IP Library Granted Patent US 9,956,297
Granted Patent B2
US 9,956,297 · App. 15/167,109 · Granted May 1, 2018

FAP-activated proteasome inhibitors for treating solid tumors

Inventors: William W. Bachovchin (Cambridge, MA); Hung-sen Lai (Andover, MA); Sarah E. Poplawski (Belmont, MA)
Assignee: Trustees of Tufts College
A61K47/48361A61K31/69A61K38/07A61K45/06A61K47/54C07K5/06026C07K5/06034C07K5/06078C07K5/081C07K5/0806C07K5/0808C07K5/0812C07K5/0821C07K5/1016G01N33/574A61K38/00
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Quick Facts
Patent No.
US 9,956,297
App. No.
15/167,109
Granted
May 1, 2018
Kind
B2
Abstract

Disclosed are proteasome inhibitors, fibroblast activation protein (FAP)-activated prodrugs of proteasome inhibitors, and pharmaceutically acceptable salts of the inhibitors and prodrugs. Also disclosed are related pharmaceutical compositions, and methods of using the inhibitors and prodrugs and compositions thereof, for example, in treating cancer or other cell proliferative diseases. In vitro and in vivo methods of quantifying the expression of FAP in a biopsy sample and a mammal, respectively, are also disclosed.

Claims (30)

1. A method of treating cancer, psoriasis, restenosis, or other cell proliferative disease, comprising administering to a mammal in need thereof a therapeutically effective amount of a fibroblast activation protein (FAP)-activated proteasome inhibitor represented by formula III:

wherein

R 1 —(C═O)— represents an acyl N-terminal blocking group;

R 2 represents H, lower alkyl, or a mono- or di-hydroxy-substituted lower alkyl;

R 3 represents lower alkyl;

R 4 is absent

R 5 represents a hydrophobic amino acid sidechain;

R 6 represents alkyl, cycloalkyl, aryl, heterocycle or —(CH 2 ) n —R 7 ;

R 7 represents aryl, aralkyl, cycloalkyl, alkoxy, alkylthio, —OH or —SH;

R 11 represents H or lower alkyl;

W represents

Y 1 and Y 2 are independently OH, or a group capable of being hydrolyzed to a hydroxyl group; or Y 1 and Y 2 taken together with the B to which they are attached form a ring having from 5 to 8 atoms in the ring structure; and

n is an integer in the range of 1 to 8.

2. The method of claim 1 , wherein the FAP-activated proteasome inhibitor is represented by

3. The method of claim 1 , wherein the method is a method of treating cancer.

4. The method of claim 3 , wherein the cancer is a solid tumor.

5. The method of claim 4 , wherein the solid tumor is prostate, pancreatic, or breast cancer.

6. The method of claim 3 , wherein the cancer is pancreatic cancer.

7. The method of claim 3 , wherein the cancer is multiple myeloma.

8. The method of claim 1 , wherein Y 1 is OH; and Y 2 is OH.

9. The method of claim 2 , wherein the method is a method of treating cancer.

10. The method of claim 8 , wherein the method is a method of treating cancer.

11. The method of claim 9 , wherein the cancer is a solid tumor.

12. The method of claim 11 , wherein the solid tumor is prostate, pancreatic, or breast cancer.

13. The method of claim 12 , wherein the cancer is pancreatic cancer.

14. The method of claim 9 , wherein the cancer is multiple myeloma.

15. The method of claim 10 , wherein the cancer is a solid tumor.

16. The method of claim 15 , wherein the solid tumor is prostate, pancreatic, or breast cancer.

17. The method of claim 16 , wherein the cancer is pancreatic cancer.

18. The method of claim 10 , wherein the cancer is multiple myeloma.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jan 4, 2017
From: TUFTS UNIVERSITY BOSTON
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 041239/0689 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 3, 2016
From: BACHOVCHIN, WILLIAM W.; LAI, HUNG-SEN; POPLAWSKI, SARAH E.
To: TRUSTEES OF TUFTS COLLEGE
Reel/Frame 038801/0363 →
Continuity (3)
Continuation 14241666
Provisional Application 61528824 · Aug 30, 2011
Related Publication 20160346401A1 · Dec 1, 2016