IP Library Granted Patent US 10,440,974
Granted Patent B2
US 10,440,974 · App. 15/399,764 · Granted Oct 15, 2019

Methionine-rich composition for feeding animals

Inventor: Patrick Fuertes (Lomme, FR)
Assignee: Evonik Degussa GmbH
A23K20/142A23L5/20C12P13/06C12P13/12A23V2002/00
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Quick Facts
Patent No.
US 10,440,974
App. No.
15/399,764
Granted
Oct 15, 2019
Kind
B2
Abstract

The present invention relates to a novel liquid or crystalline methionine composition, obtained by means of biomass bioconversion by means of microorganisms that are suitable for producing methionine.

Claims (62)

1. A feed additive for feeding animals comprising a methionine composition resulting from a fermentation process, said methionine composition comprising:

from 60 to 95% by weight of methionine;

from 0.05 to 2.5% by weight of N-acetylmethionine; and

from 0.05 to 3.5% by weight of isoleucine.

2. The feed additive of claim 1 , said methionine composition further comprising:

from 1.0 to 6.0% by weight of amino acids other than methionine, N-acetylmethionine and isoleucine;

from 0.1 to 2% by weight of total sugars; and

from 0.05 to 2.5% by weight of lipids.

3. The feed additive of claim 1 , wherein said additive is a liquid.

4. The feed additive of claim 1 , wherein said methionine composition comprises:

from 60 to 80% by weight of methionine;

from 0.5 to 2.0% by weight of N-acetylmethionine; and

from 0.20 to 1.5% by weight isoleucine.

5. The feed additive of claim 2 , said methionine composition further comprising:

from 2 to 6% by weight of amino acids other than methionine, N-acetylmethionine and isoleucine;

from 0.5 to 2% by weight of total sugars; and

from 0.05 to 2.5% by weight of lipids.

6. The feed additive of claim 1 , said methionine composition comprising:

from 70 to 90% by weight of methionine;

from 0.05 to 2.5% by weight of N-acetylmethionine; and

from 0.10 to 1.0% by weight of isoleucine.

7. The feed additive of claim 2 , said methionine composition further comprising:

from 2 to 6% by weight of amino acids other than methionine, N-acetylmethionine and isoleucine;

from 0.25 to 2% by weight of total sugars; and

from 0.05 to 2.5% by weight of lipids.

8. The feed additive of claim 2 , wherein said additive is a liquid.

9. The feed additive of claim 1 , said methionine composition comprising:

from 80 to 95% by weight of methionine;

from 0.05 to 0.5% by weight of N-acetylmethionine; and

from 0.05 to 5.0% by weight of isoleucine.

10. The feed additive of claim 2 , said methionine composition further comprising:

from 1.0 to 5.0% by weight of amino acids other than methionine, N-acetylmethionine and isoleucine;

from 0.1 to 1.5% by weight of total sugars, and less than 0.3% by weight of lipids.

11. A process for preparing the feed additive of claim 1 comprising:

clarifying fermentation medium in which a microorganism that has been modified to produce methionine has been cultured and removing insoluble and soluble organic impurities from said fermentation medium to obtain a liquid crude composition; and

recovering the feed additive.

12. The process for preparing a feed additive of claim 11 , wherein the liquid crude composition further comprises:

from 2 to 6% by weight of amino acids other than methionine, N-acetylmethionine and isoleucine;

from 0.1 to 2% by weight of total sugars; and

from 0.05 to 2.5% by weight of lipids.

13. The process for preparing a feed additive of claim 11 , said process further comprising:

demineralizing the liquid crude solution in order to remove cations and anions from said fermentation medium to obtain a demineralized liquid crude composition comprising:

from 70 to 90% by weight of methionine;

from 0.05 to 2.5% by weight of N-acetylmethionine; and

from 0.10 to 1.0% by weight of isoleucine.

14. The process for preparing a feed additive of claim 13 , said demineralized liquid crude composition further comprising:

from 2 to 6% by weight of amino acids other than methionine, N-acetylmethionine and isoleucine;

from 0.25 to 2% by weight of total sugars; and

from 0.05 to 2.5% by weight of lipids.

15. The process for preparing a feed additive of claim 11 , wherein the feed additive is liquid and said process does not comprise a crystallization step.

16. The process for preparing a feed additive of claim 11 , further comprising:

crystallizing solid crude methionine from an optionally demineralized, liquid crude composition.

17. The process for preparing a feed additive of claim 16 , said method further comprising:

separating, optionally washing, and optionally milling methionine crystals in order to obtain a solid crude composition.

18. The process for preparing a feed additive of claim 16 , wherein said solid crude composition comprises:

from 80 to 95% by weight of methionine;

from 0.05 to 0.5% by weight of N-acetylmethionine; and

from 0.05 to 5.0% by weight of isoleucine.

19. The process for preparing a feed additive of claim 18 , wherein the solid crude methionine composition further comprises:

from 1.0 to 5.0% by weight of amino acids other than methionine, N-acetylmethionine and isoleucine;

from 0.1 to 1.5% by weight of total sugars; and

less than 0.3% by weight of lipids.

Assignments (4)
CHANGE OF NAME Recorded Nov 18, 2019
From: EVONIK DEGUSSA GMBH
To: EVONIK OPERATIONS GMBH
Reel/Frame 051045/0872 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 20, 2017
From: METABOLIC EXPLORER
To: EVONIK DEGUSSA GMBH
Reel/Frame 042752/0744 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 6, 2017
From: FUERTES, PATRICK
To: ROQUETTE FRERES
Reel/Frame 040869/0770 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 6, 2017
From: ROQUETTE FRERES
To: METABOLIC EXPLORER
Reel/Frame 040869/0778 →
Priority Claims (1)
FR 09 57183 · Oct 14, 2009 · national
Continuity (2)
Continuation 13501490
Related Publication 20170112166A1 · Apr 27, 2017