IP Library Granted Patent US 10,280,498
Granted Patent B2
US 10,280,498 · App. 15/291,570 · Granted May 7, 2019

High temperature, damage tolerant superalloy, an article of manufacture made from the alloy, and process for making the alloy

Inventors: Karl A. Heck (West Lawn, PA); Samuel J. Kernion (Lancaster, PA)
Assignee: CRS HOLDINGS, INC.
C22F1/10C22C19/05C22C19/056
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Quick Facts
Patent No.
US 10,280,498
App. No.
15/291,570
Granted
May 7, 2019
Kind
B2
Abstract

A nickel-base alloy is disclosed that has the following weight percent composition. C about 0.005 to about 0.06 Cr about 13 to about 17 Fe about 4 to about 20 Mo about 3 to about 9 W up to about 8 Co up to about 12 Al about 1 to about 3 Ti about 0.6 to about 3 Nb up to about 5.5 B about 0.001 to about 0.012 Mg about 0.0010 to about 0.0020 Zr about 0.01 to about 0.08 Si up to about 0.7 P up to about 0.05 and the balance is nickel, usual impurities, and minor amounts of other elements as residuals from alloying additions during melting. The alloy provides a combination of high strength, good creep resistance, and good resistance to crack growth. A method of heat treating a nickel base superalloy to improve the tensile ductility of the alloy is also disclosed. An article of manufacture made from the nickel base superalloy described herein is also disclosed.

Claims (109)

1. A nickel-base superalloy that provides a combination of high strength, good creep resistance, and good resistance to crack growth, said alloy consisting essentially of, in weight percent:

C about 0.005 to about 0.1

Cr about 13 to about 17

Fe about 4 to about 20

Mo about 3 to about 9

W up to about 8

Co up to about 8

Al about 1 to about 3

Ti about 0.6 to about 3

Nb up to about 5.5

B about 0.001 to about 0.015

Mg about 0.0001 to about 0.0050

Zr about 0.001 to about 0.08

Si up to about 0.7

P up to about 0.05

and the balance is nickel, usual impurities, and minor amounts of other elements as residuals from alloying additions during melting.

2. The alloy as claimed in claim 1 which contains at least about 0.01% carbon.

3. The alloy as claimed in claim 1 which contains at least about 14% chromium.

4. The alloy as claimed in claim 1 which contains at least about 3.5% molybdenum.

5. The alloy as claimed in claim 1 which contains not more than about 17% iron.

6. The alloy as claimed in claim 1 which contains at least about 1% niobium.

7. The alloy as claimed in claim 1 which contains at least about 1% titanium.

8. A nickel-base superalloy that provides a combination of high strength, good creep resistance, and good resistance to crack growth, said alloy consisting essentially of, in weight percent:

C about 0.01 to about 0.05

Cr about 14 to about 16

Fe about 8 to about 17

Mo about 3.5 to about 8

W up to about 4

Co up to about 8

Al about 1.5 to about 2.5

Ti about 1 to about 2.5

Nb about 1 to about 5

B about 0.003 to about 0.010

Mg about 0.0001 to about 0.0020

Zr about 0.015 to about 0.06

Si up to about 0.7

P up to about 0.05

and the balance is nickel, usual impurities, and minor amounts of other elements as residuals from alloying additions during melting.

9. The alloy as claimed in claim 8 which contains at least about 0.02% carbon.

10. The alloy as claimed in claim 8 which contains at least about 14.5% chromium.

11. The alloy as claimed in claim 8 which contains at least about 3.8% molybdenum.

12. The alloy as claimed in claim 8 which contains not more than about 16% iron.

13. The alloy as claimed in claim 8 which contains up to about 5% cobalt.

14. The alloy as claimed in claim 8 which contains at least about 2% niobium.

15. The alloy as claimed in claim 8 which contains at least about 1.5% titanium.

16. A nickel-base superalloy that provides a combination of high strength, good creep resistance, and good resistance to crack growth, said alloy consisting essentially of, in weight percent:

C about 0.02 to about 0.04

Cr about 14.5 to about 15.5

Fe about 9 to about 16

Mo about 3.8 to about 4.5

W up to about 3

Co up to about 5

Al about 1.8 to about 2.2

Ti about 1.5 to about 2.1

Nb about 2 to about 4.5

B about 0.004 to about 0.008

Mg about 0.0001 to about 0.0016

Zr about 0.02 to about 0.04

Si up to about 0.7

P up to about 0.05

and the balance is nickel, usual impurities, and minor amounts of other elements as residuals from alloying additions during melting.

17. An article of manufacture having a combination of high strength, good creep resistance, and good resistance to crack growth, said article being made from a nickel-base superalloy that consists essentially of, in weight percent:

C about 0.005 to about 0.06

Cr about 13 to about 17

Fe about 4 to about 20

Mo about 3 to about 9

W up to about 8

Co up to about 8

Al about 1 to about 3

Ti about 0.6 to about 3

Nb up to about 5.5

B about 0.001 to about 0.012

Mg about 0.0001 to about 0.0020

Zr about 0.01 to about 0.08

Si up to about 0.7

P up to about 0.05

and the balance is nickel, usual impurities, and minor amounts of other elements as residuals from alloying additions during melting, wherein said alloy is characterized by a solvus temperature.

18. An article of manufacture having a combination of high strength, good creep resistance, and good resistance to crack growth, said article being made from a nickel-base superalloy that consists essentially of, in weight percent:

C about 0.01 to about 0.05

Cr about 14 to about 16

Fe about 8 to about 17

Mo about 3.5 to about 8

W up to about 4

Co up to about 8

Al about 1.5 to about 2.5

Ti about 1 to about 2.5

Nb about 1 to about 5

B about 0.003 to about 0.010

Mg about 0.0001 to about 0.0020

Zr about 0.015 to about 0.06

Si up to about 0.7

P up to about 0.05

and the balance is nickel, usual impurities, and minor amounts of other elements as residuals from alloying additions during melting, wherein the alloy has a γ′ solvus temperature not greater than about 1860° F.

19. An article of manufacture having a combination of high strength, good creep resistance, and good resistance to crack growth, said article being made from a nickel-base superalloy that consists essentially of, in weight percent:

C about 0.01 to about 0.05

Cr about 14 to about 16

Fe about 8 to about 17

Mo about 3.5 to about 8

W up to about 4

Co up to about 8

Al about 1.5 to about 2.5

Ti about 1 to about 2.5

Nb about 1 to about 5

B about 0.003 to about 0.010

Mg about 0.0001 to about 0.0020

Zr about 0.015 to about 0.06

Si up to about 0.7

P up to about 0.05

and the balance is nickel, usual impurities, and minor amounts of other elements as residuals from alloying additions during melting, wherein the alloy has a γ′ solvus temperature greater than about 1880° F. and when the article is annealed at a temperature below the solvus temperature, the alloy contains not more than about 1% tungsten.

Assignments (2)
ENTITY CONVERSION Recorded Nov 18, 2021
From: CRS HOLDINGS, INC.
To: CRS HOLDINGS, LLC
Reel/Frame 059002/0754 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 15, 2017
From: HECK, KARL A.; KERNION, SAMUEL J.
To: CRS HOLDINGS, INC.
Reel/Frame 042716/0133 →
Continuity (1)
Related Publication 20180100222A1 · Apr 12, 2018
Cited By (2)
US 12,435,393 US 12,492,452