IP Library Granted Patent US 10,479,849
Granted Patent B2
US 10,479,849 · App. 15/341,461 · Granted Nov 19, 2019

Low emission propylene-based polymer resins

Inventors: Jeffrey Salek (Pittsburgh, PA); Mark Chappell (Pittsburgh, PA); Bryan Dawson (Pittsburgh, PA)
Assignee: BRASKEM AMERICA, INC.
C08F110/06C08L23/12C08L2205/025
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,479,849
App. No.
15/341,461
Granted
Nov 19, 2019
Kind
B2
Abstract

A propylene-based polymer resin is characterized by a low volatile emission signature. For example, the propylene-based polymer resin may have a volatile organic compound content no greater than 125 ppm, a semi-volatile organic compound content no greater than 500 ppm, and a C36 oligomeric content no greater than 250 ppm.

Claims (47)

1. A propylene-based polymer resin comprising:

a volatile organic compound content no greater than 125 ppm;

a semi-volatile organic compound content no greater than 500 ppm; and

a C36 oligomeric content no greater than 250 ppm, wherein the propylene-based polymer resin is produced utilizing a Ziegler-Natta catalyst.

2. The propylene-based polymer resin of claim 1 , wherein the resin has a tan delta of less than 10.0 at an angular frequency of 0.1 rad/s (180° C.).

3. The propylene-based polymer resin of claim 1 , wherein the volatile organic compound content is no greater than 115 ppm.

4. The propylene-based polymer resin of claim 1 , wherein the semi-volatile organic compound content is no greater than 175 ppm.

5. The propylene-based polymer resin of claim 1 , wherein the C36 oligomeric content is no greater than 220 ppm.

6. The propylene-based polymer resin of claim 1 , wherein the resin comprises a melt flow rate greater than 115 g/10 min.

7. The propylene-based polymer resin of claim 1 , wherein the resin comprises a crystallinity greater than 65%.

8. The propylene-based polymer resin of claim 1 , wherein the resin comprises a mesopentad content greater than 97%.

9. The propylene-based polymer resin of claim 1 , wherein the resin comprises a homopolymer polypropylene.

10. The propylene-based polymer resin of claim 1 , wherein the resin comprises a propylene-ethylene copolymer.

11. The propylene-based polymer resin of claim 1 , wherein the resin comprises a propylene-alpha olefin copolymer.

12. The propylene-based polymer resin of claim 11 , wherein the alpha olefin comprises at least one monomer selected from the group consisting of 1-butene, 1-pentene, 1-hexene, 1-heptene, 1-octene, 1-nonene, 1-decene, 1-undecene, 1-dodecene, and combinations of any thereof.

13. The propylene-based polymer resin of claim 1 , wherein the resin is an in-reactor resin.

14. An impact copolymer polypropylene composition comprising:

a rubber phase comprising a propylene-ethylene copolymer; and

a matrix phase comprising the propylene-based polymer resin of claim 1 .

15. A molded article comprising the propylene-based polymer resin of claim 1 .

16. A propylene-based polymer resin comprising:

a volatile organic compound content no greater than 125 ppm;

a semi-volatile organic compound content no greater than 500 ppm;

a C36 oligomeric content no greater than 250 ppm;

a melt flow rate greater than 30 g/10 min.;

a Mw/Mn of greater than 5;

a crystallinity greater than 50%; and

a mesopentad content greater than 92%, wherein the propylene-based polymer resin is produced utilizing a Zeigler-Natta catalyst.

17. The propylene-based polymer resin of claim 16 , wherein the resin is an in-reactor resin.

18. An impact copolymer propylene composition comprising:

a rubber phase comprising a propylene-ethylene copolymer; and

a matrix phase comprising the propylene-based polymer resin of claim 16 .

19. A molded article comprising the propylene-based polymer resin of claim 16 .

20. A homopolymer polypropylene resin comprising:

a volatile organic compound content no greater than 125 ppm;

a semi-volatile organic compound content no greater than 500 ppm;

a C36 oligomeric content no greater than 250 ppm;

a melt flow rate greater than 30 g/10 min.;

a crystallinity greater than 50%; and

a mesopentad content greater than 92%, wherein the propylene-based polymer resin is produced utilizing a Zeigler-Natta catalyst.

21. The homopolymer polypropylene resin of claim 20 , wherein the resin is an in-reactor resin.

22. An impact copolymer polypropylene composition comprising:

a rubber phase comprising a propylene-ethylene copolymer; and

a matrix phase comprising the homopolymer polypropylene resin of claim 20 .

23. A molded article comprising the homopolymer polypropylene resin of claim 20 .

24. The propylene-based polymer resin of claim 1 , wherein the resin has a Mw/Mn of greater than 5.

25. The propylene-based polymer resin of claim 1 , wherein the Zeigler-Natta catalyst is a non-metallocene Ziegler-Natta catalyst.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 29, 2018
From: SALEK, JEFFREY; CHAPPELL, MARK; DAWSON, BRYAN
To: BRASKEM AMERICA, INC.
Reel/Frame 047335/0110 →
Continuity (2)
Provisional Application 62249465 · Nov 2, 2015
Related Publication 20170121432A1 · May 4, 2017