IP Library Granted Patent US 10,131,930
Granted Patent B2
US 10,131,930 · App. 15/185,792 · Granted Nov 20, 2018

Filtration methods and devices

Inventors: Patrick A. Mach (Shorewood, MN); Raj Rajagopal (Woodbury, MN); Wensheng Xia (Woodbury, MN); Jinsheng Zhou (Woodbury, MN); Chunmei Guo (Woodbury, MN)
Assignee: 3M Innovative Properties Company
C12Q1/04B01D63/00B01D69/02B01D69/10B01J20/267B01J20/2805B01J20/28047C12Q1/24C12Q1/689G01N33/68B01D2323/39B01D2325/022B01D2325/12
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Quick Facts
Patent No.
US 10,131,930
App. No.
15/185,792
Granted
Nov 20, 2018
Kind
B2
Abstract

A method of filtering a liquid sample that includes passing a sample comprising at least one biological organism through a filter membrane at a passive water volume flux of at least 10 L/m 2 ·h·psi, wherein the filter membrane comprises a Bubble Point pore size of no more than 1.0 μm, thereby retaining at least one biological organism on the surface of the membrane; and detecting the at least one biological organism retained on the surface of the filter membrane.

Claims (30)

1. A system comprising:

a liquid sample comprising at least one biological organism;

a filter device comprising:

a pocket comprising a pocket surface that defines a pocket volume;

an absorbent member disposed on at least a portion of the pocket surface, wherein the absorbent member is a hydrogel; and

a filter membrane disposed on at least a portion of the absorbent member in fluid communication with the pocket volume, wherein flow of liquid into the absorbent member occurs when a liquid flows through the filter membrane and a biological organism in the liquid sample is retained by the filter membrane, wherein the filter membrane forms the pocket.

2. The system of claim 1 , wherein the filter membrane is a multi-zone membrane.

3. The system of claim 2 , wherein the multi-zone membrane comprises an open side in functional communication with the absorbent member and a tight side in fluid communication with the pocket volume.

4. The system of claim 3 , wherein the tight side has a smaller Bubble Point pore size relative to the open side.

5. The system of claim 3 , wherein the functional communication is capable of generating a water flux gradient sufficient to draw liquid across the filter membrane and into the absorbent member.

6. The system of claim 1 , wherein the pocket further comprises a sample port.

7. The system of claim 5 , wherein the water flux gradient is at least 10 L/m2.h.psi.

8. The system of claim 1 , wherein the filter membrane has a Bubble Point pore size of no more than 1.0 μm.

9. The system of claim 1 , wherein the filter membrane comprises a polyolefin porous membrane, an ethylene-chlorotrifluoroethylene copolymer porous membrane, a polyacrylonitrile porous membrane, a polycarbonate porous membrane, a polyester porous membrane, a cellulose ester porous membrane, a polyamide porous membrane, a polyethersulfone porous membrane, a polysulfone porous membrane, a polyvinylidene fluoride (PVDF) porous membrane, a polyacrylonitrile nanofiber membrane, a PVDF nanofiber membrane, a cellulose ester nanofiber membrane, a polyvinyl acetate or alcohol nanofiber membrane, or a polyvinyl butyral nanofiber membrane.

10. The system of claim 1 , wherein the filter membrane comprises a Thermally Induced Phase (TIPS) membrane or a nanofiber membrane.

11. A system comprising:

a liquid sample comprising at least one biological organism;

a filter device comprising:

a pocket comprising a pocket surface that defines a pocket volume;

an absorbent member disposed on at least a portion of the pocket surface, wherein the absorbent member is a hydrogel; and

a filter membrane disposed on at least a portion of the absorbent member in fluid communication with the pocket volume, wherein flow of liquid into the absorbent member occurs when a liquid flows through the filter membrane and a biological organism in the liquid sample is retained by the filter membrane, wherein the absorbent member is enveloped by the filter membrane.

12. The system of claim 11 , wherein the filter membrane is a multi-zone membrane.

13. The system of claim 12 , wherein the multi-zone membrane comprises an open side in functional communication with the absorbent member and a tight side in fluid communication with the pocket volume.

14. The system of claim 13 , wherein the tight side has a smaller Bubble Point pore size relative to the open side.

15. The system of claim 13 , wherein the functional communication is capable of generating a water flux gradient sufficient to draw liquid across the filter membrane and into the absorbent member.

16. The system of claim 15 , wherein the water flux gradient is at least 10 L/m2.h.psi.

17. The system of claim 11 , wherein the pocket further comprises a sample port.

18. The system of claim 11 , wherein the filter membrane has a Bubble Point pore size of no more than 1.0 μm.

19. The system of claim 11 , wherein the filter membrane comprises a polyolefin porous membrane, an ethylene-chlorotrifluoroethylene copolymer porous membrane, a polyacrylonitrile porous membrane, a polycarbonate porous membrane, a polyester porous membrane, a cellulose ester porous membrane, a polyamide porous membrane, a polyethersulfone porous membrane, a polysulfone porous membrane, a polyvinylidene fluoride (PVDF) porous membrane, a polyacrylonitrile nanofiber membrane, a PVDF nanofiber membrane, a cellulose ester nanofiber membrane, a polyvinyl acetate or alcohol nanofiber membrane, or a polyvinyl butyral nanofiber membrane.

20. The system of claim 11 , wherein the filter membrane comprises a Thermally Induced Phase (TIPS) membrane or a nanofiber membrane.

Assignments (3)
SECURITY INTEREST Recorded Sep 2, 2022
From: NEOGEN CORPORATION; NEOGEN FOOD SAFETY US HOLDCO CORPORATION
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 061372/0264 →
PATENT ASSIGNMENT AGREEMENT Recorded Sep 1, 2022
From: 3M INNOVATIVE PROPERTIES COMPANY
To: GARDEN US HOLDCO CORPORATION
Reel/Frame 061365/0688 →
CHANGE OF NAME Recorded Sep 1, 2022
From: GARDEN US HOLDCO CORPORATION
To: NEOGEN FOOD SAFETY US HOLDCO CORPORATION
Reel/Frame 061370/0437 →
Continuity (3)
Continuation 13701935
Provisional Application 61352205 · Jun 7, 2010
Related Publication 20160362718A1 · Dec 15, 2016