IP Library Granted Patent US 10,189,271
Granted Patent B2
US 10,189,271 · App. 15/240,213 · Granted Jan 29, 2019

Non-foaming aqueous particle-free inkjet ink compositions

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,189,271
App. No.
15/240,213
Granted
Jan 29, 2019
Kind
B2
Abstract

Colorless or colored coatings can be ink jetted onto a substrate using an aqueous particle-free inkjet ink composition that has a viscosity of less than 5 centipoises, and that includes a combination of an anionic polyether polyurethane and an anionic acrylic polymer or anionic styrene-acrylic polymer, in a total amount of less than or equal to 20 weight %. The composition can be colorless (free of colorants) or it can contain a suitable colorant to provide a color image. The composition also includes a defoamer that has a hydrophilic-lipophilic balance value of at least 3 and up to and including 5, and which is present in an amount of at least 0.15 weight % and up to and including 1 weight %. Such composition can be used in inkjet printing methods including recirculation apparatus and methods, and can be provided as part of an ink set.

Claims (33)

1. An aqueous colorless particle-free inkjet ink composition that has a viscosity of less than 5 centipoises (0.005 N-sec) at 25° C., and comprises:

an anionic polyether polyurethane having an acid number of at least 50 and an anionic acrylic polymer or anionic styrene-acrylic polymer having an acid number of at least 50; wherein the weight ratio of the anionic polyether polyurethane to the anionic acrylic polymer or anionic styrene-acrylic polymer is from 1:9 to and including 9:1, and the total amount of the anionic polyether polyurethane and the anionic acrylic polymer or anionic styrene-acrylic polymer is less than or equal to 20 weight % based on the total aqueous colorless particle-free inkjet ink composition weight, and

a defoamer that has a hydrophilic-lipophilic balance value of at least 3 and up to and including 5, which defoamer is present in an amount of at least 0.15 weight % and up to and including 1 weight %, based on the total aqueous colorless particle-free inkjet ink composition weight.

2. The aqueous colorless particle-free inkjet ink composition of claim 1 , wherein the defoamer has a hydrophilic-lipophilic balance value of at least 3 and up to and including 4.

3. The aqueous colorless particle-free inkjet ink composition of claim 1 , wherein the defoamer is present in an amount of at least 0.2 weight % and up to and including 0.8 weight %, based on the total aqueous colorless particle-free inkjet ink composition weight.

4. The aqueous colorless particle-free inkjet ink composition of claim 1 , comprising a mixture of at least one anionic acrylic polymer or anionic styrene-acrylic polymer having a molecular weight of at least 2,000 and up to and including 10,000 Daltons, and at least one anionic acrylic polymer or at least one anionic styrene-acrylic polymer having a molecular weight greater than 10,000 Daltons.

5. The aqueous colorless particle-free inkjet ink composition of claim 1 , wherein a total amount of the anionic polyether polyurethane and the anionic acrylic polymer or the anionic styrene-acrylic polymer is at least 5 weight % and up to and including 18 weight %, based on the total aqueous colorless particle-free inkjet ink composition weight.

6. The aqueous colorless particle-free inkjet ink composition of claim 1 , further comprising a modified polysiloxane in an amount of up to and including 1 weight %, based on the total aqueous colorless particle-free inkjet ink composition weight.

7. The aqueous colorless particle-free inkjet ink composition of claim 1 , comprising less than 0.2 weight % of a wax based on the total aqueous colorless particle-free inkjet ink composition weight.

8. A method of inkjet printing, comprising:

providing a substrate,

ink jetting the aqueous colorless particle-free inkjet ink composition onto the substrate from a recirculating main fluid supply containing the aqueous colorless particle-free inkjet ink composition,

wherein the aqueous colorless particle-free inkjet ink composition has a viscosity of less than 5 centipoises (0.005 N-sec) at 25° C., and comprises:

an anionic polyether polyurethane having an acid number of at least 50 and an anionic acrylic polymer or anionic styrene-acrylic polymer having an acid number of at least 50; wherein the weight ratio of the anionic polyether polyurethane to the anionic acrylic polymer or anionic styrene-acrylic polymer is from 1:9 to and including 9:1, and the total amount of the anionic polyether polyurethane and the anionic acrylic polymer or anionic styrene-acrylic polymer is less than or equal to 20 weight % based on the total aqueous colorless particle-free inkjet ink composition weight, and

a defoamer that has a hydrophilic-lipophilic balance value of at least 3 and up to and including 5, which defoamer is present in an amount of at least 0.15 weight % and up to and including 1 weight %, based on the total aqueous colorless particle-free inkjet ink composition weight.

9. The method of claim 8 , comprising:

supplying the aqueous colorless particle-free inkjet ink composition as a continuous stream from the recirculating main fluid supply,

during ink jetting, breaking the continuous stream into both printing ink drops and non-printing ink drops; and

collecting and returning the non-printing drops to the recirculating main fluid supply.

10. The method of claim 9 , carried out using a continuous inkjet printing apparatus comprising the recirculating main fluid supply.

11. The method of claim 8 , wherein the ink jetting is carried out at a drop generation frequency of at least 100 kHz with a near nozzle velocity of at least 10 m/sec.

12. The method of claim 8 , wherein the aqueous colorless particle-free inkjet ink composition has a viscosity of less than or equal to 3 centipoises (0.003 N-sec) at 25° C.

13. The method of claim 8 , wherein the aqueous colorless particle-free inkjet ink composition has a static surface tension of less than 38 dynes/cm when measured by the Wilhelmy Plate method.

14. The method of claim 8 comprising:

ink jetting the aqueous colorless particle-free inkjet ink composition, as colorless printing drops to provide increased glossiness of colored areas or non-colored areas of a colored image by at least 3 gloss units compared to the glossiness of the colored areas or non-colored areas of the colored image without the aqueous colorless particle-free inkjet ink composition, as measured by a 75° glossmeter.

15. An ink set comprising at least the following individual inks:

1) the aqueous colorless particle-free inkjet ink composition of claim 1 ; and

2) an aqueous color inkjet ink composition that comprises at least one colorant.

16. The ink set of claim 15 , wherein the aqueous color inkjet ink composition that comprises at least one colorant is one of the following compositions:

an aqueous cyan inkjet ink composition,

an aqueous magenta inkjet ink composition,

an aqueous yellow inkjet ink composition, or

an aqueous black inkjet ink composition.

Assignments (9)
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 4, 2021
From: EASTMAN KODAK COMPANY
To: ALTER DOMUS (US) LLC
Reel/Frame 056733/0681 →
NOTICE OF SECURITY INTERESTS Recorded Mar 4, 2021
From: EASTMAN KODAK COMPANY
To: BANK OF AMERICA, N.A., AS AGENT
Reel/Frame 056984/0001 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 4, 2021
From: EASTMAN KODAK COMPANY
To: ALTER DOMUS (US) LLC
Reel/Frame 056734/0233 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 4, 2021
From: EASTMAN KODAK COMPANY
To: ALTER DOMUS (US) LLC
Reel/Frame 056734/0001 →
RELEASE OF SECURITY INTEREST Recorded Jul 30, 2019
From: JP MORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: EASTMAN KODAK COMPANY; FAR EAST DEVELOPMENT LTD.; PFC, INC.; KODAK (NEAR EAST), INC.; KODAK AMERICAS, LTD.; KODAK IMAGING NETWORK, INC.; KODAK PORTUGUESA LIMITED; KODAK REALTY, INC.; LASER PACIFIC MEDIA CORPORATION; PAKON, INC.; QUALEX, INC.; KODAK PHILIPPINES, LTD.; NPEC, INC.; CREO MANUFACTURING AMERICA LLC; KODAK AVIATION LEASING LLC
Reel/Frame 049901/0001 →
RELEASE OF SECURITY INTEREST Recorded Jul 22, 2019
From: JP MORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: QUALEX, INC.; EASTMAN KODAK COMPANY; FAR EAST DEVELOPMENT LTD.; FPC, INC.; KODAK (NEAR EAST), INC.; KODAK AMERICAS, LTD.; KODAK IMAGING NETWORK, INC.; KODAK PORTUGUESA LIMITED; KODAK REALTY, INC.; LASER PACIFIC MEDIA CORPORATION; PAKON, INC.; KODAK PHILIPPINES, LTD.; NPEC, INC.; CREO MANUFACTURING AMERICA LLC; KODAK AVIATION LEASING LLC
Reel/Frame 050239/0001 →
SECURITY INTEREST Recorded Nov 16, 2016
From: EASTMAN KODAK COMPANY; FAR EAST DEVELOPMENT LTD.; FPC INC.; KODAK (NEAR EAST), INC.; KODAK AMERICAS, LTD.; KODAK REALTY, INC.; LASER-PACIFIC MEDIA CORPORATION; QUALEX INC.; KODAK PHILIPPINES, LTD.; NPEC INC.
To: JP MORGAN CHASE BANK, N.A.
Reel/Frame 040340/0017 →
SECURITY INTEREST Recorded Nov 16, 2016
From: EASTMAN KODAK COMPANY; FAR EAST DEVELOPMENT LTD.; FPC INC.; KODAK (NEAR EAST), INC.; KODAK AMERICAS, LTD.; KODAK REALTY, INC.; LASER-PACIFIC MEDIA CORPORATION; QUALEX INC.; KODAK PHILIPPINES, LTD.; NPEC INC.
To: BANK OF AMERICA N.A.
Reel/Frame 040340/0193 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 18, 2016
From: LUSSIER, BARBARA BOLAND; LINEHAN, DANIEL TALBOT
To: EASTMAN KODAK COMPANY
Reel/Frame 039474/0841 →