IP Library Granted Patent US 10,711,146
Granted Patent B2
US 10,711,146 · App. 15/341,948 · Granted Jul 14, 2020

Method of three-dimensional printing

Inventors: Guerino G. Sacripante (Oakville, CA); Ke Zhou (Oakville, CA)
Assignee: XEROX CORPORATION
C09D11/104B29C48/05B29C48/92B29C64/106B29C64/118B29C64/30B33Y10/00B33Y70/00B33Y80/00B29C48/001B29C48/022B29C48/78B29C48/911B29C2948/92695B29C2948/92704B29K2067/00B29K2067/04B29K2995/002B29K2995/006B29L2009/00
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Quick Facts
Patent No.
US 10,711,146
App. No.
15/341,948
Granted
Jul 14, 2020
Kind
B2
Abstract

A sustainable material suitable for three-dimensional printing is disclosed. The sustainable material comprises a resin derived from a bio-based diacid monomer and a bio-based glycol monomer. The resulting sustainable material provides a much more robust 3-D printing material with different properties than conventional materials.

Claims (15)

1. A sustainable three-dimensional printing material comprising:

a filament consisting of:

a sustainable resin derived from a bio-based diacid monomer and bio-based glycol monomer;

wherein when the sustainable resin is polybutylene succinate, the weight average molecular weight of the sustainable resin is from about 10,000 grams/mole to about 500,000 grams/mole; further wherein the polybutylene succinate is produced through the reaction of bio-based succinic acid and 1,4-butane-diol as shown by the reaction scheme below:

wherein n is from about 100 to about 100,000;

a colorant; and

an optional conductive material.

2. The three-dimensional printing material of claim 1 , wherein the sustainable resin is derived from about 45 to about 55 percent by mole equivalent of bio-based diacid monomer, and from about 45 to about 55 percent by mole equivalent of the bio-based glycol monomer, provided that the sum of both is 100 percent.

3. The three-dimensional printing material of claim 1 , wherein the sustainable resin has a softening point of from about 120° C. to about 200° C.

4. The three-dimensional printing material of claim 1 , wherein the sustainable resin has a freezing point of from about 20° C. to about 60° C.

5. The three-dimensional printing material of claim 1 , wherein the sustainable resin has a viscosity of from about 200 centipoise to about 10,000 centipoise at 100° C. to about 200° C.

6. The three-dimensional printing material of claim 1 , wherein the sustainable resin has a melting point of from about 75° C. to about 150° C.

7. The three-dimensional printing material of claim 1 , wherein the sustainable resin is present in the sustainable material in an amount of from about 90% to about 99% by weight.

8. The three-dimensional printing material of claim 1 , wherein the colorant is present in the sustainable material in an amount of from about 1% to about 10% by weight.

9. The three-dimensional printing material of claim 1 having a Young's Modulus of from about 0.5 to about 5 gigapascals, and a Yield Stress of from about 10 to about 100 megapascals.

Assignments (10)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2025
From: XEROX CORPORATION
To: GENESEE VALLEY INNOVATIONS, LLC
Reel/Frame 073842/0479 →
SECOND LIEN NOTES PATENT SECURITY AGREEMENT Recorded Jul 2, 2025
From: XEROX CORPORATION
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 071785/0550 →
FIRST LIEN NOTES PATENT SECURITY AGREEMENT Recorded Apr 11, 2025
From: XEROX CORPORATION
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 070824/0001 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT RF 064760/0389 Recorded Feb 13, 2024
From: CITIBANK, N.A., AS COLLATERAL AGENT
To: XEROX CORPORATION
Reel/Frame 068261/0001 →
SECURITY INTEREST Recorded Feb 13, 2024
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 066741/0001 →
SECURITY INTEREST Recorded Nov 20, 2023
From: XEROX CORPORATION
To: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 065628/0019 →
SECURITY INTEREST Recorded Jun 22, 2023
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 064760/0389 →
RELEASE OF SECURITY INTEREST IN PATENTS AT R/F 062740/0214 Recorded May 18, 2023
From: CITIBANK, N.A., AS AGENT
To: XEROX CORPORATION
Reel/Frame 063694/0122 →
SECURITY INTEREST Recorded Nov 10, 2022
From: XEROX CORPORATION
To: CITIBANK, N.A., AS AGENT
Reel/Frame 062740/0214 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 2, 2016
From: SACRIPANTE, GUERINO G.; ZHOU, KE
To: XEROX CORPORATION
Reel/Frame 040202/0159 →
Continuity (2)
Division 14537215 · Nov 10, 2014
Related Publication 20170051168A1 · Feb 23, 2017