a monomeric fraction containing one or more monomeric compounds having a molecular weight (Mw) of less than or equal to 250 Dalton (Da);

(b) from 20 to 80 wt % of an oligomeric fraction containing one or more oligomeric compounds having a molecular weight (Mw) of more than 250 Dalton (Da);

(c) from 0 wt % to 25 wt % of tar;

wherein the percentage of saturated carbon atoms in the oligomeric fraction is more than or equal to 35%, based on the total amount of carbon atoms present;

wherein the one or more oligomeric compounds are liquid at ambient temperature (20° C.) and pressure (1 bar absolute);

wherein the percentage of saturated carbon atoms in the oligomeric compound fraction that is liquid at ambient temperature (20° C.) and pressure (1 bar absolute) is more than or equal to 50%, based on the total amount of carbon atoms; and

wherein the weight ratio of the monomeric compound(s) to the oligomeric compound(s) lies in the range from 4:1 to 1:4.

2. The product of claim 1 , wherein the one or more monomeric compounds is selected from a group consisting of substituted tetrahydrofurane, substituted tetrahydropyran, substituted guaiacol, substituted syringol, and any combination thereof in an amount of more than or equal to 20 wt %, based on the total weight of monomeric compounds.

3. The product of claim 1 , wherein the tar has a molecular weight (Mw) from more than 2000 Dalton (Da) up to and including 30000 Dalton (Da).

4. The product of claim 1 comprising from 25 wt % to 75 wt % of one or more monomeric compounds having a molecular weight (Mw) of less than or equal to 250 Dalton (Da).

5. The product of claim 1 comprising from 25 wt % to 75 wt % of one or more oligomeric compounds having a molecular weight (Mw) of more than or equal to 250 Dalton (Da).

6. The product of claim 1 wherein more than or equal to 40wt % of the oligomeric compounds is liquid at ambient temperature (20° C.) and pressure (1 bar absolute), based on the total weight of oligomeric compounds.

7. The product of claim 1 wherein the percentage of saturated carbon atoms in the oligomeric fraction is more than or equal to 60%, based on the total amount of carbon atoms present.

8. The product of claim 1 wherein the percentage of saturated carbon atoms in the oligomeric fraction is more than or equal to 70%, based on the total amount of carbon atoms present.

Assignments (1)
CHANGE OF NAME Recorded Mar 7, 2022
From: SHELL OIL COMPANY
To: SHELL USA, INC.
Reel/Frame 059694/0819 →
Priority Claims (1)
EP 10162722 · May 12, 2010 · regional
Continuity (2)
Division 13106553 · May 12, 2011
Related Publication 20160326441A1 · Nov 10, 2016