IP Library Granted Patent US 10,213,389
Granted Patent B2
US 10,213,389 · App. 15/257,653 · Granted Feb 26, 2019

Controlled release compositions comprising a combination of isosorbide dinitrate and hydralazine hydrochloride

Inventors: Gurvinder Singh Rekhi (Suwanee, GA); Richard Sidwell (Cumming, GA); Sharon Hamm (Atlanta, GA)
Assignee: Recro Gainesville LLC
A61K9/4808A61K9/485A61K9/4825A61K9/4858A61K9/4866A61K9/5026A61K9/5078A61K9/5084A61K31/34A61K31/403A61K31/4745A61K31/502A61K31/58A61K31/704
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Quick Facts
Patent No.
US 10,213,389
App. No.
15/257,653
Granted
Feb 26, 2019
Kind
B2
Abstract

The invention relates to a controlled release composition comprising a combination of isosorbide dinitrate and hydralazine, such as hydralazine hydrochloride, that in operation delivers the drug in a pulsed or multi-modal manner for the treatment of angina, ischaemic heart disease, arterial hypertension and related disease conditions. Preferably, the isosorbide dinitrate and hydralazine hydrochloride can be released from the dosage form in an erodable, diffusion and/or osmotic-controlled release profile.

Claims (10)

1. A hard gelatin capsule comprising:

a population of isosorbide dinitrate immediate-release beads comprising: isosorbide dinitrate in an amount from about 2.5 mg to about 30 mg, mannitol, povidone, silicon dioxide, and sugar spheres;

a population of isosorbide dinitrate sustained-release beads comprising: isosorbide dinitrate in an amount from about 2.5 mg to about 30 mg, mannitol, povidone, silicon dioxide, sugar spheres, triethyl citrate, an ammonio methacrylate copolymer, and a methacrylic acid copolymer;

a population of hydralazine immediate-release beads comprising: hydralazine, or a salt thereof, in an amount from about 0.5 mg to about 60 mg, povidone, silicon dioxide, sugar spheres, and citric acid; and

a population of hydralazine sustained-release beads comprising: hydralazine, or a salt thereof, in an amount from about 2.5 mg to about 30 mg, povidone, silicon dioxide, sugar spheres, citric acid, an ammonio methacrylate copolymer, a methacrylic acid copolymer, and triethyl citrate.

2. The capsule of claim 1 wherein the hydralazine is hydralazine hydrochloride.

3. A method for the treatment of a patient having angina, ischaemic heart disease, or arterial hypertension comprising orally administering to the patient a therapeutically effective amount of the capsule of claim 1 .

4. A method for the treatment of a patient having angina, ischaemic heart disease, or arterial hypertension comprising orally administering to the patient a therapeutically effective amount of the capsule of claim 2 .

5. The capsule of claim 1 , wherein the populations of isosorbide dinitrate immediate-release beads and hydralazine immediate-release beads comprise about 10% to about 60% of the total population of beads.

6. The capsule of claim 1 , wherein the populations of isosorbide dinitrate sustained-release beads and hydralazine sustained-release beads comprise about 30% to about 90% of the total population of beads.

Assignments (18)
RELEASE OF SECURITY INTEREST Recorded Dec 18, 2025
From: OAKTREE FUND ADMINISTRATION, LLC
To: SOCIETAL CDMO GAINESVILLE, LLC
Reel/Frame 073261/0070 →
SECURITY INTEREST Recorded Dec 17, 2025
From: SOCIETAL CDMO, INC.; SOCIETAL CDMO GAINESVILLE, LLC
To: ARES CAPITAL CORPORATION, AS ADMINISTRATIVE AGENT
Reel/Frame 073250/0079 →
RELEASE OF SECURITY INTEREST Recorded Apr 10, 2024
From: ROYAL BANK OF CANADA
To: SOCIETAL CDMO GAINESVILLE, LLC
Reel/Frame 067060/0587 →
SECURITY INTEREST Recorded Apr 10, 2024
From: SOCIETAL CDMO GAINESVILLE, LLC
To: OAKTREE FUND ADMINISTRATION, LLC
Reel/Frame 067060/0699 →
SECURITY INTEREST Recorded Dec 17, 2022
From: SOCIETAL CDMO GAINESVILLE, LLC (F/K/A RECRO GAINESVILLE, LLC)
To: ROYAL BANK OF CANADA, AS ADMINISTRATIVE AGENT
Reel/Frame 062132/0646 →
CHANGE OF NAME Recorded Dec 16, 2022
From: RECRO GAINESVILLE LLC
To: SOCIETAL CDMO GAINESVILLE, LLC
Reel/Frame 063055/0210 →
RELEASE OF SECURITY INTEREST Recorded Dec 16, 2022
From: ATHYRIUM OPPORTUNITIES III ACQUISITION LP
To: SOCIETAL CDMO GAINESVILLE, LLC
Reel/Frame 062123/0339 →
CORRECTIVE ASSIGNMENT TO CORRECT THE RECEIVING PARTY'S NAME PREVIOUSLY RECORDED AT REEL: 044165 FRAME: 0783. ASSIGNOR(S) HEREBY CONFIRMS THE GRANT OF SECURITY INTEREST . Recorded Mar 8, 2019
From: RECRO GAINESVILLE LLC
To: ATHYRIUM OPPORTUNITIES III ACQUISITION LP
Reel/Frame 048540/0737 →
SECURITY INTEREST Recorded Nov 17, 2017
From: RECRO GAINESVILLE LLC
To: ATHYRIUM OPPORTUNITIES III ACQUSITION LP
Reel/Frame 044165/0783 →
CHANGE OF NAME Recorded Sep 13, 2017
From: ALKERMES SCIENCE ONE LIMITED
To: DARAVITA LIMITED
Reel/Frame 043574/0258 →
MERGER Recorded Sep 13, 2017
From: RECRO TECHNOLOGY LLC
To: RECRO GAINESVILLE LLC
Reel/Frame 043574/0494 →
ASSET TRANSFER AGREEMENT Recorded Sep 13, 2017
From: ELAN PHARMA INTERNATIONAL LIMITED
To: EDT PHARMA HOLDINGS LIMITED
Reel/Frame 043844/0001 →
CHANGE OF NAME Recorded Sep 13, 2017
From: EDT PHARMA HOLDINGS LIMITED
To: ALKERMES PHARMA IRELAND LIMITED
Reel/Frame 043844/0144 →
INTELLECTUAL PROPERTY TRANSFER AND LICENSE AGREEMENT Recorded Sep 13, 2017
From: ALKERMES PHARMA IRELAND LIMITED
To: ALKERMES SCIENCE ONE LIMITED
Reel/Frame 043844/0302 →
BUSINESS TRANSFER AGREEMENT Recorded Sep 13, 2017
From: DARAVITA LIMITED
To: ALKERMES PHARMA IRELAND LIMITED
Reel/Frame 043844/0353 →
ASSET TRANSFER AND LICENSE AGREEMENT Recorded Sep 13, 2017
From: ALKERMES PHARMA IRELAND LIMITED
To: DV TECHNOLOGY LLC
Reel/Frame 043844/0379 →
CHANGE OF NAME Recorded Sep 13, 2017
From: DV TECHNOLOGY LLC
To: RECRO TECHNOLOGY LLC
Reel/Frame 043844/0446 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 13, 2017
From: REKHI, GURVINDER SINGH; SIDWELL, RICHARD; HAMM, SHARON
To: ELAN PHARMA INTERNATIONAL LIMITED
Reel/Frame 043573/0697 →
Continuity (6)
Continuation 15017690 · Feb 8, 2016
Continuation 14638984 · Mar 4, 2015
Continuation 13606915 · Sep 7, 2012
Continuation 13278787 · Oct 21, 2011
Continuation 11262672 · Oct 31, 2005
Related Publication 20170209381A1 · Jul 27, 2017