IP Library Granted Patent US 10,485,257
Granted Patent B2
US 10,485,257 · App. 15/400,325 · Granted Nov 26, 2019

Method of making steviol glycosides

Inventors: Avetik Markosyan (Yerevan, AM); Cyrille Jarrin (Muret, FR); Patrick Robe (Lanta, FR); Rob ter Halle (Beziege, FR); Indra Prakash (Alpharetta, GA); Venkata Sai Prakash Chaturvedula (Alpharetta, GA)
Assignee: PureCircle Sdn Bhd
A23L27/36C07H15/24C12P19/18C12P19/56C12Y204/01A23V2002/00Y02P20/582
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Quick Facts
Patent No.
US 10,485,257
App. No.
15/400,325
Granted
Nov 26, 2019
Kind
B2
Abstract

Methods of preparing highly purified steviol glycosides, particularly rebaudiosides A, D and X are described. The method includes expression of UDP-glucosyltransferases from Stevia rebaudiana Bertoni, which are capable converting certain steviol glycosides to rebaudiosides A, D and X. The highly purified rebaudiosides A, D and X, are useful as non-caloric sweetener in edible and chewable compositions such as any beverages, confectioneries, bakery products, cookies, and chewing gums.

Claims (7)

1. A method for adding at least one glucose unit to a steviol glycoside substrate to provide a target steviol glycoside, comprising contacting the steviol glycoside substrate with a recombinant biocatalyst protein enzyme comprising UDP-glucosyltransferase, wherein the target steviol glycoside is Rebaudioside X.

2. The method of claim 1 , wherein the steviol glycoside substrate is selected from the group consisting of steviolmonoside, steviolbioside, nibusoside, rebaudioside E, rebaudioside Ci, rebaudioside 1 , stevioside, rebaudioside A, rebaudioside D, synthetic steviol glycosides and combinations thereof.

3. The method of claim 1 , further comprising the step of purifying the Rebaudioside X to a purity of greater than about 80% by weight.

4. The method or claim 1 , further comprising the step of purifying, the Rebaudioside X to a purity of greater than about 90% by weight.

5. The method of claim 1 , further comprising the step of purifying the Rebaudioside X to a purity of greater than about 95% by weight.

6. The method of claim 1 , wherein the UDP-glucosyltransferase is expressed in a host microorganism.

7. The method of claim 6 , wherein the host microorganism is selected from the group consisting of: Escherichia coli, Saccharomyces species, Aspergillus species, and Pisehia species.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 11, 2019
From: MARKOSYAN, AVETIK; JARRIN, CYRILLE; ROBE, PATRICK; TER HALLE, ROB
To: PURECIRCLE SDN BHD; LIBRAGEN S.A.
Reel/Frame 050690/0898 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 11, 2019
From: LIBRAGEN S.A.
To: PURECIRCLE SDN BHD
Reel/Frame 050690/0903 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 11, 2019
From: PRAKASH, INDRA
To: THE COCA-COLA COMPANY
Reel/Frame 050690/0925 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 11, 2019
From: CHATURVEDULA, VENKATA SAI PRAKASH
To: THE COCA-COLA COMPANY
Reel/Frame 050690/0935 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 5, 2018
From: THE COCA-COLA COMPANY
To: PURECIRCLE SDN BHD
Reel/Frame 046787/0788 →
Continuity (5)
Continuation 14954213 · Nov 30, 2015
Division 14469076 · Aug 26, 2014
Continuation PCTUS2013030439 · Mar 12, 2013
Provisional Application 61649978 · May 22, 2012
Related Publication 20170112176A1 · Apr 27, 2017
Cited By (1)
US 12,371,677