IP Library Granted Patent US 10,596,603
Granted Patent B2
US 10,596,603 · App. 15/265,392 · Granted Mar 24, 2020

Method of producing gluten free oats

Inventors: Mark A. Arlinghaus (Minneapolis, MN); Troy D. Bierbaum (Brooklyn Park, MN); Christine M. Nowakowski (Plymouth, MN); Daniel J. Winderl (Plymouth, MN); Philip K. Zietlow (Wayzata, MN)
Assignee: General Mills, Inc.
B07C5/3425A23L7/143G01N21/85G01N21/94A23V2002/00B07C2501/0081G01N2021/8592
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Quick Facts
Patent No.
US 10,596,603
App. No.
15/265,392
Granted
Mar 24, 2020
Kind
B2
Abstract

The separation of oats from a combination of grains is performed by obtaining optical data includes both reflectance data and visual data and then analyzing the data in multiple ways, including analyzing information obtained based on ratios of wavelengths and grain imagery. The reflectance data relies on near infrared spectroscopy at requisite ratios of wavelengths in the range of 1100 nm to 2200 nm, while the grain imagery encompasses images of both sides of each of the combination of grains and can also take into account grain size and shape differentiations. The results is an oats separation process wherein at least 99% of foreign grains are rejected with only about 3% of the oats being rejected, while enabling volume processing of grains and establishing a supply of oats with a gluten level well below 20 ppm.

Claims (41)

1. A method of producing gluten-free oats from a combination of grains comprising:

optically analyzing the combination of grains employing ratios of wavelengths; and

separating the oats from the combination of grains to establish a supply of oats having a gluten level below 20 ppm based on the optical analysis.

2. The method of claim 1 , wherein optically analyzing the combination of grains is performed utilizing near infrared cameras operating in the range of 1100 nm to 2200 nm.

3. The method of claim 2 , further comprising: employing band pass filters for the cameras centered at 1220 nm and 1460 nm.

4. The method of claim 2 , wherein the ratios of wavelengths are selected from the group consisting of 1460 nm/1211 nm, 1653 nm/1211 nm, 1653 nm/1460 nm, 1211 nm/1460 nm, and 1211 nm/1653 nm.

5. The method of claim 2 , further comprising: extracting size and shape information from data received from camera data, wherein separating the oats is further performed based on the size and shape information.

6. The method of claim 1 , wherein optically analyzing the combination of grains includes evaluating near infrared reflectance data at just two wavelength ratios.

7. The method of claim 1 , wherein optically analyzing the combination of grains employs both near infrared spectroscopy at requisite ratios of wavelengths and visual imagery for identifying and separating foreign grains of the combination of grains from the oats.

8. The method of claim 1 , further comprising: utilizing visible spectrum cameras to obtain image data of both sides of the combination of grains, wherein separating the oats is further performed based on the image data.

9. The method of claim 1 , wherein separating the oats from the combination of grains constitutes rejecting at least 99% of foreign grains while rejecting only about 3% of the oats.

10. The method of claim 1 , wherein separating the oats from the combination of grains results in oats with a gluten level of no greater than 10 ppm.

11. The method of claim 1 , further comprising: employing discriminant analysis in separating the oats from the combination of grains.

12. The method of claim 1 , wherein the oats are separated from the combination of grains through volume processing.

13. The method of claim 1 , wherein employing ratios of wavelengths includes employing ratios of peak heights at the wavelengths by:

measuring seed spectra in a scan,

identifying wavelengths of spectral peaks in the scan using first derivatives of the spectra,

measuring spectral peak heights at the identified wavelengths, and

determining the ratios of peak heights at the identified wavelengths; and wherein separating the oats includes:

keeping seeds with ratios that correspond to oats, and

removing seeds with ratios that do not correspond to oats.

14. The method of claim 1 , wherein employing ratios of wavelengths includes employing ratios of peak heights at the wavelengths and wherein separating the oats includes keeping seeds with ratios of peak heights that correspond to oats and removing seeds with ratios of peak heights that do not correspond to oats.

15. The method of claim 1 , wherein employing ratios of wavelengths includes employing ratios of peak heights at the wavelengths by:

measuring seed spectra in a scan;

identifying wavelengths of spectral peaks in the scan;

measuring spectral peak heights at the identified wavelengths; and

determining the ratios of peak heights at the identified wavelengths, and wherein separating the oats includes:

keeping seeds with ratios of peak heights that correspond to oats; and

removing seeds with ratios of peak heights that do not correspond to oats.

16. A method of producing gluten-free oats from a combination of grains comprising:

obtaining optical data on the combination of grains, wherein at least a portion of the optical data is obtained from one or more cameras;

analyzing the optical data; and

separating the oats from the combination of grains to establish a supply of oats having a gluten level below 20 ppm based on the analysis of the optical data.

17. The method of claim 16 , wherein the optical data is obtained utilizing near infrared cameras operating in the range of 1100 nm to 2200 nm.

18. The method of claim 16 , wherein analyzing the optical data includes analyzing reflectance data utilizing ratios of wavelengths selected from the group consisting of 1460 nm/1211 nm, 1653 nm/1211 nm, 1653 nm/1460 nm, 1211 nm/1460 nm, and 1211 nm/1653 nm.

19. The method of claim 16 , further comprising: extracting size and shape information from the optical data, wherein separating the oats is further performed based on the size and shape information.

20. The method of claim 16 , wherein separating the oats from the combination of grains constitutes rejecting at least 99% of foreign grains while rejecting only about 3% of the oats.

21. The method of claim 16 , wherein separating the oats from the combination of grains results in oats with a gluten level of no greater than 10 ppm.

22. The method of claim 16 , wherein the optical data includes both reflectance and visual data.

23. The method of claim 22 , wherein the visual data includes images of both sides of each of the combination of grains.

24. The method of claim 16 , wherein analyzing the optical data includes employing visual imagery for identifying and separating foreign grains of the combination of grains from the oats.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 14, 2016
From: ARLINGHAUS, MARK E; NOWAKOWSKI, CHRISTINE M; BIERBAUM, TROY D; WINDERL, DANIEL J; ZIETLOW, PHILIP K
To: GENERAL MILLS, INC.
Reel/Frame 039741/0651 →
Continuity (3)
Continuation 13782497 · Mar 1, 2013
Provisional Application 61605561 · Mar 1, 2012
Related Publication 20170001220A1 · Jan 5, 2017