IP Library Granted Patent US 10,422,802
Granted Patent B2
US 10,422,802 · App. 15/217,093 · Granted Sep 24, 2019

Devices and methods for detecting amniotic fluid in vaginal secretions

Inventors: Boris Fuks (Billerica, MA); Dmitrii D. Petrunin (Moscow, RU); Evgeny I. Zaraisky (Moscow, RU); Marina N. Boltovskaya (Moscow, RU); Svetlana V. Nazimova (Moscow, RU); Nelly A. Starosvetskaya (Moscow, RU); Alexandr Konstantinov (Nashua, NH); Margarita I. Marshiskaia (Moscow, RU)
Assignee: Qiagen Sciences, LLC
G01N33/6854G01N33/558G01N33/577G01N33/689G01N2333/471G01N2800/36G01N2800/368Y10S435/805Y10S435/81Y10S435/97Y10S436/805Y10S436/807Y10S436/81Y10S436/811Y10S436/815Y10S436/817
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Quick Facts
Patent No.
US 10,422,802
App. No.
15/217,093
Granted
Sep 24, 2019
Kind
B2
Abstract

The present invention relates to a diagnostic method for the detection of small quantities of amniotic fluid in the vagina. More specifically, the invention relates to the detection of PAMG-1 in the vagina using anti-PAMG-1 antibodies.

Claims (19)

1. A method of detecting amniotic fluid in a sample comprising a vaginal secretion of a pregnant woman using a combination of at least two placenta alpha microglobulin-1 (PAMG-1)-specific monoclonal antibodies, wherein said at least two monoclonal antibodies are selected from the group consisting of M271, produced by hybridoma N271, deposited with the Russian National Collection of Industrial Microorganisms (VKPM) Depository and assigned accession number VKPM-93; M52, produced by hybridoma N52, deposited with the VKPM and assigned accession number VKPM-92; and M42, produced by hybridoma N42, deposited with the VKPM and assigned accession number VKPM-94, the method comprising:

(a) contacting the sample with said at least two PAMG-1-specific monoclonal antibodies;

(b) detecting a PAMG-1/antibody complex when the concentration of PAMG-1 in the sample exceeds a predefined detection threshold of 5 nanograms per milliliter; and

(c) determining that said sample contains amniotic fluid if said PAMG-1/antibody complex is detected in step (b).

2. The method of claim 1 , wherein said at least two monoclonal antibodies are M271 and M52.

3. The method of claim 1 , wherein one of said at least two monoclonal antibodies is bound to a marker.

4. The method of claim 3 , wherein the marker is a dye particle or colloidal gold.

5. The method of claim 1 , wherein said predefined threshold amount is in the range of 5 to 50 nanograms per milliliter.

6. The method of claim 1 , wherein said at least two monoclonal antibodies are used in a strip device.

7. The method of claim 6 , wherein said strip device comprises a detector section which is upstream from a capture section, wherein one of said at least two PAMG-1 specific monoclonal antibodies is a mobilizable antibody present in the detector section, and the other of said at least two monoclonal antibodies is immobilized in the capture section.

8. The method of claim 7 , wherein said immobilized antibody has a lower PAMG-1 binding affinity than said mobilizable antibody.

9. The method of claim 7 , wherein the mobilizable antibody in said detector section further comprises a marker; and

wherein mobilization of said mobilizable antibody by a fluid sample introduced to the strip device permits binding of the mobilizable antibody to any PAMG-1 in the sample, and binding of the mobilizable antibody-PAMG-1 complex formed thereby to the immobilized antibody in said capture section.

10. The method of claim 9 , wherein said PAMG-1/antibody complex is detected by detecting the presence of the marker in the capture section of said strip device.

11. The method of claim 10 , wherein said marker is a dye particle or colloidal gold.

12. A method of detecting amniotic fluid in a sample comprising a vaginal secretion of a pregnant woman using a combination of at least two placenta alpha microglobulin-1 (PAMG-1)-specific monoclonal antibodies, wherein said at least two monoclonal antibodies are selected from the group consisting of M271, produced by hybridoma N271, deposited with the Russian National Collection of Industrial Microorganisms (VKPM) Depository and assigned accession number VKPM-93; M52, produced by hybridoma N52, deposited with the VKPM and assigned accession number VKPM-92; and M42, produced by hybridoma N42, deposited with the VKPM and assigned accession number VKPM-94, the method comprising:

(a) contacting the sample with a strip device, said strip device comprising a detector section which is upstream from a capture section, wherein one of said at least two PAMG-1 specific monoclonal antibodies is a mobilizable antibody present in the detector section, and the other of said at least two monoclonal antibodies is immobilized in the capture section, and wherein said immobilized antibody has a lower PAMG-1 binding affinity than said mobilizable antibody;

(b) detecting a PAMG-1/antibody complex when the concentration of PAMG-1 in the sample exceeds a predefined detection threshold of 5 nanograms per milliliter; and

(c) determining that said sample contains amniotic fluid if said PAMG-1/antibody complex is detected in step (b).

Assignments (2)
MERGER Recorded Aug 3, 2018
From: N-DIA, INC.
To: QIAGEN SCIENCES, LLC
Reel/Frame 046705/0948 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 22, 2016
From: FUKS, BORIS; PETRUNIN, DMITRII D.; ZARAISKY, EVGENY I.; BOLTOVSKAYA, MARINA N.; NAZIMOVA, SVETLANA V.; STAROSVETSKAYA, NELLY A.; KONSTANTINOV, ALEXANDR; MARSHISKAIA, MARGARITA I.
To: N-DIA, INC.
Reel/Frame 039564/0022 →
Continuity (5)
Division 13213735 · Aug 19, 2011
Continuation 12722369 · Mar 11, 2010
Continuation 10524668
Provisional Application 60403407 · Aug 13, 2002
Related Publication 20160327565A1 · Nov 10, 2016