IP Library Granted Patent US 10,662,449
Granted Patent B2
US 10,662,449 · App. 15/311,794 · Granted May 26, 2020

Method for producing compound and compound production system used in production method

Inventors: Makoto Kano (Yokohama, JP); Takamitsu Kariya (Yokohama, JP); Hiroyasu Banba (Yokohama, JP); Tomohiko Mawatari (Yokohama, JP); Takeshi Kato (Otake, JP); Tsutomu Hirachi (Tokyo, JP); Keizo Tachibana (Yokohama, JP); Masahiro Kamide (Toyohashi, JP); Megumu Morimoto (Tokyo, JP)
Assignees: Mitsubishi Chemical Corporation; Mitsubishi Chemical Engineering Corporation
C12P13/02C12M1/02C12M23/58C12M27/02
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Quick Facts
Patent No.
US 10,662,449
App. No.
15/311,794
Granted
May 26, 2020
Kind
B2
Abstract

This method for producing a compound uses a continuous tank reactor which is provided with two or more reaction tanks for producing the compound and with a reaction liquid feeding pipe that feeds a reaction liquid from an upstream reaction tank to a downstream reaction tank, said method being characterized in that the Reynold's number of the reaction liquid that flows in the reaction liquid feeding pipe is configured to be 1800-22000. Furthermore, this compound production system is used in said method for producing a compound, and is formed by housing at least one of the reaction tanks in a portable container.

Claims (15)

1. A method for producing acrylamide in a continuous tank reactor, the method comprising:

flowing a reaction liquid, which comprises acrylonitrile, a biocatalyst, and an acid or alkali solution from an upstream reaction tank to a downstream reaction tank via a reaction liquid feeding pipe at a Reynolds number of 2,000 to 20,000, wherein the continuous tank reactor comprises two or more reaction tanks, and the reaction liquid feeding pipe connects the upstream reaction tank to the adjacent downstream reaction tank, and a height of a liquid surface of the downstream reaction tank is lower than the height of the liquid surface of the upstream reaction tank,

wherein the method produces acrylamide.

2. The method according to claim 1 , wherein at least one tank of the reaction tanks is accommodated in a portable container, and a value obtained by dividing an inner volume (m 3 ) of the portable container by a flow rate (m 3 /hour) of the reaction liquid flowing in the at least one reaction tank accommodated in the portable container is from 5 to 70 hours.

3. The method according to claim 1 , further comprising:

supplying an acrylonitrile-containing liquid to at least one tank of the reaction tanks;

supplying raw water to at least one tank of the reaction tanks; and

supplying a biocatalyst aqueous dispersion to at least one tank of the reaction tanks.

4. The method according to claim 1 , further comprising:

supplying an acrylonitrile-containing liquid, raw water and a biocatalyst aqueous dispersion to at least a tank positioned at the most upstream side of the reaction liquid.

5. The method of claim 1 , wherein at least one tank of the reaction tanks is accommodated in a portable container, and wherein a total volume of the at least one tank accommodated in the portable container is ⅙ to ⅗ of an inner volume of the portable container.

6. The method of claim 1 , wherein at least one tank of the reaction tanks is accommodated in a portable container, and wherein another portable container is disposed on the portable container in which the at least one tank of the reaction tanks is accommodated.

7. The method of claim 1 , wherein at least one tank of the reaction tanks is accommodated in a portable container, and wherein a volume of the at least one reaction tank accommodated in the portable container is from 6.4 m 3 to 22.9 m 3 .

8. The method of claim 1 , wherein the liquid surface height difference between the reaction tank and the adjacent reaction tank is 0.05 to 10 cm.

9. The method of claim 1 , wherein the liquid surface height difference between the reaction tank and the adjacent reaction tank is 0.1 to 3 cm.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 19, 2021
From: MITSUBISHI CHEMICAL ENGINEERING CORPORATION
To: MITSUBISHI CHEMICAL CORPORATION
Reel/Frame 055334/0300 →
CORPORATE NAME CHANGE Recorded Jun 19, 2017
From: MITSUBISHI RAYON CO., LTD.
To: MITSUBISHI CHEMICAL CORPORATION
Reel/Frame 042886/0294 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 16, 2017
From: KANO, MAKOTO; KARIYA, TAKAMITSU; BANBA, HIROYASU; MAWATARI, TOMOHIKO; KATO, TAKESHI; HIRACHI, TSUTOMU; TACHIBANA, KEIZO; KAMIDE, MASAHIRO; MORIMOTO, MEGUMU
To: MITSUBISHI RAYON CO., LTD.; MITSUBISHI CHEMICAL ENGINEERING CORPORATION
Reel/Frame 042728/0940 →