IP Library Granted Patent US 9,896,424
Granted Patent B2
US 9,896,424 · App. 15/241,799 · Granted Feb 20, 2018

Methods of making sulfurized derivatives

Inventors: Stephen A. Di Biase (River Forest, IL); Syed Q. A. Rizvi (Painesville, OH); Georgeta Hategan (Plainfield, IL)
Assignee: Elevance Renewable Sciences, Inc.
C07D307/60C08F20/14C08F20/68C08F120/04C08F120/10C08F122/105C08F210/14C10L1/1883C10L1/1905C10L1/224C10M107/32C10M129/68C10M129/72C10M133/16C10M135/04C10M135/06C10M145/08C10M149/02C10M159/20C11C3/00C11C3/003C11D3/3746C10M2201/02C10M2201/062C10M2203/1006C10M2203/1025C10M2205/028C10M2205/0285C10M2207/123C10M2207/282C10M2209/04C10M2209/1023C10M2215/08C10M2215/28C10M2217/06C10M2219/022C10M2219/024C10M2219/044C10M2219/046C10N2210/01C10N2210/02C10N2210/03C10N2210/04C10N2210/05C10N2220/021C10N2220/022C10N2230/06C10N2230/08C10N2230/70C10N2240/10C10N2250/10C10N2260/06C10N2260/09C10N2270/02
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Quick Facts
Patent No.
US 9,896,424
App. No.
15/241,799
Granted
Feb 20, 2018
Kind
B2
Abstract

This disclosure relates to sulfurized derivatives made from functionalized monomers. The disclosure relates to lubricants, functional fluids, fuels, dispersants, detergents and functional compositions (e.g., cleaning solutions, food compositions, etc.)

Claims (21)

1. A method of making sulfurized derivatives of metathesis-derived compounds, the method comprising:

providing a functionalized monomer, wherein the functionalized monomer is a compound having an unsaturated hydrocarbyl group having 8 to 12 carbon atoms with a functional group attached thereto, wherein said functional group is a carboxylic acid group of an ester thereof, and wherein the unsaturated hydrocarbyl group has a carbon-carbon double bond in the terminal position; and

reacting the functionalized monomer with a sulfurizing agent to form a sulfurized derivative.

2. The method of claim 1 , wherein the unsaturated hydrocarbyl group is linear.

3. The method claim 1 , wherein the unsaturated hydrocarbyl group has 1 or 2 carbon-carbon double bonds.

4. The method of claim 2 , wherein the unsaturated hydrocarbyl group has 1 or 2 carbon-carbon double bonds.

5. The method of claim 1 , wherein the hydrocarbyl group is a 1-decenyl group.

6. The method of claim 1 , wherein the functional group is a monoglyceride ester of a carboxylic acid, a diglyceride ester of a carboxylic acid, or a triglyceride ester of a carboxylic acid.

7. The method of claim 5 , wherein the functional group is a monoglyceride ester of a carboxylic acid, a diglyceride ester of a carboxylic acid, or a triglyceride ester of a carboxylic acid.

8. The method of claim 1 , wherein the functional group is a triglyceride ester of a carboxylic acid.

9. The method of claim 5 , wherein the functional group is a triglyceride ester of a carboxylic acid.

10. The method of claim 1 , wherein the functional group is a methyl ester of a carboxylic acid, a ethyl ester of a carboxylic acid, or a propyl ester of a carboxylic acid, or a butyl ester of a carboxylic acid.

11. The method of claim 5 , wherein the functional group is a methyl ester of a carboxylic acid, a ethyl ester of a carboxylic acid, or a propyl ester of a carboxylic acid, or a butyl ester of a carboxylic acid.

12. The method of claim 1 , wherein the functional group is a methyl ester of a carboxylic acid.

13. The method of claim 5 , wherein the functional group is a methyl ester of a carboxylic acid.

14. The method of claim 12 , wherein the functionalized monomer is selected from the group consisting of: methyl 8-nonenoate, methyl 9-decenoate, methyl 10-undecenoate, and methyl 9-dodecenoate.

15. The method of claim 14 , wherein the functionalized monomer is methyl 9-decenoate.

16. The method of claim 14 , wherein the functionalized monomer is methyl 10-undecenoate.

17. The method of claim 14 , wherein the functionalized monomer is methyl 9-dodecenoate.

18. The method of claim 1 , wherein the functionalized monomer is derived from a process that comprises the reaction of a vegetable oil with a short-chain olefin, wherein the short-chain olefin is selected from the group consisting of: ethylene, 1-propene, 1-butene, 1-pentene, 1-hexene, 1-heptene, 1-octene, 1-nonene, 1-decene, 1-undecene, 1-dodecene, 1-tridecene, 1-tetradecene, 1-pentadecene, 1-hexadecene, 1-octadecene, 1-eicosene, and mixtures of two or more thereof.

19. The method of claim 18 , wherein the vegetable oil is selected from the group consisting of: soybean oil, rapeseed oil, corn oil, sesame oil, cottonseed oil, sunflower seed oil, canola oil, safflower oil, palm oil, palm kernel oil, linseed oil, castor oil, olive oil, peanut oil, coriander oil, almond oil, and wheat germ oil.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 15, 2020
From: ELEVANCE RENEWABLE SCIENCES, INC.
To: WILMAR TRADING PTE LTD
Reel/Frame 052942/0933 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 7, 2016
From: DIBIASE, STEPHEN AUGUSTINE; RIZVI, SYED Q.A.; HATEGAN, GEORGETA
To: ELEVANCE RENEWABLE SCIENCES, INC.
Reel/Frame 039964/0868 →
Continuity (9)
Continuation 13428268 · Mar 23, 2012
Continuation In Part 13281108 · Oct 25, 2011
Provisional Application 61510159 · Jul 21, 2011
Provisional Application 61467273 · Mar 24, 2011
Provisional Application 61467275 · Mar 24, 2011
Provisional Application 61467276 · Mar 24, 2011
Provisional Application 61467279 · Mar 24, 2011
Provisional Application 61467292 · Mar 24, 2011
Related Publication 20160355492A1 · Dec 8, 2016