IP Library Granted Patent US 10,596,728
Granted Patent B2
US 10,596,728 · App. 15/379,260 · Granted Mar 24, 2020

Polymer powder for powder bed fusion methods

Inventors: Wolfgang Diekmann (Waltrop, DE); Maik Grebe (Bochum, DE)
Assignee: Evonik Operations GmbH
B29B9/16B29C64/153C08G69/08C08G69/26C08J3/128C08K5/01B29B2009/163B29K2077/00B29K2105/251B29K2995/0093B33Y10/00B33Y70/00C08J2300/22C08J2377/02C08J2377/06C08K2201/013
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Quick Facts
Patent No.
US 10,596,728
App. No.
15/379,260
Granted
Mar 24, 2020
Kind
B2
Abstract

A polymer powder having a surface energy of less than 35 mN/m is suitable for melting/sintering powder particles for layer-by-layer production of three-dimensional objects.

Claims (28)

1. A method for producing a polymer powder having a surface energy of less than 35 mN/m, said method comprising:

coating a polymer powder with a hydrophobic substance, thereby obtaining the polymer powder having a surface energy of less than 35 mN/m.

2. The method according to claim 1 , wherein the coating is effected at a temperature of not more than 100° C.

3. The method according to claim 1 , wherein the coating is effected in a suspension.

4. The method according to claim 1 , wherein said hydrophobic substance is selected from the group consisting of alkanes, alkenes and mixtures thereof.

5. The method according to claim 1 , wherein the polymer of the polymer powder is at least one member selected from the group consisting of a polyamide and a copolyamide.

6. The method according to claim 1 , wherein the polymer powder has a Wadell sphericity is at least 0.5.

7. The method according to claim 1 , wherein the polymer powder has a surface energy of less than 32 mN/m.

8. The method according to claim 1 , wherein the polymer powder has a surface energy of less than 30 mN/m.

9. The method according to claim 1 , wherein a proportion of the hydrophobic substance accounts for 0.15% to 20% by weight, based on the total weight of polymer powder and the hydrophobic substance.

10. The method according to claim 1 , wherein the hydrophobic substance has a melting point of not more than 160° C. and a boiling point of at least 190° C.

11. A powder bed fusion method, comprising:

selectively laser sintering, selectively absorbing sintering, or selectively inhibition sintering a polymer powder having a surface energy of less than 35 mN/m.

12. A shaped body obtainable by the method according to claim 11 .

13. The method according to claim 11 , wherein the polymer of the polymer powder is at least one member selected from the group consisting of a polyamide and a copolyamide.

14. The method according to claim 11 , wherein the polymer powder has a Wadell sphericity is at least 0.5.

15. The method according to claim 11 , wherein the polymer powder has a surface energy of less than 32 mN/m.

16. The method according to claim 11 , wherein the polymer powder has a surface energy of less than 30 mN/m.

17. The method according to claim 11 , wherein

said polymer powder comprises a hydrophobic substance on a surface thereof, and

a proportion of the hydrophobic substance accounts for 0.15% to 20% by weight, based on the total weight of polymer powder and the hydrophobic substance.

18. The method according to claim 11 , wherein

said polymer powder comprises a hydrophobic substance on a surface thereof, and

the hydrophobic substance has a melting point of not more than 160° C. and a boiling point of at least 190° C.

19. The method according to claim 11 , wherein

said polymer powder comprises a hydrophobic substance on a surface thereof, and

said hydrophobic substance is selected from the group consisting of alkanes, alkenes, and mixtures thereof.

20. The method according to claim 11 , wherein surface energy is determined by a contact angle method.

Assignments (2)
CHANGE OF NAME Recorded Nov 18, 2019
From: EVONIK DEGUSSA GMBH
To: EVONIK OPERATIONS GMBH
Reel/Frame 051045/0872 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 23, 2017
From: DIEKMANN, WOLFGANG; GREBE, MAIK
To: EVONIK DEGUSSA GMBH
Reel/Frame 041046/0257 →
Priority Claims (1)
EP 15199919 · Dec 14, 2015 · regional
Continuity (1)
Related Publication 20170165913A1 · Jun 15, 2017
Cited By (1)
US 12,605,909