IP Library Granted Patent US 10,472,443
Granted Patent B2
US 10,472,443 · App. 15/190,381 · Granted Nov 12, 2019

Highly random acrylamide-acrylic acid copolymers

Inventors: Stephen Marrou (Mount Prospect, IL); Xiangyang Zhu (Denver, CO); Heqing Huang (Naperville, IL)
Assignee: Ecolab USA Inc.
C08F220/56C08F2/32
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Quick Facts
Patent No.
US 10,472,443
App. No.
15/190,381
Granted
Nov 12, 2019
Kind
B2
Abstract

Highly random acrylamide-acrylic acid copolymers are described. Ionic crosslinking of the highly random copolymers in dilute solution results in improved viscosity and gel strength compared to copolymers prepared by conventional methods. The ionically crosslinked copolymers are useful in enhanced oil recovery processes.

Claims (9)

1. A crosslinked composition comprising a water source, about 100 ppm to 1500 ppm of a copolymer of acrylamide and acrylic acid, and about 5 ppm to 100 ppm of an ionic crosslinker, wherein the copolymer has about 50 mole % to 80 mole % acrylamide residues and a blockiness index of about 0.90 to 1.1.

2. The composition of claim 1 wherein the copolymer consists essentially of acrylamide and acrylic acid residues.

3. The composition of claim 1 wherein the copolymer comprises more than 50 mole % acrylamide residue.

4. The composition of claim 1 wherein the copolymer comprises about 70 mole % acrylamide residue.

5. The composition of claim 1 wherein the ionic crosslinker comprises a salt of a multivalent cation comprising Ca 2+ , Mg 2+ , Zn 2+ , Cr 2+ , Cr 3+ , Al 3+ , or a combination of two or more thereof.

6. The composition of claim 5 wherein the counterion of the ionic crosslinker is a residue of an organic acid.

7. The composition of claim 6 wherein the organic acid is acetic acid or citric acid.

8. The composition of claim 1 wherein the viscosity of the crosslinked composition is about 2 to 1000 times the viscosity of the corresponding composition without the ionic crosslinker.

9. The composition of claim 1 wherein the blockiness index is about 0.95 to 1.05.

Assignments (8)
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2024
From: CHAMPIONX USA INC.
To: CHAMPIONX LLC
Reel/Frame 067768/0888 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: CHAMPIONX USA INC.
Reel/Frame 060304/0267 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 10, 2020
From: ECOLAB USA INC.
To: CHAMPIONX USA INC.
Reel/Frame 053749/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: CHAMPIONX USA INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 052848/0368 →
SECURITY INTEREST Recorded Jun 5, 2020
From: CHAMPIONX USA INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 053250/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2019
From: MARROU, STEPHEN; ZHU, XIANGYANG; HUANG, HEQING
To: ECOLAB USA INC.
Reel/Frame 048219/0469 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 23, 2016
From: MARROU, STEPHEN; ZHU, XIANGYANG; HUANG, HEQING
To: ECOLAB USA INC.
Reel/Frame 038993/0936 →
Continuity (2)
Provisional Application 62186107 · Jun 29, 2015
Related Publication 20160376389A1 · Dec 29, 2016